References
- We wish to thank Prof. Nathan Kornblum for his advice and guidance during the initial phase of this work
- 1978 . Presented in part at the 30th Annual Southeastern Regional Meeting of the American Chemical Society . November 8–10 1978 , Savannah, Georgia.
- Sodium hypophosphite (Baker analyzed reagent) was dried overnight at 130° in vacuum. Triethyloxonium tetrafluoroborate was prepared from epichlorohydrin.4
- Meerwein , H. , Battenberg , E. , Gold , H. , Pfeil , E. and Willfang , J. 1939 . J. Prakt. Chem. , 54 : 83 N. Kornblum and R. A. Brown, J. Am. Chem. Soc., 86, 2681 (1964)
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- Fitch , S. J. 1964 . J. Am. Chem. Soc. , 86 : 61
- Gallagher , M. J. and Honegger , H. 1978 . J. Chem. Soc. Chem. Comm. , : 54 This exchange reaction has been studied recently
- Ivanov , B. E. and Kudryavtseva , L. A. 1968 . C. A. , 68 : 78359 Propyl hypophosphite and larger esters are available by the direct esterification of hypophosphorous acid: E. E. Nifant'ev and L. P. Levitan, C. A. 63, 4152a (1965)