References
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- Eisch , J. J. and Galle , J. E. 1976 . J. Org. Chem. , 41 : 2615 Additional pyrolyses of α,β–epoxysilanes have been reported in the following papers M. Lesbre, G. Bertrand, G. Manuel, and P. Mazerolles, C. R. Acad. Sci. Paris, Ser. C, 284, 709(1977)
- Vapor phase chromatographic (VPC) analyses were performed on a Varian model 90-P instrument using helium as the carrier gas, using a 20 ft × 0.25 in. aluminum column packed with 25% Car-bowax 20M on Chromosorb W
- Neumann , H. and Seebach , D. 1976 . Tetrahedron Lett. , : 4839 We have also prepared the trans vinyl si lane 1b6b from the corresponding vinyl iodide by treatment with t-BuLi followed by Me3SiCl The vinylsilane from that procedure was contaminated with 1–2% of the cis isomer
- CHCl3 (δ 7.25) was used as the internal reference
- From a separate but similar experiment (on a smaller scale)