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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 9, 1979 - Issue 8
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Original Articles

Synthesis and Characterization of Certain 5-Alkoxydihydro-2(3H)-Furanones

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Pages 683-688 | Received 13 Apr 1979, Published online: 05 Dec 2006

References

  • Muller , C. J. , Kepner , R. E. and Webb , A. D. 1973 . Amer. J. Enol. Viticult. , 24 : 5
  • Kuwamura , T. and Takahashi , H. 1969 . Bull. Chem. Soc. Jap. , 42 : 1345
  • Fairbourne , A. , Gibson , G. P. and Stephens , D. W. 1932 . J. Chem. Soc. , : 1965
  • Webb , A. D. , Eriksson , K. , Muller , C. J. and Kepner , R. E. 1976 . Amer. J. Enol. Viticult. , 27 : 27
  • Stevens , M. A. E. I. duPont de Nemours and Company . U.S. Patent #2, 859, 218 . 1958 .
  • Schenck , G. O. 1953 . Liebigs Ann. Chem. , 584 : 156
  • This was found to be especially true of the products resulting from ethanol
  • An exception to this was the 5-(2-phenylethoxy)-2(5H)-furanone which required 24 hours under the same reaction conditions to undergo reduction
  • Spinning band distillation was necessary to get a pure sample of the 5-ethoxydihydro-2(3H)-furanone
  • Kovats , E. 1965 . Advan. Chromatog. , 1 : 229 Retention indices were calculated as recommended by Kovats
  • The 5-(2-phenylethoxy)dihydro-2(3H)-furanone did not give a sufficiently well-formed peak under any chromatographic conditions tried to permit calculation of meaningful retention indices

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