A Convenient Procedure for Preparative Scale Oxidation of Enones

References

• Stork , G. , Meisels , A. and Davies , J. E. 1963 . J. Am. Chem. Soc. , 85 : 3419
   Google Scholar
• Wolfe , S. , Hasan , S. K. and Campbell , J. R. 1970 . J. Chem. Soc., Chem. Comm. , : 1420
   Google Scholar
• von Rudloff , E. 1956 . Can. J. Chem. , 33 : 1714
   Google Scholar
• Pappo , R. and Jung , C. J. 1962 . Tetrahedron Lett. , : 365
   Google Scholar
• Turner , R. B. 1950 . J. Am. Chem. Soc. , 72 : 579
   Web of Science ®Google Scholar
• Corey , E. J. and Boger , D. L. 1978 . Tetrahedron Lett. , : 4597
   Google Scholar
• Heathcock , C. H. and Chaudarian , C. G. 1975 . J. Org. Chem. , 40 : 2970
   PubMedGoogle Scholar
• Belew , J. S. 1969 . “Oxidation,” , 321 New York : Marcel Dekker, Inc. .
   Google Scholar
• In one experiment a sample obtained from a nitric acid workup of a conventional ozonolysis decomposed violently on standing. Prior analysis of this sample did not reveal the presence of ozonide or hydroperoxide. This occurance gave ample support for the need of a safe workup procedure.
   Google Scholar
• Methyltrialkyl (C8-C10) ammonium chloride. Registered trademark of Ashland Chemical Co., Division of Ashland Oil.
   Google Scholar
• Henshall , T. , Silbermann , W. E. and Webster , J. G. 1955 . J. Am. Chem. Soc. , 77 : 6656
   Google Scholar
• Identical to published spectrum: Pouchert, C. J. and Campbell, J. R., “The Aldrich Library of NMR Spectra,” V.II. Spectrum 179-D.
   Google Scholar