References
- Takeda , M. and Kaito , M. 1981 . J. Synthetic Org. Chem. Jpn. , 39 : 39
- Morita , K. , Suzuki , Z. and Hirose , H. 1968 . Bull. Chem. Soc. Jpn. , 41 : 41 see also Miyakoshi, T., Omichi, H., Saito, S., Nippon Kagaku Zasshi, 1979, 748
- Compared with 5, trimethylaluminium gave a marked decrease (55%) in the yield of the adduct under the same conditions.
- CH2Cl2 is the solvent of choice, compared to THF, CH3CN, PhH, or t-BuOH
- When α,β-unsaturated aldehydes (cinnamaldehyde and 2-hexenal) were used instead of the saturated aldehyde under the sarre reaction conditions, only 1,2-adducts were obtained in low yield (19% and 9%, respectively).
- Baizer , M. M. and Anderson , J. D. 1965 . J. Org. Chem. , 30 : 30
- McLure , J. D. 1970 . J. Org. Chem. , 35 : 35
- Hoffmann , H. M. R. and Rabe , J. 1983 . Angew. Chem. Int. Ed. Engl. , 22 : 22 Two interesting reports of the synthesis of 2-(1-hydroxy-alkyl acrylic esters have appeared recently
- Papageorgion , C. and Benezra , C. 1984 . Tetrahedron Lett. , 25 : 25
- All nmr spectra were obtained as CDCl3 solution