References
- David Ladd , L. and Weinstock , Joseph . 1981 . J. Org. Chem. , 46 : 203
- Identified as the trimethoxy derivative (2a, mp: 91–92. 5°C, acetone) which was prepared by refluxing 2 with excess dimethyl sulfate and K2CO3 in acetone; 360 MHz lH NMR (CDCl3) showed three OCH3's at 3. 67, 3. 77 and 3. 92; CI mass spectrum m/e 263 (M+H). Anal. Calcd for Cl5Hl5FO3: C, 68.69; H, 5. 76. Found: C, 68. 65; H, 5. 77
- Wakefield , B. J. 1974 . “The Chemistry of Organolithium Compounds” , 172 Oxford : Pergamon Press .
- Ogino , T. and Mochizuki , K. 1979 . Chem. Lett. , 443
- Godfrey , I. M. , Sargent , M. V. and Elix , J. A. 1974 . J. C. S. Perkin I , 1353
- Suzuki , Y. and Takahashi , H. 1983 . Chem. Pharm. Bull. , 31 : 1751
- GC/MS showed two components with m/e 353 [(M+H)+ corresponding to ll] and two components with m/e 492 (M+ corresponding to 12). GC/IR showed two components with aromatic aldehyde carbonyl absorption at 1706 cm−l corresponding to 11 and nine components lacking carbonyl absorptions and differing only in the 1142–1008 cm−1 region (aromatic C-F and ring substitutions) consistent with the isomers of 12
- Ogata , Y. , Kowasaki , A. and Sugiura , F. 1968 . Tetrahedron , 24 : 5001
- U. S. Patent, 4, 124, 643 . 1978 . (To UOP, Inc., Des Plains, Ill.)
- Kirk , K. L. 1976 . J. Org. Chem. , 41 : 2373