A New Synthesis of α-Cyano Substituted Vinyl Sulfides Using Cyano(methylthio)Methyltrimethylsilane

References

• Mignani , S. , Beaujean , M. , Janousek , A. , Merenyi , R. and Viehe , H. G. 1981 . Tetrahedron , 37 ( Supplement No. 1 ) : 111
   Google Scholar
• Warren , S. 1980 . Chem. Ind. , : 824 and references cited therein
   Google Scholar
• Durman , J. , Hunt , P. G. and Warren , S. 1983 . Tetrahedron Lett. , 24 : 2113
   Google Scholar
• Sella , L. and Boucher , J. L. 1982 . Tetrahedron Lett. , 23 : 953
   Google Scholar
• Gundermann , K. D. and Röhrl , E. 1974 . Liebigs Ann. Chem. , : 1661
   Google Scholar
• Pochat , F. 1978 . Tetrahedron Lett. , : 2683
   Google Scholar
• Dinizo , S. E. , Freerksen , R. W. , Pabst , W. E. and Watt , D. S. 1976 . J. Org. Chem. , 41 : 2846
   Web of Science ®Google Scholar
• Silylation of alkanephosphonates has been described
   Google Scholar
• Aboujaoude , E. E. , Liétjé , S. and Collignon , N. 1986 . Synthesis , : 934
   Google Scholar
• Kawashima , T. , Ishii , T. and Inamoto , N. 1987 . Bull. Chem. Soc. Jpn. , 60 : 1831
   Web of Science ®Google Scholar
• Emde , H. and Simchen , G. 1977 . Synthesis , : 636 For a example of the silylation of other α-substituted acetonitrile with TMSOTf, see:
   Google Scholar
• Characteristic of (2): bp 72–74°C/4 mmHg 1H NMR (CDC13) δ 0.28 (S, 9H), 2.35 (s, 3H), 280 (S, 1H) IR (neat) Cm−1 2225 (CN)
   Google Scholar