References
- Mignani , S. , Beaujean , M. , Janousek , A. , Merenyi , R. and Viehe , H. G. 1981 . Tetrahedron , 37 ( Supplement No. 1 ) : 111
- Warren , S. 1980 . Chem. Ind. , : 824 and references cited therein
- Durman , J. , Hunt , P. G. and Warren , S. 1983 . Tetrahedron Lett. , 24 : 2113
- Sella , L. and Boucher , J. L. 1982 . Tetrahedron Lett. , 23 : 953
- Gundermann , K. D. and Röhrl , E. 1974 . Liebigs Ann. Chem. , : 1661
- Pochat , F. 1978 . Tetrahedron Lett. , : 2683
- Dinizo , S. E. , Freerksen , R. W. , Pabst , W. E. and Watt , D. S. 1976 . J. Org. Chem. , 41 : 2846
- Silylation of alkanephosphonates has been described
- Aboujaoude , E. E. , Liétjé , S. and Collignon , N. 1986 . Synthesis , : 934
- Kawashima , T. , Ishii , T. and Inamoto , N. 1987 . Bull. Chem. Soc. Jpn. , 60 : 1831
- Emde , H. and Simchen , G. 1977 . Synthesis , : 636 For a example of the silylation of other α-substituted acetonitrile with TMSOTf, see:
- Characteristic of (2): bp 72–74°C/4 mmHg 1H NMR (CDC13) δ 0.28 (S, 9H), 2.35 (s, 3H), 280 (S, 1H) IR (neat) Cm−1 2225 (CN)