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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 18, 1988 - Issue 12
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Original Articles

The Reaction of Organoboranes with Trimethylsilyl Azide in a Neutral Medium: Synthesis of Primary Amines

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Pages 1363-1369 | Published online: 19 Dec 2006

References

  • Morris , D. R. and Marton , L. J. , eds. 1981 . Polyamines in Biology and Medicine , New York : Marcel Dekker, Inc .
  • Kabalka , G. W. , Henderson , D. A. and Varma , R. S. 1987 . Orctanometallics , 6 : 1369
  • Methoxytrimethylsilane was independently prepared via the reaction of chlorotrimethylsilane with excess methanol in presence of pyridine. The 29Si-NMR revealed a singlet at 17.75 ppm corresponding to methoxytrimethylsilane. See: Silicon Compounds, Register and Review, Petrarch Systems Silanes & Silicones, p 62, 1987
  • Kabalka , G. W. and Hedgeock , H. C. Jr . 1975 . J. Org. Chem. , 40 : 1776
  • Gilsdorf , R. T. and Nord , F. F. 1952 . J. Am. Chem. Soc. , 74 : 1837
  • Vogel , A. 1981 . Textbook of Practical Organic Chemistry , London : Longman .
  • Adamson , D. W. and Kenner , J. 1934 . J. Chem. Soc. , : 838
  • Alder , K. and Stein , G. 1936 . Justus Liebigs Ann. Chem. , 523 : 183
  • Breur , G. and Schnitzer , J. 1936 . J. Monatsh. Chem. , 68 : 301
  • Kabalka , G. W. , Sastry , K. A. R. , McCollum , G. W. and Yoshika , H. 1981 . J. Ora. Chem. , 46 : 4296
  • Freund and König . 1893 . Ber. , 26 : 2875
  • Attempts to isolate the hydrochloride and picrate salte of 5-benzoxy hexylamine failed

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