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- Crystal data for 2. C12H16O2, M = 384.5, Space group PT, a = 6.630 (1), b = 9.073 (2), c = 9.836 (2) A0 · α = 90.14 (3), β = 105.14 (3), λ = 92.85 (3), U = 527.34 A3. DC = 1.211g cm−3, Z = 2, F (000) = 208.0, μ(MO–Kα) = 0.08 MM−1, λ = 0.71069nm. Of 1546 reflections collected, 1255 reflections I 3 σ (I) were used for calculations. The structure was solved by direct methods. The hydrogen atoms were located from a fourier map. The full-matrix least squares refinement was completed using anisotropic thermal parameters for all non-hydrogen atoms. The final R was 0.0357 and RW = 90.0436, where W = 1/(σ2 (F) + 0.00188 F2). The number of parameters refined were 129 and the goodness of fit is 2.90
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