Publication Cover
Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 23, 1993 - Issue 3
52
Views
4
CrossRef citations to date
0
Altmetric
Original Articles

Synthesis of Spirodiones and Their Structure Determination by X-Ray Crystallography

, , , , &
Pages 297-310 | Received 10 Aug 1992, Published online: 23 Sep 2006

References

  • Craig Jaspere , P. G. , Curran , Dennis P. and Thomas Ferig , L. 1991 . Chem. Rev. , 91 : 1237
  • Curran , D. P. 1991 . Syn. Lett. , : 63
  • Curran , D. P. 1988 . Synthesis. , : 417 & 489
  • Ramiah , M. 1987 . Tetrahedron. , 43 : 3541
  • Giese , B. 1985 . Angew. Chem. Int. Ed. Engl. , 24 : 553
  • Giese , B. 1986 . Radicals in Organic Synthesis: formation of Carbon—Carbon bonds , Oxford : Pergamon press .
  • Hart , D. J. 1984 . Science. , : 223 & 883
  • Beckwith , A. L. J. 1981 . Tetrahedron. , 37 : 3073
  • Janardhanam , S. , Balakumar , A. and Rajagopalan , K. (Communicated)
  • Janardhanam , S. , Shanmugam , P. and Rajagopalan , K. (Communicated)
  • Stork , Gilbert and Robert , Mook Jr. 1987 . J. Am. Chem. Soc. , 109 : 2829 – 31 .
  • Nozaki , Kyoko , Oshima , Koichio and Utimoto , Kittiro . 1987 . J. Am. Chem. Soc. , 109 : 2547 – 49 .
  • Vijaya Bhaskar , K. and Subba Rao , G. S. R. 1989 . Tetrahedron Lett. , 30 : 225
  • Robert , Mook Jr. and Michael Sher , Philip . 1988 . Org. Syn. , 66 : 75 – 80 .
  • Biggs , Karsen R. , Parsens , Philip T. , David , J. Tapolzcay and Mark Underwood , J. 1989 . Tetrahedron Lett. , 30 : 7115 – 16 .
  • Lee , Eun , Hur , Changur and Min Park , Cheol . 1990 . Tetrahedron Lett. , 31 : 5039 – 40 .
  • Middleton , Donald S. and Nigel Simpkins , S. 1990 . Tetrahedron. , 46 : 545 – 64 .
  • Eric Enholm , J. , Buoff , J. A. and Luz Jaramillo , M. 1990 . Tetrahedron Lett. , 31 : 3737 – 30 .
  • Moufid , Nadira and Cahpluer , Yves . 1991 . Treahedron Lett. , 32 : 1799 – 1802 .
  • Pak , H. , Canalda , I. I. and Fraser-Reid , B. 1990 . J. Org. Chem. , 55 : 3009
  • Hayashi , Tamio , Kanehira , Koichi , Hagihara , Toshiya and Kumuda , Makotv . 1988 . J. Org. Chem. , 53 : 113 – 20 .
  • Ganesh Raj , S. P. 1988 . Ph. D. Thesis University of Madras .
  • Brunner , Henri and Kraus , Jorg . 1989 . J. Mol. Catalysis. , 49 : 133 – 142 .
  • Paquette , L. A. 1990 . Angew. Chem. Int. Ed. Engl. , 29 : 609 – 626 .
  • Crystal data for 2. C12H16O2, M = 384.5, Space group PT, a = 6.630 (1), b = 9.073 (2), c = 9.836 (2) A0 · α = 90.14 (3), β = 105.14 (3), λ = 92.85 (3), U = 527.34 A3. DC = 1.211g cm−3, Z = 2, F (000) = 208.0, μ(MO–Kα) = 0.08 MM−1, λ = 0.71069nm. Of 1546 reflections collected, 1255 reflections I 3 σ (I) were used for calculations. The structure was solved by direct methods. The hydrogen atoms were located from a fourier map. The full-matrix least squares refinement was completed using anisotropic thermal parameters for all non-hydrogen atoms. The final R was 0.0357 and RW = 90.0436, where W = 1/(σ2 (F) + 0.00188 F2). The number of parameters refined were 129 and the goodness of fit is 2.90
  • Plamondon , Josee and Cannone , Persephone . 1991 . Tetrahedron Lett. , 32 : 589 – 592 .

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.