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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 27, 1997 - Issue 1
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Original Articles

A Simple Procedure for the Preparation of 4-(α-Mercaptobenzyl)Phenoxyacetic Acid, A Thiol Linker Unit Used in Solid Phase Synthesis of Peptide-α-Thioacids

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Pages 187-194 | Received 07 Jul 1996, Published online: 19 Aug 2006

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  • HPLC Assay: Column: PLRP-S, 300Å (50x7.5 mm); A=H2O (0.1% CF3COOH); B=90:10 CH3CN/H2O(0.1% CF3COOH); detection at 260 nm; flow rate 2 mL/min; linear gradient program: 1% to 90% B in 30 min. tR 3=17.4 min and 5=21.8 min
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