Easy Preparation of Collman-Type Reagents: Reaction Of [HFe(Co)₄]⁻ with tris(Dimethylamino)phosphine

References and notes

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• A color change from brown-pink to yellow is observed, but IR and 31P NMR monitoring of the solution do not indicate any transformation. Such a triggerring by evaporation has been reported for the synthesis of [Et4N]+, [HFe(CO)3(PPh3)]-, a precursor for [Fe(CO)3(PPh3)]2-, a monophosphorus analog of the Collman dianion: Chen, Y. S. and Ellis, J. E., J. Am. Chem. Soc., 1982, 104, 1141.
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• Brunet , J.-J. , Chauvin , R. , Diallo , O. , Donnadieu , B. , Jaffart , J. and Neibecker , D. in press . manuscript in preparation
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