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- Some characterization data for new compounds : 2b: oil, 1H NMR (CDCl3): δ 3.95 (s, 3H), 5.45 (s, 2H), 6.78 (d, 2H, J = 9.0 Hz), 7.08 (d, 2H, J = 9.0 Hz). IR (Neat) μ 1550 and 1355 cm−1 (NO2). 7b : oil, 1H NMR (CDCl3): δ 5.52 (s, 2H), 6.85 (d, 2H, J = 9.0 Hz), 7.42 (s, 1H). Compound 3b b.p. is compared with authentic sample obtained from Aldrich Chemical Co
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