69
Views
2
CrossRef citations to date
0
Altmetric
Research Article

Enhanced Matrix Removal-Lipid (EMR-L): a novel approach for efficient clean-up in systemic toxicological analysis of drugs and pesticides

, , , , , , , & show all
Received 28 Jun 2023, Accepted 05 Sep 2023, Published online: 21 Sep 2023

References

  • Anastassiades M, Lehotay SJ, Štajnbaher D, Schenck FJ. Fast and easy multiresidue method employing acetonitrile extraction/partitioning and “Dispersive solid-phase extraction” for the determination of pesticide residues in produce. J AOAC Int. 2003;86(2):412–431. doi:10.1093/jaoac/86.2.412
  • De Berardis S, De Paola EL, Montevecchi G, Garbini D, Masino F, Antonelli A, Melucci D. Determination of four Alternaria alternata mycotoxins by QuEChERS approach coupled with liquid chromatography-tandem mass spectrometry in tomato-based and fruit-based products. Food Res Int. 2018;106:677–685. doi:10.1016/j.foodres.2018.01.032
  • González-Curbelo MÁ, Varela-Martínez DA, Riaño-Herrera DA. Pesticide-residue analysis in soils by the QuEChERS method: a review. Molecules. 2022;27(13):4323. doi:10.3390/molecules27134323
  • Lehotay SJ. Determination of pesticide residues in foods by acetonitrile extraction and partitioning with magnesium sulfate: collaborative study. J AOAC Int. 2007;90(2):485–520. doi:10.1093/jaoac/90.2.485
  • González-Curbelo MÁ, Socas-Rodríguez B, Herrera-Herrera AV, González-Sálamo J, Hernández-Borges J, Rodríguez-Delgado MÁ. Evolution and applications of the QuEChERS method. TrAc Trend Anal Chem. 2015;71:169–185. doi:10.1016/j.trac.2015.04.012
  • Usui K, Hashiyada M, Hayashizaki Y, Igari Y, Hosoya T, Sakai J, Funayama M. Application of modified QuEChERS method to liver samples for forensic toxicological analysis. Forensic Toxicol. 2014;32:139–147. doi:10.1007/s11419-013-0199-0
  • Mizuno S, Lee XP, Fujishiro M, Matsuyama T, Yamada M, Sakamoto Y, Kusano M, Zaitsu K, Hasegawa C, Hasegawa I, et al. High-throughput determination of valproate in human samples by modified QuEChERS extraction and GC-MS/MS. Leg Med. 2018;31:66–73. doi:10.1016/j.legalmed.2018.01.002
  • Bragança I, Plácido A, Paíga P, Domingues VF, Delerue-Matos C. QuEChERS: a new sample preparation approach for the determination of ibuprofen and its metabolites in soils. Sci Total Environ. 2012;433:281–289. doi:10.1016/j.scitotenv.2012.06.035
  • Jeong IS, Kwak BM, Ahn JH, Jeong SH. Determination of pesticide residues in milk using a QuEChERS-based method developed by response surface methodology. Food Chem. 2012;133(2):473–481. doi:10.1016/j.foodchem.2012.01.004
  • Vera J, Correia-Sá L, Paíga P, Bragança I, Fernandes VC, Domingues VF, Delerue-Matos C. QuEChERS and soil analysis. An overview. Sample Prep. 2013;1(2013):54–77. doi:10.2478/sampre-2013-0006
  • Westland JL, Dorman FL. QuEChERS extraction of benzodiazepines in biological matrices. J Pharm Anal. 2013;3(6):509–517. doi:10.1016/j.jpha.2013.04.004
  • Brandhonneur N, Mendes MD, Lepvrier E, Esseiva EF, Chevanne F, Le Corre P. A micro-QuEChERS method coupled to GC–MS for the quantification of pesticides in specific maternal and fetal tissues. J Pharmaceut Biomed. 2015;104:90–96. doi:10.1016/j.jpba.2014.10.035
  • Huertas-Pérez JF, Arroyo-Manzanares N, Havlíková L, Gámiz-Gracia L, Solich P, García-Campaña AM. Method optimization and validation for the determination of eight sulfonamides in chicken muscle and eggs by modified QuEChERS and liquid chromatography with fluorescence detection. J Pharmaceut Biomed. 2016;124:261–266. doi:10.1016/j.jpba.2016.02.040
  • Wen CH, Lin SL, Fuh MR. Determination of sulfonamides in animal tissues by modified QuEChERS and liquid chromatography tandem mass spectrometry. Talanta. 2017;164:85–91. doi:10.1016/j.talanta.2016.11.006
  • Oliveira FA, Pereira EN, Gobbi JM, Soto-Blanco B, Melo MM. Multiresidue method for detection of pesticides in beef meat using liquid chromatography coupled to mass spectrometry detection (LC-MS) after QuEChERS extraction. Food Addit Contam. 2018;35(1):94–109. doi:10.1080/19440049.2017.1395519
  • Zhao DLL Multi residue Analysis of Pesticides in Avocado with Agilent Bond Elut EMR—Lipid by LC/MS/MS. Agilent Technologies; 2015.
  • Ciscato CBC, Ozawa J, Nascimento S Sample Cleanup Methods for Multi residue Pesticide GC/MS/MS Analysis in Avocado. Agilent Technologies; 2016.
  • Zhao L Benefits of EMR—Lipid Cleanup with Enhanced Post Treatment on Pesticides Analysis by GC/MS/MS. Agilent Technologies; 2016.
  • Moreno-González D, Alcántara-Durán J, Addona SM, Beneito-Cambra M. Multi-residue pesticide analysis in virgin olive oil by nanoflow liquid chromatography high resolution mass spectrometry. J Chromatogr A. 2018;1562:27–35. doi:10.1016/j.chroma.2018.05.053
  • Drummer OH, Gerostamoulos J. Postmortem drug analysis: analytical and toxicological aspects. Ther Drug Monit. 2002;24(2):199–209. doi:10.1097/00007691-200204000-00002
  • Drummer OH. Requirements for bioanalytical procedures in postmortem toxicology. Anal Bioanal Chem. 2007;388:1495–1503. doi:10.1007/s00216-007-1238-7
  • Drummer OH. Post-mortem toxicology. Forensic Sci Int. 2007;165(2–3):199–203. doi:10.1016/j.forsciint.2006.05.020
  • Butzbach DM. The influence of putrefaction and sample storage on post-mortem toxicology results. Forensic Sci Med Pathol. 2010;6:35–45. doi:10.1007/s12024-009-9130-8
  • Skopp G. Postmortem toxicology. Forensic Sci Med Pathol. 2010 Dec;6:314–325. doi:10.1007/s12024-010-9150-4
  • Politi L, Groppi A, Polettini A, Montagna M. A rapid screening procedure for drugs and poisons in gastric contents by direct injection-HPLC analysis. Forensic Sci Int. 2004;141(2–3):115–120. doi:10.1016/j.forsciint.2004.01.010
  • LeBeau MA. ANSI/ASB standard 036 for method validation in forensic toxicology has replaced SWGTOX’s version. J Anal Toxicol. 2020;44(4):414–414. doi:10.1093/jat/bkz115
  • Han L, Matarrita J, Sapozhnikova Y, Lehotay SJ. Evaluation of a recent product to remove lipids and other matrix co-extractives in the analysis of pesticide residues and environmental contaminants in foods. J Chromatogr A. 2016;1449:17–29. doi:10.1016/j.chroma.2016.04.052
  • Baduel C, Mueller JF, Tsai H, Ramos MJ. Development of sample extraction and clean-up strategies for target and non-target analysis of environmental contaminants in biological matrices. J Chromatogr A. 2015;1426:33–47. doi:10.1016/j.chroma.2015.11.040

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.