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- The yield of gem-N3P3(NPPh3)2Cl4 from gem-N3P3(NH2)(NPPh3)Cl4 can also be improved by using benzene instead of tetrachloromethane as the solvent9
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- It was possible to isolate the compound, gem-N3P3(NH2)(NPPh3)Cl4s (0.5 g) from the reaction mixture at this stage by using column chromatography Silica gel : eluant, benzene(1) + dichloromethane(4).
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