200
Views
4
CrossRef citations to date
0
Altmetric
Extraction

Salting-out assisted liquid-liquid extraction method combined with GC-MS for the determination of topiramate in aqueous solutions: development and application of the methodology

, , &
Pages 2303-2312 | Received 28 Aug 2018, Accepted 23 May 2019, Published online: 01 Jun 2019

References

  • Neto, J.G.; Marchetti, R.L. (2005) Aspectos epidemiológicos e relevância dos transtornos mentais associados à epilepsia. Revista Brasileira De Psiquiatria, 27: 323–328. doi: 10.1590/S1516-44462005000400013.
  • Vannucci Campos, D.; Lopim, G.M.; Da Silva, D.A.; de Almeida, A.A.; Amado, D.; Arida, R.M. (2017) Epilepsy and exercise: an experimental study in female rats. Physiology & Behavior, 171: 120–126. doi: 10.1016/j.physbeh.2016.12.040.
  • Mohammadi, B.; Mohammadi, B.; Tammari, E.; Fakhri, S.; Bahrami, G. (2013) Applicability of LC-MS/MS to optimize derivatization of topiramate with FMOC-Cl using reacted/intact drug ratio. Journal of Chromatography B, 928: 32–36. doi: 10.1016/j.jchromb.2013.02.041.
  • Pinto, E.C.;, et al. (2016) Topiramate: a review of analytical approaches for the drug substance, its impurities and pharmaceutical formulations. Journal of Chromatography Science, 54: 280–290.
  • Matar, K.M.;. (2010) Therapeutic drug monitoring of topiramate by liquid chromatography-tandem mass spectrometry. Clinica Chimica Acta, 411: 729–734. doi: 10.1016/j.cca.2010.02.003.
  • Ni, Y.; Zhou, Y.; Xu, M.; He, X.; Li, H.; Haseeb, S.; Chen, H.; Li, W. (2015) Simultaneous determination of phentermine and topiramate in human plasma by liquid chromatography-tandem mass spectrometry with positive/negative ion-switching electrospray ionization and its application in pharmacokinetic study. Journal of Pharmaceutical and Biomedical Analysis, 107: 444–449. doi: 10.1016/j.jpba.2015.01.035.
  • Conway, J.M.; Birnbaum, A.K.; Marino, S.E.; Cloyd, J.C.; Remmel, R.P. (2012) A sensitive capillary GC-MS method for analysis of topiramate from plasma obtained from single-dose studies. Biomedical Chromatography : BMC. doi: 10.1002/bmc.1749.
  • Lee, H.Z.S.; Ong, M.C.; Lim, J.L.W.; Yap, T.W.A. (2017. Challenges in GC–MS analysis: case studies onLEE, H. Z. S. et al. Challenges in GC–MS analysis: case studies on phenibut and ethylphenidate. Forensic Science International, 277: 166–178. 2017. phenibut and ethylphenidate. Forensic Sci. Int. 277, 166–178 doi: 10.1016/j.forsciint.2017.06.002.
  • Hahn, R.Z.; Antunes, M.V.; Costa Arnhold, P.; Andriguetti, N.B.; Verza, S.G.; Linden, R. (2017) Determination of topiramate in dried blood spots using single-quadrupole gas chromatography–mass spectrometry after flash methylation with trimethylanilinium hydroxide. Journal of Chromatography B, 1046: 131–137. doi: 10.1016/j.jchromb.2017.01.047.
  • Nassar, R.; Trivella, A.; Mokh, S.; Al-Iskandarani, M.; Budzinski, H.; Mazellier, P. (2017) Journal of Photochemistry and Photobiology A : chemistry amitriptyline, and clomipramine drugs in aqueous media. Journal of Photochemistry and Photobiology A: Chemistry, 336: 176–182. doi: 10.1016/j.jphotochem.2016.12.008.
  • Marín-García, M.; Ioele, G.; Franquet-Griell, H.; Lacorte, S.; Ragno, G.; Tauler, R. (2018) Investigation of the photodegradation profile of tamoxifen using spectroscopic and chromatographic analysis and multivariate curve resolution. Chemometrics and Intelligent Laboratory Systems, 174: 128–141. doi: 10.1016/j.chemolab.2018.01.011.
  • Bae, E.; Lee, J.; Shin, J.-W.; Moon, J.; Lee, K.-J.; Shin, Y.-W.; Kim, T.-J.; Shin, D.; Jang, I.-J.; Lee, S.K. (2016) Factors influencing topiramate clearance in adult patients with epilepsy : A population pharmacokinetic analysis. Seizure, 37: 8–12. doi: 10.1016/j.seizure.2016.02.002.
  • Manitpisitkul, P.; Curtin, C.R.; Shalayda, K.; Wang, -S.-S.; Ford, L.; Heald, D.L. (2014) Pharmacokinetics of topiramate in patients with renal impairment, end-stage renal disease undergoing hemodialysis, or hepatic impairment. Epilepsy Research, 108: 891–901. doi: 10.1016/j.eplepsyres.2014.03.011.
  • Sánchez, M.D.N.; Oliveira, E.; Otero-Glez, A.; Santos Nores, J.; Igrejas, G.; Lodeiro, C.; Capelo, J.L.; Santos, H.M. (2014) Microextraction by packed sorbent and salting-out-assisted liquid-liquid extraction for the determination of aromatic amines formed from azo dyes in textiles. Talanta, 119: 375–384. doi: 10.1016/j.talanta.2013.10.019.
  • Tsai, C.J.; Liao, F.-Y.; Weng, J.-R.; Feng, C.-H. (2017) Tandem derivatization combined with salting-out assisted liquid–liquid microextraction for determination of biothiols in urine by gas chromatography–mass spectrometry. Journal of Chromatography A, 1524: 29–36. doi: 10.1016/j.chroma.2017.09.069.
  • Akram, S.; Sultana, B.; Asi, M.R.; Mushtaq, M. (2018) Salting-out-assisted liquid–liquid extraction and reverse-phase high-performance liquid chromatographic monitoring of thiacloprid in fruits and vegetables. Separation Science and Technology, 53: 1563–1571. doi: 10.1080/01496395.2017.1417317.
  • Razmara, R.S.; Daneshfar, A.; Sahrai, R. (2011) Determination of methylene blue and sunset yellow in wastewater and food samples using salting-out assisted liquid-liquid extraction. Journal of Industrial and Engineering Chemistry, 17: 533–536. doi: 10.1016/j.jiec.2010.10.028.
  • Valente, I.M.; Gonçalves, L.M.; Rodrigues, J.A. (2013) Another glimpse over the salting-out assisted liquid – liquid extraction in acetonitrile/water mixtures. Journal of Chromatography A, 1308: 58–62. doi: 10.1016/j.chroma.2013.08.014.
  • Hou, B.J.; Wei, Y.-Q.; Ma, F.; Wang, X.-N.; Yang, S.-Z. (2018) Chelatometric salting-out extraction and characteristics of flavonoids from Folium nelumbinis based on an ethanol/K2HPO4system. Separation Science and Technology, 53: 717–724. doi: 10.1080/01496395.2017.1397023.
  • Martins, M.L.; Primel, E.G.; Caldas, S.S.; Prestes, O.D.; Adaime, M.B.; Zanella, R. (2012) Microextração Líquido-Líquido Dispersiva (DLLME): fundamentos e aplicações. Scientia Chromatographica, 4: 35–51. doi: 10.4322/sc.2012.004.
  • Li, J.;, et al. (2018) Salting-out effect of sodium carbonate on the liquid–liquid equilibrium of (Water + Dichloromethane + N,N-Dimethylacetamide) system at temperature T =(298.15 and 308.15) K. Separation Science and Technology, 00: 1–10.
  • Wen, Y.; Li, J.; Yang, F.; Zhang, W.; Li, W.; Liao, C.; Chen, L. (2013) Salting-out assisted liquid-liquid extraction with the aid of experimental design for determination of benzimidazole fungicides in high salinity samples by high-performance liquid chromatography. Talanta, 106: 119–126. doi: 10.1016/j.talanta.2012.12.011.
  • Wang, M.; Rejtar, T.; Wang, M.; Bones, J.; Cha, S.; Clodfelder-Miller, B.; Richardson, E.; Binns, S.; Dahiya, S.; Sgroi, D.; Karger, B.L. (2011) Coupling of acetonitrile deproteinization and salting-out extraction with acetonitrile stacking in chiral capillary electrophoresis for the determination of warfarin enantiomers. Journal of Chromatography A, 1218: 4045–4051. doi: 10.1016/j.chroma.2011.09.022.
  • Song, X.; Li, J.; Liao, C.; Chen, L. (2011) Ultrasound-assisted dispersive liquid – liquid microextraction combined with low solvent consumption for determination of polycyclic aromatic hydrocarbons in seawater by GC – MS. Chromatographia, 74: 89–98. doi: 10.1007/s10337-011-2048-9.
  • Teju, E.; Tadesse, B.; Megersa, N. (2017) Salting-out-assisted liquid–liquid extraction for the preconcentration and quantitative determination of eight herbicide residues simultaneously in different water samples with high-performance liquid chromatography. Separation Science and Technology, 6395: 1–11. doi: 10.1080/01496395.2016.1276596.
  • Neto, Á.J., dos S;. (2009) Problemas com o formato dos picos em cromatografia líquida. Journal of Chromatographic Science, 1: 69–77.
  • Ribani, M.; Bottoli, C.B.G.; Collins, C.H.; Jardim, I.C.S.F.; Melo, L.F.C. (2004) Validação Em Métodos Cromatográficos E Eletroforéticos. Química Nova, 27: 771–780. doi: 10.1590/S0100-40422004000500017.
  • Prudêncio Dutra, M.; Da, C.; Viana, A.C.; de Oliveira, D.; Pereira, G.E.; Dos Santos Lima, M. (2018) Rapid determination of the aromatic compounds methyl-anthranilate, 2′-aminoacetophenone and furaneol by GC-MS: method validation and characterization of grape derivatives. Food Research International, 107: 613–618. doi: 10.1016/j.foodres.2018.03.020.
  • Harris, D.C.;. (2011) Quantitative Chemical Analysis, 8ª ed., LTC: Rio de Janeiro, Brazil.
  • Magiera, S.; Kwietniowska, E. (2016) Fast, simple and efficient salting-out assisted liquid-liquid extraction of naringenin from fruit juice samples prior to their enantioselective determination by liquid chromatography. Food Chemistry, 211: 227–234. doi: 10.1016/j.foodchem.2016.05.045.
  • Niu, Z.; Yu, C.; He, X.; Zhang, J.; Wen, Y. (2017) Salting-out assisted liquid–liquid extraction combined with gas chromatography-mass spectrometry for the determination of pyrethroid insecticides in high salinity and biological samples. Journal of Pharmaceutical and Biomedical Analysis, 143: 222–227. doi: 10.1016/j.jpba.2017.05.046.
  • Villalba, M.L.; Enrique, A.V.; Higgs, J.; Castaño, R.A.; Goicoechea, S.; Taborda, F.D.; Gavernet, L.; Lick, I.D.; Marder, M.; Bruno Blanch, L.E. (2016) Novel sulfamides and sulfamates derived from amino esters : synthetic studies and anticonvulsant activity. European Journal of Pharmacology, 774: 55–63. doi: 10.1016/j.ejphar.2016.02.001.

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.