Publication Cover
Ozone: Science & Engineering
The Journal of the International Ozone Association
Volume 22, 2000 - Issue 6
661
Views
61
CrossRef citations to date
0
Altmetric
Original Articles

Application of DNPH Derivatization with LC/MS to the Identification of Polar Carbonyl Disinfection Byproducts in Drinking Water

, , , &
Pages 653-675 | Received 03 Sep 1999, Accepted 06 Jan 2000, Published online: 31 Mar 2009

References

  • Rice , R. RICE International Consulting Enterprises personal communication
  • Richardson , S. D. 1998 . “Drinking Water Disinfection By-products” . In The Encyclopedia of Environmental Analysis and Remediation , Edited by: Meyers , R. A. Vol. 3 , 1398 – 1421 . New York : John Wiley & Sons .
  • Glaze , W. H. and Weinberg , H. S. 1993 . Identification and Occurrence of Ozonation By-Products in Drinking Water , Denver, CO : American Water Works Association Research Foundation .
  • Glaze , W. H. , Koga , M. and Cancilla , D. 1989 . “Ozonation Byproducts. 2. Improvement of an Aqueous-Phase Derivatization Method for the Detection of Formaldehyde and Other Carbonyl Compounds Formed by the Ozonation of Drinking Water” . Environ. Sci. Technol. , 23 : 838 – 847 .
  • Haag , W. R. and Hoigne , J. 1983 . “Ozonation of Bromide-Containing Water: Kinetics of Formation of Hypobromous Acid and Bromate” . Environ. Sci. Technol. , 17 : 261 – 267 .
  • Coleman , W. E. , Munch , J. W. , Ringhand , H. P. , Kaylor , W. H. and Mitchell , D. E. 1992 . “Ozonation/Post-Chlorination of Humic Acid: A Model for Predicting Drinking Water Disinfection By-products” . Ozone: Sci., & Eng. , 14 : 51 – 69 .
  • Glaze , W. H. 1986 . “Reaction Products of Ozone: A Review” . Environ. Health Perspec. , 69 : 151 – 157 .
  • Lelacheur , R. M. , Sonnenberg , L. B. , Singer , P. C. , Christman and Charles , M. J. 1993 . “Identification of Carbonyl Compounds in Environmental Samples” . Environ. Sci. Technol. , 27 : 2745 – 2753 .
  • Anderson , L. J. , Johnson , J. D. and Christman , R. F. 1985 . “The Reaction of Ozone with Isolated Aquatic Fulvic Acid” . Org. Geochem. , 8 : 65 – 69 .
  • Lawrence , J. , Tosine , H. , Onuska , R. I. and Comba , M. E. 1992 . “The Ozonation of Natural Waters: Product Identification” . Ozone Sci. Eng. , 14 : 55 – 64 .
  • Killops , S. D. 1986 . “Volatile Ozonation Products of Aqueous Humic Material” . Water Res. , 20 : 153 – 165 .
  • Richardson , S. D. , Thruston , A. D. Jr. , Caughran , T. V. , Chen , P. H. , Collette , T. W. , Floyd , T. L. , Schenck , K. S. , Lykins , B. W. Jr. , Sun , G. and Majetich , G. 1999 . “Identification of New Ozone Disinfection Byproducts in Drinking Water” . Environ. Sci. Technol. , 33 : 3368 – 3377 .
  • Krasner , S. W. , Gramith , J. T. , Means , E. G. , Patania , N. L. , Najm , I. N. and Aieta , E. M. 1991 . “Formation and Control of Brominated Organic Disinfection By-products” . Proc. AWWA WQTC . 1991 , Denver, CO.
  • Amy , G. L. and Siddiqui , M. S. 1991 . “Ozone-Bromide Interactions in Water Treatment” . Proc. AWWA WQTC . 1991 , Denver, CO.
  • Collette , T. W. , Richardson , S. D. and Thruston , A. D. Jr. 1994 . “Identification of Bromohydrins in Ozonated Water” . Appl. Spectrosc. , 48 : 1181 – 1192 .
  • Cavanaugh , J. E. , Weinberg , H. S. , Gold , A. , Sangaiah , R. , Marbury , D. , Glaze , W. H. , Collette , T. W. , Richardson , S. D. and Thruston , A. D. Jr. 1992 . “Ozonation Byproducts: Identification of Bromohydrins from the Ozonation of Natural Waters with Enhanced Bromide Levels” . Environ. Sci. Technol. , 26 : 1658 – 1662 .
  • Richardson , S. D. , Thruston , A. D. JR. , Caughran , T. V. , Chen , P. H. , Collette , T. W. , Floyd , T. L. , Schenck , K. M. , Lykins , B. W. Jr. , Sun , G. and Majetich , G. 1999 . “Identification of New Drinking Water Disinfection Byproducts Formed in the Presence of Bromide” . Environ. Sci. Technol. , 33 : 3378 – 3383 .
  • Xie , Y. and Reckhow , D. A. 1997 . “Development of a Method to Identify Keto Acids in Ozonated Fulvic Acid Solutions” . J. Mass Spectrom. , 32 : 99 – 102 .
  • Spaulding , R. S. , Frazey , P. , Rao , X. and Charles , M. J. 1999 . “Measurement of Hydroxy Carbonyls and Other Carbonyls in Ambient Air Using Pentafluorobenzyl Alcohol as a Chemical Ionization Reagent” . Anal. Chem. , 71 : 3420 – 3427 .
  • Schlitt , H. 1997 . “Impinger Sampling Coupled to High-Performance Liquid Chromatography by a Modified Autoinjector Interface” . J. Chromatog. A , 762 : 187 – 192 .
  • Kölliker , S. , Oehme , M. and Dye , C. 1998 . “Structure Elucidation of 2,4-Dinitrophenylhydrazone Derivatives of Carbonyl Compounds in Ambient Air by HPLC/MS and Multiple MS/MS Using Atmospheric Chemical Ionization in the Negative Ion Mode” . Anal. Chem. , 70 : 1979 – 1985 .
  • Grosjean , E. , Green , P. G. and Grosjean , D. 1999 . “Liquid Chromatography Analysis of Carbonyl (2,4-Dinitrophenyl)hydrazones with Detection by Diode Array Ultraviolet Spectroscopy and by Atmospheric Pressure Negative Chemical Ionization Mass Spectrometry” . Anal. Chem. , 71 : 1851 – 1861 .
  • Riggin , R. M. 1984 . Compendium of Methods for the Determination of Toxic Organic Compounds in Ambient Air , Research Triangle Park, NC : U.S. Environmental Protection Agency . EPA-600/4–84-04
  • Purdue , L. H. , Dayton , D. P. , Rice , J. and Bursey , J. Oct. 31 1991 . Technical Assistance Document for Sampling and Analysis of Ozone Precursors , Oct. 31 , Research Triangle Park, NC : Atmospheric Research and Exposure Assessment Laboratory, U.S. Environmental Protection Agency . EPA-600/4–84-041
  • Lodge , J. P. Jr. , ed. 1989 . Methods of Air Sampling and Analysis , 3rd edition , 293 – 295 . Chelsea, MI : Lewis Publishers .
  • Grosjean , E. and Grosjean , D. 1995 . “Liquid Chromatographic Analysis of C1-C10 Carbonyls” . Int. J. Environ. Anal. Chem. , 61 : 47 – 64 .
  • Ravandi , A. , Kuksis , A. , Myher , J. J. and Marai , L. 1995 . “Determination of Lipid Ester Ozonides and Core Aldehydes by High-Performance Liquid Chromatography with On-line Mass Spectrometry” . J. Biochem. Biophys. Methods , 30 : 271 – 285 .
  • Kamido , H. , Kuksis , A. , Marai , A. , Myher , J. J. and Pang , H. 1992 . “Preparation, Chromatography and Mass Spectrometry of Cholesteryl Ester and Glycerolipid-Bound Aldehyde” . Lipids , 27 : 645 – 650 .
  • Menet , M -C. , Gueylard , D. , Fievet , M-H. and Thuillier , A. 1996 . “Fast Specific Separation and Sensitive Quantification of Bactericidal and Sporicidal Aldehydes by High-Performance Liquid Chromatography: Example of Glutaraldehyde Determination” . J. Chromatog. B , 692 : 79 – 86 .
  • Goldring , C. , Casini , A. F. , Maellaro , E. , Del Bello , B. and Comporti , M. 1993 . “Determination of 4-Hydroxynonenal by High-Performance Liquid Chromatography with Electrochemical Detection” . Lipids , 28 : 141 – 145 .
  • Navarro-Gonzalez , R. , Negron-Mendoza , A. and Albarran , G. 1991 . “Analysis of Keto Acids as Their Methyl Esters of 2,4-Dinitrophenylhydrazone Derivatives by Gas Chromatography and Gas Chromatography-Mass Spectrometry” . J. Chromatog. , 587 : 247 – 254 .
  • Ariga , N. 1972 . “Thin-Layer Chromatography of Keto Acid 2,4-Dinitrophenylhydrazones” . Anal. Biochem. , 49 : 436 – 441 .
  • Kieber , R. J. and Mopper , K. 1990 . “Determination of Picomolar Concentrations of Carbonyl Compounds in Natural Waters, Including seawater, by Liquid Chromatography” . Environ. Sci. Technol. , 24 : 1477 – 1481 .
  • Takami , K. , Kuwata , K. , Sugimae , A. and Nakamoto , M. 1985 . “Trace Determination of Aldehydes in Water by High-Performance Liquid Chromatography” . Anal. Chem. , 47 : 243 – 245 .
  • Takeda , S. , Wakida , S. , Yamane , M. and Higashi , K. 1994 . “Analysis of Lower Aliphatic Aldehydes in Water by Micellar Electrokinetic Chromatography with Derivatization to 2,4-Dinitrophenylhydrazones” . Electrophoresis , 15 : 1332 – 1334 .
  • Olson , K. L. and Swarin , S. J. 1985 . “Determination of Aldehydes and Ketones by Derivatization and Liquid Chromatography-Mass Spectrometry” . J. Chromatog. , 333 : 337 – 347 .
  • Munch , J. W. , Munch , D. J. , Winslow , S. D. , Wendelken , S. C. and Pepich , B. V. 1998 . “A User's Guide to Aldehyde Analysis Using PFBHA Derivatization and GC/ECD Detection: Avoiding the Pitfalls” . Proc. A WWA WQTC . 1998 , San Diego, CA.
  • Behforouz , M. , Bolan , J. L. and Flynt , M. S. 1985 . “2,4-Dinitrophenylhydrazones: A Modified Method for the Preparation of These Derivatives and an Explanation of Previous Conflicting Results” . J. Org. Chem. , 50 : 1186 – 1189 .
  • Binding , N. , Muller , W. and Witting , U. 1996 . “Syn/Anti Isomerization of 2,4-Dinitrophenylhydrazones in the Determination of Airborne Unsymmetrical Aldehydes and Ketones Using 2,4-Dinitrophenylhydrazine Derivatization” . Fresenius J. Anal. Chem. , 356 : 315 – 319 .
  • Richardson , S. D. , Caughran , T. V. , Poiger , T. , Thruston , A. D. Jr. , Collette , T. W. , Patterson , K. S. and Lykins , B. W. JR . 1997 . “Identification of New Drinking Water Disinfection By-products” . Proc. Am. Soc. Mass Spectrom. Conf. . 1997 , Palm Springs, CA.
  • Karabatos , G. J. , Vane , F. M. , Taller and Hsi , N. J. 1964 . “Structural Studies by Nuclear Magnetic Resonance. VIII. Ring-Substituted Phenylhydrazones, Semicarbazones, and Thiosemicarbazones” . J. Am. Chem. Soc. , 86 : 3351 – 3357 .

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.