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Food Additives & Contaminants Volume 24, 2007 - Issue 4
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Original Articles

Validation of an analytical method for the determination of spiramycin, virginiamycin and tylosin in feeding-stuffs by thin-layer chromatography and bio-autography

Ursula Vincent European Commission, Joint Research Centre, Institute for Reference Materials and Measurements, Food Safety & Quality Unit, Retieseweg, B-2440 Geel, Belgium
,
Gisele Gizzi European Commission, Joint Research Centre, Institute for Reference Materials and Measurements, Food Safety & Quality Unit, Retieseweg, B-2440 Geel, Belgium
,
Christoph von Holst European Commission, Joint Research Centre, Institute for Reference Materials and Measurements, Food Safety & Quality Unit, Retieseweg, B-2440 Geel, BelgiumCorrespondence[email protected]
,
Jacob De Jong RIKILT Institute of Food Safety, Bornsesteeg 45, PO Box 230, NL-6708 PD Wageningen, the Netherlands
&
Jacques Michard Laboratoire de la Répression des Fraudes, Rue Antoine Joly 26, F-35000 Rennes, France
Pages 351-359 | Received 07 Jul 2006, Accepted 14 Oct 2006, Published online: 30 Mar 2007

References

  • De Jong , J , Tomassen , MJH , Van Egmond , HJ , Van Rhijn , JA , Zuidema , T , Michard , J , Genouel , C , Brambilla , G , Nunes da Costa , JMG Nordkvist , E . 2006 . “ Towards a control strategy for banned antibiotics and growth promoters in feed: The SIMBAG-FEED project ” . In Antimicrobial growth promoters. Where do we go from here , Edited by: Barug , D , De Jong , J , Kies , AK and Verstegen , MWA . p. 211 Wageningen : Wageningen Academic Publishers .
  • European Community . 1970 . Council Directive 70/24/EEC of 23 November 1970 concerning additives in feedingstuffs . Official Journal of the European Communities L , 270 : 1
  • European Community . 1972 . Third Commission Directive 72/199/EEC of 27 April 1972 establishing Community methods of analysis for the official control of feedingstuffs . Official Journal of the European Communities L , 123 : 6 – 34 .
  • European Community . 1984a . Commission Directive 84/4/EEC of 20 December 1983 amending Directives 71/393/EEC, 72/199/EEC and 78/633/EEC establishing Community methods of analysis for the official control of feedingstuffs . Official Journal of the European Communities L , 015 : 28 – 38 .
  • European Community . 1984b . Tenth Commission Directive 84/425/EEC of 25 July 1984 establishing Community methods of analysis for the official control of feedingstuffs . Official Journal of the European Communities L , 238 : 34 – 38 .
  • European Community . 1998 . Council Regulation No 2821/98 of 17 December 1998 amending, as regards withdrawal of the authorisation of certain antibiotics, Directive 70/524/EEC concerning additives in feedingstuffs . Official Journal of the European Communities L , 351 : 4 – 8 .
  • Gafner , JL . 1999 . Identification and semi-quantitative estimation of antibiotics added to complete feeds, premixes and concentrates . Journal of the Association of Official Analytical Chemistry , 82 : 1 – 8 .
  • Hajee , CAJ , Van Rhijn , JA , Lasaroms , JJP , Keukens , HJ and De Jong , J . 2001 . Development and validation of a method for the determination of sub-additive levels of virginiamycin in compound animal feeds by liquid chromatography . Analyst , 126 : 1332 – 1338 .
  • Horwitz , W , Kamps , LR and Boyer , KW . 1980 . Quality assurance in the analysis of foods and trace constituents . Journal of the Association of Official Analytical Chemistry , 63 : 1344 – 1354 .
  • Houglum , JE and Tasler , MK . 1996 . LC assay of tylosin in animal feeds . Journal of the Association of Official Analytical Chemistry , 79 ( 2 ) : 369 – 374 .
  • Kramer , GN , Oostra , A , De Vos , P , Teipel , K , Emteborg , H and Conneely , P . 2004 . Production of 4 blank and 10 spiked compound feeds for SCA SIMBAG-FEED; SIMBAG-FEED Report 8.5 GER/RM/10/2004/November/10. RIKILT
  • Langton , SD , Chevennement , R , Nagelkerke , N and Lombard , B . 2002 . Analysing collaborative trials for qualitative microbiological methods: accordance and concordance . International Journal of Food Microbiology , 79 : 175 – 181 .
  • Michard , J and Joubert , M . 2005 . Method protocol for tylosin, spiramycin and virginiamycin in animal feedingstuffs by thin layer chromatography SIMBAG-FEED Report 4.6. RIKILT
  • Serano , F , Brambilla , G and Von Holst , C . 2004 . Homogeneity study of test material MAT 1 to MAT 10 SIMBAG-FEED Report Work Package. IRMM and RIKILT
  • Von Holst , C . 2002 . Homogeneity study of pre-mixtures containing the feed additives at defined concentration. SIMBAG-FEED Report Work Package 8. IRMM and RIKILT

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