A spherical FOX-7 crystal: Preparation, characterization, solubility and thermodynamic study

References

• Acree, W. E., and A. I. Zvaigzne. 1991. Thermodynamic properties of nonelectrolyte solutions: Part 4. Estimation and mathematical representation of solute activity coefficients and solubilities in binary solvents using the nibs and modified Wilson equation. Thermochimica Acta 178: 151–67. doi: 10.1016/0040-6031(91)80307-5.
   Web of Science ®Google Scholar
• Apelblat, A., and E. Manzurola. 1999. Solubilities ofo-acetylsalicylic, 4-aminosalicylic, 3,5-dinitrosalicylic, andp-toluic acid, and magnesium-DL-aspartate in water fromT=(278 to 348) K. The Journal of Chemical Thermodynamics 31 (1): 85–91. doi: 10.1006/jcht.1998.0424.
   Web of Science ®Google Scholar
• Barata, P. A., and M. L. Serrano. 1996. Salting-out precipitation of potassium dihydrogen phosphate (KPD). I. Precipiation mechanism. Journal of Crystal Growth 160 (3–4): 361–69. doi: 10.1016/0022-0248(95)00740-7.
   Web of Science ®Google Scholar
• Cai, H. Q., Y. J. Shu, W. F. Yu, Y. Tian, G. Y. Zeng, and B. B. Cheng. 2004. Synthesis and Characteristics of 1,1-diamino-2,2-dinitroethylene. Chemical Research and Application 16 (2): 264–65. doi: 10.1038/sj.cr.7290254.
   Google Scholar
• Chen, J., and B. L. Trout. 2008. Computational study of solvent effects on the molecular self-assembly of tetrolic acid in solution and implications for the polymorph formed from crystallization. Journal of Physical Chemistry B 112 (26): 7794. doi: 10.1021/jp7106582.
   PubMed Web of Science ®Google Scholar
• Chen, L. Z. 2017. The study on crystallization process of Hexanitrostrilbene. PhD diss., North University of China.
   Google Scholar
• Fu, Q. B. 2007. Synthesis and properties of 1,1-Diamino-2,2-Dinitroethylene. PhD diss., Sichuan University.
   Google Scholar
• Gantiva, M., and F. Martinez. 2010. Thermodynamic analysis of the solubility of ketoprofen in some propylene glycol+water cosolvent mixtures. Fluid Phase Equilibria 293 (2): 242–50. doi: 10.1016/j.fluid.2010.03.031.
   Web of Science ®Google Scholar
• Gu, C. H., H. Li, R. B. Gandhi, and K. Raghavan. 2004. Grouping solvents by statistical analysis of solvent property parameters: Implication to polymorph screening. International Journal of Pharmaceutics 283 (1–2): 117–25. doi: 10.1016/j.ijpharm.2004.06.021.
   PubMed Web of Science ®Google Scholar
• Guo, H.-J., X. Dang, F. Yang, D.-L. Cao, Y.-X. Li, W.-H. Hu, Z.-M. Jiang, Z.-H. Li, Z.-Y. Li, and L.-W. Zhang. 2017. Solubility and thermodynamic properties of a kind of explosives in four binary solvents. Journal of Molecular Liquids 247: 313–27. doi: 10.1016/j.molliq.2017.09.097.
   Web of Science ®Google Scholar
• Krug, R. R., W. G. Hunter, and R. A. Grieger. 1976. Enthalpy-entropy compensation. 1. Some fundamental statistical problems associated with the analysis of van’t Hoff and Arrhenius data. Journal of Physical Chemistry 80 (21): 2335–41. doi: 10.1021/j100562a006.
   Web of Science ®Google Scholar
• Latypov, N. V., J. Bergman, A. Langlet, U. Wellmar, and U. Bemm. 1998. Synthesis and reaction of 1,1-Diamino-2,2-dinitroethylene. Tetrahedron 54 (38): 11525–36. doi: 10.1016/s0040-4020(98)00673-5.
   Web of Science ®Google Scholar
• Li, J., Z. Wang, Y. Bao, and J. Wang. 2013. Solid–liquid phase equilibrium and mixing properties of cloxacillin benzathine in pure and mixed solvents. Industrial & Engineering Chemistry Research 52 (8): 3019–26. doi: 10.1021/ie3031423.
   Web of Science ®Google Scholar
• Liu, L. 2018. Crystallization of high-energy low-sensitivity explosive FOX-7. PhD diss., Southwest University of Science and Technology.
   Google Scholar
• Liu, Z., Q. Yin, H. Zhang, and J. Gong. 2014. Investigation of the crystallization of disodium 5ʹ-inosinate in a water + ethanol system: Solubility, nucleation mechanism, and crystal morphology. Industrial & Engineering Chemistry Research 53 (21): 8913–19. doi: 10.1021/ie404073p.
   Web of Science ®Google Scholar
• Long, Z. K. 2013. Research Development of 1,1-diamino-2,2-dinitroethylene Synthesis. Guangzhou Chemistry 38 (4): 70–78. doi: 10.16560/j.cnki.gzhx.2013.04.011.
   Google Scholar
• Mersmann, A. 1990. Calculation of interfacial tensions. Journal of Crystal Growth 102 (4): 841–47. doi: 10.1016/0022-0248(90)90850-K.
   Web of Science ®Google Scholar
• Noubigh, A., and M. Abderrabba. 2016. Solid–liquid phase equilibrium and thermodynamic properties of vanillic acid in different pure solvents. Journal of Molecular Liquids 223: 261–66. doi: 10.1016/j.molliq.2016.07.004.
   Web of Science ®Google Scholar
• Ostmark, H., A. Langlet, H. Bergman, U. Wellmar, and U. Bemm. 1998. FOX-7: A new explosive with low sensitivity and high performance. Proceedings of 11th International Symposium on Detonation. Snowmass Village, CO, USA, 11: 807–12.
   Google Scholar
• Perlovich, G. L., S. V. Kurkov, A. N. Kinchin, and A. Bauer-Brandl. 2004. Thermodynamics of solutions III: Comparison of the solvation of (+)-naproxen with other NSAIDs. European Journal of Pharmaceutics and Biopharmaceutics 57 (2): 411–20. doi: 10.1016/j.ejpb.2003.10.021.
   PubMed Web of Science ®Google Scholar
• Ren, X. T., D. Y. Ye, N. Ding, J. X. He, and Y. Y. Guo. 2015. A molecular dynamics simulation of solvent effects on the crystal morphology of FOX-7. Acta Armamentarii 36 (2): 272–78. doi: 10.3969/j.1000-1093.2015.02.012.
   Google Scholar
• Shakeel, F., N. Haq, N. A. Siddiqui, F. K. Alanazi, and I. A. Alsarra. 2015. Correlation of solubility of bioactive compound reserpine in eight green solvents at (298.15 to 338.15) K. Journal of Chemical and Engineering Data 60 (3): 775–80. doi: 10.1021/je500893g.
   Web of Science ®Google Scholar
• Simkova, L., F. Liska, and J. Ludvik. 2011. 2,2-Dinitroethene-1,1-Diamine. Current Organic Chemistry 15 (17): 2983–95. doi: 10.2174/138527211798357100.
   Web of Science ®Google Scholar
• Sohnel, O. 1982. Electrolyte crystal-aqueous solution interfacial tensions from crystallization data. Journal of Crystal Growth 57 (1): 101–08. doi: 10.1016/0022-0248(82)90254-8.
   Web of Science ®Google Scholar
• Xiao, H. M. 1998. High Energy Compounds. Beijing: Science Press.
   Google Scholar
• Xu, K. Z., J. R. Song, F. Q. Zhao, Z. H. Cao, H. X. Ma, R. Z. Hu, H. X. Gao, and J. Huang. 2007. Special heat capacity, thermodynamic properties and adiabatic time-to-explosion of 1,1-diamino-2,2-dinitroethylene. Acta Chimica Sinica 65 (24): 2827–31.
   Web of Science ®Google Scholar
• Yang, J. X., H. Wu, Y. G. Wang, Q. H. Luan, J. Zhang, G. Wang, and H. X. Hao. 2015. Thermodynamics of 4’-bromomethyl-2-cyanobiphenyl in different solvents. The Journal of Chemical Thermodynamics 83: 77–84. doi: 10.1016/j.jct.2014.12.002.
   Web of Science ®Google Scholar
• Yaws, C. L. 1999. Chemical properties handbook. Beijing: World Publishing Corporation.
   Google Scholar
• Zhang, D., Y. Wang, S. Ma, S. Wu, and H. Hao. 2013. Determination of solubility and induction time of ceftazidime. Journal of Chemical and Engineering Data 58 (1): 176–82. doi: 10.1021/je301036u.
   Web of Science ®Google Scholar
• Zhao, K., P. Yang, S. Du, K. Li, X. Li, Z. Li, Y. Liu, L. Lin, B. Hou, and J. Gong. 2016. Determination and correlation of solubility and thermodynamics of mixing of 4-aminobutyric acid in mono-solvents and binary solvent mixtures. Journal of Chemical Thermodynamics 102: 276–86. doi: 10.1016/j.jct.2016.07.014.
   Web of Science ®Google Scholar
• Zhao, X., J. H. Rui, and S. S. Feng. 2011. Preparation of spherical RDX by recrystallization. Journal of Beijing Institute of Technology 31 (1): 5–7. doi: 10.1631/jzus.A1000141.
   Google Scholar
• Zhao, X.-H., J.-L. Wang, L.-Z. Chen, L.-Y. Liu, and Z.-H. Han. 2019. Crystallization thermodynamics of FOX-7 in three binary mixed solvents. Journal of Molecular Liquids 295: 111445. doi: 10.1016/j.molliq.2019.111445.
   Web of Science ®Google Scholar
• Zhou, C., X. P. Huang, Y. S. Zhou, X. J. Wang, and X. Y. Fu. 2007. Crystal structure and thermal decomposition of FOX-7. Chinese Journal of Explosives and Propellants 30 (1): 60–63.
   Google Scholar