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Original Articles

Single-crystal diffraction at megabar conditions by synchrotron radiation

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Pages 511-522 | Received 07 Jun 2013, Accepted 30 Jul 2013, Published online: 25 Aug 2013

REFERENCES

  • Hazen Robert M, Finger Larry W. Comparative crystal chemistry. Chichester, Wiley & Sons; 1982.
  • Angel R, Downs R, Finger L. High-temperature high-pressure diffractometry. Rev Mineral Geochem. 2000;41(1):559–596. doi: 10.2138/rmg.2000.41.16
  • Miletich R, Allan DR, Kuhs WK. High pressure single-crystal techniques. Rev Mineral Geochem. 2000;41(1): 445–520. doi: 10.2138/rmg.2000.41.14
  • Boehler R, de Hantsetters K. New anvil designs in diamond-cells. High Press Res. 2004;24:391–396. doi: 10.1080/08957950412331323924
  • McMahon MI, Degtyareva O, Hejny C, Nelmes RJ. New results on old problems: the use of single-crystals in high-pressure structural studies. High Press Res. 2003;23:289–299. doi: 10.1080/0895795032000102504
  • McMahon MI, Gregoryanz E, Lundegaard LF, Loa I, Guillaume C, Nelmes RJ, Kleppe AK, Amboage M, Wilhelm H, Jephcoat AP. Structure of sodium above 100 GPa by single-crystal x-ray diffraction. Proc Natl Acad Sci USA. 2007;104:17297–17299. doi: 10.1073/pnas.0709309104
  • Gregoryanz E, Lundegaard LF, McMahon MI, Guillaume C, Nelmes RJ, Mezouar M. Structural diversity of sodium. Science. 2008;320(5879):1054–1057. doi: 10.1126/science.1155715
  • Dera P, Lavina B, Borkowski LA, Prakapenka VB, Sutton SR, Rivers ML, Downs RT, Boctor NZ, Prewitt CT. High-pressure polymorphism of Fe2P and its implications for meteorites and Earth's core. Geophys Res Lett. 2008;35:L10301. doi: 10.1029/2008GL033867
  • Dera P, Lazarz JD, Prakapenka V, Barkley M, Downs RT. New insights into the high-pressure polymorphism of SiO2 cristobalite. Phys Chem Miner. 2011;38:517–529. doi: 10.1007/s00269-011-0424-5
  • Dera P, Lavina B, Meng Y, Prakapenka VB. Structural and electronic evolution of Cr2O3 on compression to 55 GPa. J Solid State Chem. 2011;184:3040–3049. doi: 10.1016/j.jssc.2011.09.021
  • Lavina B, Dera P, Downs RT, Prakapenka V, Rivers M, Sutton S, Nicol M. Siderite at lower mantle conditions and the effects of the pressure-induced spin-pairing transition. Geophys Res Lett. 2009;36(23):L23306. doi: 10.1029/2009GL039652
  • Lavina B, Dera P, Kim E, Meng Y, Downs RT, Weck PF, Sutton SR, Zhao Y. Discovery of the recoverable high-pressure iron oxide Fe4O5. Proc Natl Acad Sci USA. 2011;108:17281–17285. doi: 10.1073/pnas.1107573108
  • Merlini M, Hanfland M, Gemmi M, Huotari S, Simonelli L, Strobel P. Fe3+ spin transition in CaFe2O4 at high pressure. Am Mineral. 2010;95:200–203. doi: 10.2138/am.2010.3347
  • Merlini M, Crichton W, Hanfland M, Gemmi M, Müller H, Kupenko I, Dubrovinsky L. Structures of dolomite at ultrahigh pressure and their influence on the deep carbon cycle. Proc Natl Acad Sci USA. 2012;109(34):13509–13514. doi: 10.1073/pnas.1201336109
  • Dubrovinsky L, Boffa-Ballaran T, Glazyrin K, Kurnosov A, Frost D, Merlini M, Hanfland M, Prakapenka V, Schouwink P, Pippinger T, Dubrovinskaia N. Single crystal X-ray diffraction at megabar pressures and temperatures of thousands degrees. High Press Res. 2010;30:620–633. doi: 10.1080/08957959.2010.534092
  • ESRF. Available from: http://www.esrf.eu/UsersAndScience/Experiments/DynExtrCond/ID09A
  • Schulze C, Lienert U, Hanfland M, Lorenzen M, Zontone F. Microfocusing of hard x-rays with cylindrically bent crystal monochromators. J Synch Rad. 1998;5:77–81. doi: 10.1107/S0909049597014568
  • Busing WR, Levy HA. Angle calculations for 3- and 4- circle X-ray and neutron diffractometers. Acta Crystallogr. 1967;22:457–464. doi: 10.1107/S0365110X67000970
  • Marresearch. Available from: http://www.marresearch.com/products.mar555.html
  • Hammersley AP, Svensson SO, Hanfland M, Fitch AN, Häusermann D. Two-dimensional detector software: from real detector to idealised image or two-theta scan. High Press Res. 1996;14:235–248. doi: 10.1080/08957959608201408
  • Agilent Xcalibur CCD system. CrysAlis Software system. Oxford: Agilent Technologies UK Ltd; 2012.
  • Sheldrick GM. SADABS. Gottingen: University of Gottingen; 2003.
  • Kabsch W. XDS. Acta Crystallogr. 2010;D66:125–132.
  • Fei Y, Ricolleau A, Frank M, Mibe K, Shen G, Prakapenka V. Toward an internally consistent pressure scale. Proc Natl Acad Sci USA. 2007;104(22):9182–9186. doi: 10.1073/pnas.0609013104
  • Datchi F, LeToullec R, Loubeyre P. Improved calibration of the SrB4O7:Sm2+ optical pressure gauge: advantages at very high pressures and high temperatures. J Appl Phys. 1997;81:3333–3339. doi: 10.1063/1.365025
  • Petricek V, Dusek M, Palatinus L. Jana2006. The crystallographic computing system. Czech Republic, Praha: Institute of Physics; 2006.
  • Mattila A, Pylkkänen T, Rueff JP, Huotari S, Vankó G, Hanfland M, Lehtinen M, Hämäläinen K. Pressure induced magnetic transition in siderite FeCO3 studied by x-ray emission spectroscopy. J Phys: Condens Matter. 2007;19(38):386206. doi: 10.1088/0953-8984/19/38/386206
  • Lavina B, Dera P, Downs RT, Tschauner O, Yang W, Shebanova O, Shen G. Effect of dilution on the spin pairing transition in rhombohedral carbonates. High Press Res. 2010;30(2):224–229. doi: 10.1080/08957959.2010.485391
  • Lavina B, Dera P, Downs RT, Yang W, Sinogeikin S, Meng Y, Shen G, Schiferl D. Structure of siderite FeCO3 to 56 GPa and hysteresis of its spin pairing transition. Phys Rev B. 2010;82(6):064110. doi: 10.1103/PhysRevB.82.064110
  • Birch F. Elasticity and constitution of the earth's interior. J Geophys Res. 1952;57:227–228. doi: 10.1029/JZ057i002p00227
  • Angel RJ. Equations of state. Rev Mineral Geochem. 2000;41(1):35–59. doi: 10.2138/rmg.2000.41.2
  • Shannon RD, Prewitt CT. Effective ionic radii in oxides and fluorides. Acta Crystallogr. 1969;B25:925–946.
  • Shannon RD. Revised effective ionic radii and systematic studies of interatomic distances in halides and chalcogenides. Acta Crystallogr. 1976;A32:751–767.
  • Isshiki M, Irifune T, Hirose K, Ono S, Ohishi Y, Watanuki T, Nishibori E, Takata M, Sakata M. Stability of magnesite and its high-pressure form in the lowermost mantle. Nature. 2004;427:60–63. doi: 10.1038/nature02181
  • Boulard E, Gloter A, Corgne A, Antonangeli D, Auzende AL, Perrillat JP, Guyot F, Fiquet G. New host for carbon in the deep earth. Proc Natl Acad Sci USA. 2011;108(13):5184–5187. doi: 10.1073/pnas.1016934108
  • Merlini M, Perchiazzi N, Hanfland M, Bossak A. Phase transition at high pressure in Cu2CO3OH2 related to the reduction of the Jahn-Teller effect. Acta Crystallogr. 2012;B68(3):266–274.
  • Merrill L, Bassett WA. The crystal structure of CaCO3(II), a high-pressure metastable phase of calcium carbonate. Acta Crystallogr. 1975;B31:343–349.
  • Mao Z, Armentrout M, Rainey E, Manning CE, Dera P, Prakapenka VB, Kavner A. Dolomite III: a new candidate lower mantle carbonate. Geophys. Res. Lett. 2011;38:L22303.
  • Merlini M, Hanfland M, Crichton W. CaCO3-III and CaCO3-VI, high-pressure polymorphs of calcite: possible host structures for carbon in the Earth's mantle. Earth Planet Sci Lett. 2012;333:265–271. doi: 10.1016/j.epsl.2012.04.036
  • Neaton JB, Ashcroft NW. Pairing in dense lithium. Nature. 1999;400:141–144. doi: 10.1038/22067
  • Hanfland M, Syassen K, Christensen NE, Novikov DL. New high-pressure phases of lithium. Nature. 2000;408: 174–178. doi: 10.1038/35041515
  • Schwarz U. Metallic high-pressure modifications of main group elements. Z Kristallogr. 2004;219:376–390. doi: 10.1524/zkri.219.6.376.34637
  • Neaton JB, Ashcroft NW. On the constitution of sodium at higher densities. Phys Rev Lett. 2001;86:2830–2833. doi: 10.1103/PhysRevLett.86.2830
  • Ma Y, Eremets M, Oganov AR, Xie Y, Trojan I, Medvedev S, Lyakhov AO, Valle M, Prakapenka V. Transparent dense sodium. Nature. 2009;458:82–185. doi: 10.1038/nature07786
  • McMahon MI, Nelmes RJ. High-pressure structures and phase transformations in elemental metals. Chem Soc Rev. 2006;35:943–963. doi: 10.1039/b517777b
  • Degtyareva VF, Degtyareva O. Structure stability in the simple element sodium under pressure. New J Phys. 2009;11:063037. doi: 10.1088/1367-2630/11/6/063037
  • Lundegaard LF, Gregoryanz E, McMahon MI, Guillaume C, Loa I, Nelmes RJ. Single-crystal studies of incommensurate Na to 1.5 Mbar. Phys Rev B. 2009;79:064105. doi: 10.1103/PhysRevB.79.064105
  • Franzen HF, Haas C, Jellinek F. Phase transitions between NiAs- and MnP-type phases. Phys Rev. 1974;B10:1248.
  • King HE, Prewitt CT. High-pressure and high-temperature polymorphism of iron sulfide (FeS). Acta Crystallogr. 1982;B38:1877–1887.
  • Ono S, Oganov AR, Brodholt JP, Vočadlo L, Wood IG, Lyakhov A, Glass CW, Côté AS, Price GD. High-pressure phase transformations of FeS: novel phases at conditions of planetary cores. Earth Planet Sci Lett. 2008;272:481–487. doi: 10.1016/j.epsl.2008.05.017
  • Lidin S. Superstructure ordering of intermetallics: B8 structures in the pseudo-cubic regime. Acta Crystallogr. 1998;B54:97–108.
  • Oszlanyi G, Suto A. Ab initio structure solution by charge flipping. Acta Crystallogr. 2004;A60:134–141.
  • Palatinus L, Chapuis G. Superflip – a computer program for the solution of crystal structures by charge flipping in arbitrary dimensions. J Appl Cryst. 2007;40:786–790. doi: 10.1107/S0021889807029238
  • Lundegaard LF, Marqués M, Stinton G, Ackland GJ, Nelmes RJ, McMahon MI. Observation of the oP8 crystal structure in potassium at high pressure. Phys Rev B. 2009;80:020101. doi: 10.1103/PhysRevB.80.020101

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