2,137
Views
26
CrossRef citations to date
0
Altmetric
Original Articles

Single-crystal X-ray diffraction at extreme conditions: a review

, &
Pages 453-465 | Received 22 Jul 2013, Accepted 07 Aug 2013, Published online: 13 Sep 2013

REFERENCES

  • Schwarz U. Metallic high-pressure modifications of main group elements. Z Kristallgr. 2004;219:376–390. doi: 10.1524/zkri.219.6.376.34637
  • McMahon MI, Gregoryanz E, Lundegaard LF, Loa I, Guillaume C, Nelmes RJ, Kleppe AK, Amboage M, Wilhelm H, Jephcoat AP. Structure of sodium above 100 GPa by single-crystal X-ray diffraction. Proc Natl Acad Sci USA. 2007;104:17297–17299. doi: 10.1073/pnas.0709309104
  • Degtyareva O. Simple metals at high pressures. In Boldyreva E, Dera P, editors. High-pressure crystallography from fundamental phenomena to technological applications. Dordrecht, The Netherlands: Springer; 2010. p. 261–280.
  • Boldyreva E. High-pressure studies of pharmaceuticals and biomimetics. Fundamentals and applications. A general introduction, In Boldyreva E, Dera P, editors. High-pressure crystallography from fundamental phenomena to technological applications. Dordrecht, The Netherlands: Springer; 2010. p. 533–543.
  • Fabbiani FPA, Dittrich B, Florence AJ, Gelbrich T, Hursthouse MB, Kuhs WF, Shankland N, Sowa H. Crystal structures with a challenge: high-pressure crystallisation of ciprofloxacin sodium salts and their recovery to ambient pressure. Cryst Eng Comm. 2009;11:1396–1406. doi: 10.1039/b822987b
  • Merrill L, Bassett WA. Miniature diamond anvil cell for single-crystal X-ray diffraction studies. Rev Sci Instrum. 1974;45:290–294. doi: 10.1063/1.1686607
  • Miletich R, Allan DR, Kuhs WF. High-pressure single-crystal techniques. Rev Mineral Geochem. 2000;41:445–519. doi: 10.2138/rmg.2000.41.14
  • Boehler R, De Hantsetters K. New anvil designs in diamond-cells. High Press Res. 2004;24:391–396. doi: 10.1080/08957950412331323924
  • Dittrich B, Hübschle CB, Holstein JJ, Fabbiani FPA. Towards extracting the charge density from normal-resolution data. J Appl Crystallogr. 2009;42:1110–1121. doi: 10.1107/S0021889809034621
  • Trots DM, Kurnosov A, Vasylechko L, Berkowski M, Boffa Ballaran T, Frost DJ. Elasticity and equation of state of . Phys Chem Minerals. 2011;38:561–567. doi: 10.1007/s00269-011-0428-1
  • Patterson BD, Abela R, Braun H-H, Flechsig U, Ganter R, Kim Y, Kirk E, Oppelt A, Pedrozzi M, Reiche S, Rivkin L, Schmidt Th, Schmitt B, Strocov VN, Tsujino S, Wrulich AF. Coherent science at the SwissFEL X-ray laser. New J Phys. 2010;12:035012. doi: 10.1088/1367-2630/12/3/035012
  • Dejoie C, McCusker LB, Baerlocher C, Abela R, Patterson BD, Kunz M, Tamura N. Using a non-monochromatic microbeam for serial snapshot crystallography. J Appl Crystallogr. 2013;46:791–794. doi: 10.1107/S0021889813005888
  • Eremets M. High pressure experimental methods. New York: Oxford University Press; 1996.
  • Dubrovinskaia N, Dubrovinsky L. Whole-cell heater for the diamond anvil cell. Rev Sci Instrum. 2003;74:3433–3437. doi: 10.1063/1.1578151
  • Dubrovinskaia N, Dubrovinsky L. Internal and external electrical heating in diamond anvil cells. In Chen I, Wang Y, Duffy TS, Shen G, Dobrzhinetskaya LF, editors. Advances in high-pressure techniques for geophysical applications. New York: Elsevier; 2005. p. 487–501.
  • Kantor I, Prakapenka V, Kantor A, Dera P, Kurnosov A, Sinogeikin S, Dubrovinskaia N, Dubrovinsky L. BX90: a new diamond anvil cell design for X-ray diffraction and optical measurements. Rev Sci Instrum. 2012;83:125102. doi: 10.1063/1.4768541
  • Rekhi S, Dubrovinsky LS, Saxena SK. Temperature-induced ruby fluorescence shifts up to a pressure of 15 GPa in an externally heated diamond anvil cell. High Temp – High Press. 1999;31:299–305. doi: 10.1068/htrt161
  • Hirose KK. Postperovskite phase transition and its geophysical implications. Rev Geophys. 2006;44:1–44. doi: 10.1029/2005RG000186
  • Dewaele A, Mezouar M, Guignot N, Loubeyre P. Melting of lead under high pressure studied using second-scale time-resolved X-ray diffraction. Phys Rev B. 2007;76:144106. doi: 10.1103/PhysRevB.76.144106
  • Dubrovinsky L, Dubrovinskaia N, Narygina O, Kantor I, Kuznetzov A, Prakapenka VB, Vitos L, Johansson B, Mikhaylushkin AS, Simak SI, Abrikosov IA. Body-centered cubic iron-nickel alloy in Earth's core. Science. 2007;316:1880–1883. doi: 10.1126/science.1142105
  • Fiquet G, Auzende AL, Siebert J, Corgne A, Bureau H, Ozawa H, Garbarino G. Melting of peridotite to 140 Gigapascals. Science. 2010;329:1516–1518. doi: 10.1126/science.1192448
  • Dubrovinsky LS, Saxena SK. Emissivity measurements on some metals and oxides using multiwavelength spectral radiometry. High Temp – High Press. 1999;31:393–399. doi: 10.1068/htrt146
  • Hirose K, Takafuji N, Sata N, Ohishi Y. Phase transition and density of subducted MORB crust in the lower mantle. Earth Planet Sci Lett. 2005;237:239–251. doi: 10.1016/j.epsl.2005.06.035
  • Ricolleau A, Perrilat J-P, Fiquet G, Daniel I, Matas J, Addad A, Menguy N, Cardon H, Mezouar M, Guignot N. Phase relations and equation of state of a natural MORB: implications for the density profile of subducted oceanic crust in the Earth's lower mantle. J Geophys Res. 2010;115:B08202. doi: 10.1029/2009JB006709
  • Shen G, Rivers M, Wang Y, Sutton SR. Laser heated diamond cell system at the Advanced Photon Source for in situ X-ray measurements at high pressure and temperature. Rev Sci Instrum. 2001;72:1273–1280. doi: 10.1063/1.1343867
  • Watanuki T, Shimomura O, Yagi T, Kondo T, Isshiki M. Construction of laser-heated diamond anvil cell system for in situ X-ray diffraction study at Spring-8. Rev Sci Instrum. 2001;72:1289–1292. doi: 10.1063/1.1343869
  • Schultz E, Mezouar M, Crichton W, Bauchau S, Blattmann G, Andrault D, Fiquet G, Boehler R, Rambert N, Sitaud B, Loubeyre P. Double-sided laser heating system for in situ high pressure–high temperature monochromatic X-ray diffraction at the ESRF. High Press Res. 2005;25:71–83. doi: 10.1080/08957950500076031
  • Prakapenka VB, Kubo A, Kuznetsov A, Laskin A, Shkurikhin O, Dera P, Rivers ML, Sutton SR. Advanced flat top laser heating system for high pressure research at GSECARS: application to the melting behavior of germanium. High Press Res. 2008;28:225–235. doi: 10.1080/08957950802050718
  • Dubrovinsky L, Glazyrin K, McCammon C, Narygina O, Greenberg E, Uebelhack S, Chumakov A, Paskarelli S, Prakapenka VB, Bock J, Dubrovinskaia N. Portable laser-heating system for diamond anvil cells. J Synchrotron Radiat. 2009;16:737–741. doi: 10.1107/S0909049509039065
  • Kupenko I, Dubrovinsky L, Dubrovinskaia N, McCammon C, Glazyrin K, Bykova E, Boffa Ballaran T, Sinmyo R, Chumakov AI, Potapkin V, Kantor A, Rüffer R, Hanfland M, Crichton W, Merlini M. Portable double-sided laser-heating system for Mössbauer spectroscopy and X-ray diffraction experiments at synchrotron facilities with diamond anvil cells. Rev Sci Instrum. 2012;83:124501. doi: 10.1063/1.4772458
  • Lavina B, Dera P, Downs RT, Yang W, Sinogeikin S, Meng Y, Shen G, Schiferl D. Structure of siderite FeCO3 to 56 GPa and hysteresis of its spin-pairing transition. Phys Rev B. 2010;82:064110. doi: 10.1103/PhysRevB.82.064110
  • Bassett WA. Deviatoric stress: a nuisance or a gold mine? J Phys: Condens Matter. 2006;18:S921–S931. doi: 10.1088/0953-8984/18/25/S01
  • Kenichi T. Absence of the c/a anomaly in Zn under high pressure with He-pressure medium. Phys Rev B. 1999;60:6171–6174. doi: 10.1103/PhysRevB.60.6171
  • Weinberger MB, Tolbert SH, Kavner A. Osmium metal studied under high pressure and nonhydrostatic stress. Phys Rev Lett. 2008;100:045506. doi: 10.1103/PhysRevLett.100.045506
  • Zhao J, Angel RJ, Ross NL. The structural variation of rhombohedral LaAlO3 perovskite under non-hydrostatic stress fields in a diamond-anvil cell. J Phys: Condens Matter. 2011;23:175901. doi: 10.1088/0953-8984/23/17/175901
  • Dubrovinsky LS, Belonoshko AB. Pressure-induced phase transition and structural changes under deviatoric stress of stishovite to CaCl2-like structure. Geochim Cosmochim Acta. 1996;60:3567–3663. doi: 10.1016/0016-7037(96)00194-9
  • Errandonea D, Meng Y, Somayazulu M, D. Häusermann, Pressure-induced transition in titanium metal: a systematic study of the effect of uniaxial stress. Phys B: Condens Matter. 2005;355:116–125. doi: 10.1016/j.physb.2004.10.030
  • Boldyreva EV, Shakhtshneider TP, Ahsbahs H, Sowa H, Uchtmann H. Effect of high pressure on the polymorphs of paracetamol. J Therm Anal Calorim. 2002;66:437–452.
  • Decker DL, Petersen S, Debray D, Lambert M. Pressure-induced ferroelastic phase-transition in : a neutron-diffraction study. Phys Rev B. 1979;19:3552–3555. doi: 10.1103/PhysRevB.19.3552
  • Resel R, Oehzelt M, Shimizu K, Nakayama A, Takemura K. On the phase-transition in anthracene induced by high pressure. Solid State Commun. 2004;129:103–106. doi: 10.1016/j.ssc.2003.09.019
  • Haines J, Léger JM, Gorelli F, Hanfland M. Crystalline post-quartz phase in silica at high pressure. Phys Rev Lett. 2001;87:15503. doi: 10.1103/PhysRevLett.87.015503
  • Machon D, Dmitriev VP, Bouvier P, Timonin PN, Shirokov VB, Weber H-P. Pseudoamorphization of . Phys Rev B. 2003;68:144104. doi: 10.1103/PhysRevB.68.144104
  • Zhao J, Angel RJ, Ross NL. Effects of deviatoric stresses in the diamond-anvil pressure cell on single-crystal samples. J Appl Crystallogr. 2010;43:743–751. doi: 10.1107/S0021889810016675
  • Angel RJ, Bujak M, Zhao J, Gatta GD, Jacobsen SD. Effective hydrostatic limits of pressure media for high-pressure crystallographic studies. J Appl Crystallogr. 2007;40:26–32. doi: 10.1107/S0021889806045523
  • Dewaele A, Loubeyre P. Pressurizing conditions in helium-pressure-transmitting medium. High Press Res. 2007;27:419–429. doi: 10.1080/08957950701659627
  • Angel RJ, Allan DR, Miletich R, Finger LW. The use of quartz as an internal pressure standard in high-pressure crystallography. J Appl Crystallogr. 1997;30:461–466. doi: 10.1107/S0021889897000861
  • Kurnosov A, Kantor I, Boffa Ballaran T, Lindhardt S, Dubrovinsky L, Kuznetsov A, Zehnder BH. A novel gas-loading system for mechanically closing of various types of diamond anvil cells. Rev Sci Instrum. 2008;79:045110. doi: 10.1063/1.2902506
  • Sato T, Funamori N, Yagi T. Helium penetrates into silica glass and reduces its compressibility. Nature Commun. 2011;2:345. doi: 10.1038/ncomms1343
  • Mao H-K, Xu J, Bell BM. Calibration of the ruby pressure gaige to 800 kbar under quasi-hydrostatic conditions. J Geophys Res. 1986;90:4673–4676. doi: 10.1029/JB091iB05p04673
  • Jacobsen SD, Holl CM, Adams KA, Fischer RA, Martin ES, Bina CR, Lin J-F, Prakapenka VB, Kubo A, Dera P. Compression of single-crystal magnesium oxide to 118 GPa and a ruby gauge for helium pressure media. Am Mineral. 2008;93:1823–1828. doi: 10.2138/am.2008.2988
  • Hess NJ, Schiferl D. Comparison of the pressure-induced frequency shift of Sm:YAG to the ruby and nitrogen vibron pressure scales from 6 to 820 K and 0 to 25 GPa and suggestions for use as a high-temperature pressure calibrant. J Appl Phys. 1992;71:2082–286.
  • Yusa H, Yagi T, Arashi H. Pressure dependence of Sm:YAG fluorescence to 50 GPa: a new calibration as a high pressure scale. J Appl Phys. 1994;75:1463–1466.
  • Mao H-K, Bell PM, Shaner JW, Steinberg DJ. Specific volume measurements of Cu, Mo, Pd, and Ag and calibration of the ruby R1 fluorescence pressure gauge from 0.06 to 1 Mbar. J Appl Phys. 1978;49:3276–3283. doi: 10.1063/1.325277
  • Decker DL, Barnett JD. Proposed thermodynamic pressure scale for an absolute high-pressure calibrant. J Appl Phys. 1970;41:833–835. doi: 10.1063/1.1658775
  • Ruoff AL, Lincoln RC, Chen JC. A new method of absolute high-pressure determination. J Phys D. 1973;55:232–234.
  • Zha C-S, Mao H-K, Hemley RJ. Elasticity of MgO and primary pressure scale to 55 GPa. Proc Natl Acad Sci USA. 2000;97:13494–13499. doi: 10.1073/pnas.240466697
  • Mao Z, Lin J-F, Jacobsen SD, Duffy TF, Chang Y-Y, Smyth JR, Frost DJ, Hauri EH, Prakapenka VB. Sound velocities of hydrous ringwoodite to 16 GPa and 673 K. Earth Planet Sci Lett. 331-2012;332:112–119.
  • Goncharov AF, Sinogeikin S, Crowhurst JC, Ahart M, Lakshtanov D, Prakapenka VB, Bass J, Beck P, Tkachev SN, Zaug JM, Fei Y. Cubic boron nitride as a primary calibrant for a high temperature pressure scale. High Press Res. 2007;27:409–417. doi: 10.1080/08957950701659726
  • Zhuravlev KK, Goncharov AF, Tkachev SN, Dera P, Prakapenka VB. Vibrational, elastic, and structural properties of cubic silicon carbide under pressure up to 75 GPa: implication for a primary pressure scale. J Appl Phys. 2013;113:113503. doi: 10.1063/1.4795348
  • Trots DM, Kurnosov A, Boffa Ballaran T, Tkachev S, Zhuravlev K, Prakapenka V, Berkowski M, Frost DJ. The Sm:YAG primary fluorescence pressure scale. J Geophys Res. submitted.
  • Kurnosov A, Beyer C, Boffa Ballaran T, Trots DM, Pamato M, Frost DJ. New resistive heating setup for single crystal experiments in diamond anvil cells. Rev Sci Instrum. submitted.
  • Wei Q, Dubrovinskaia N, Dubrovinsky L. Ruby and Sm:YAG fluorescence pressure gauges up to 120 GPa and 700 K. J Appl Phys. 2011;110:043513. doi: 10.1063/1.3624618
  • Fei Y, Ricolleau A, Frank M, Mibe K, Shen G, Prakapenka VB. Toward an internally consistent pressure scale. Proc Natl Acad Sci USA. 2007;104:9182–9186. doi: 10.1073/pnas.0609013104
  • McMahon MI, Lundegaard LF, Hejny C, Falconi S, Nelmes RJ. Different incommensurate composite crystal structure for Sc-II. Phys Rev B. 2006;73:134102. doi: 10.1103/PhysRevB.73.134102
  • Gregoryanz E, Lundegaard LF, McMahon MI, Guillaume C, Nelmes RJ, Mezouar M. Structural diversity of sodium. Science. 2008;320:1054–1057. doi: 10.1126/science.1155715
  • Lundegaard LF, Gregoryanz E, McMahon MI, Guillaume C, Loa I, Nelmes RJ. Single-crystal studies of incommensurate Na to 1.5 Mbar. Phys Rev B. 2009;79:064105. doi: 10.1103/PhysRevB.79.064105
  • Maynard-Casely HE, Bull CL, Guthrie M, Loa I, McMahon MI, Gregoryanz E, Nelmes RJ, Loveday JS. The distorted close-packed crystal structure of methane A. J Chem Phys. 2010;133:064504. doi: 10.1063/1.3455889
  • Nelmes RJ, Allan D, McMahon MI, Belmonte S. Self-hosting incommensurate structure of barium IV. Phys Rev Lett. 1999;83:4081–4084. doi: 10.1103/PhysRevLett.83.4081
  • Loa I, Nelmes RJ, Lundegaard LF, McMahon MI. Extraordinarily complex crystal structure with mesoscopic patterning in barium at high pressure. Nature Materials. 2012;11:627–631. doi: 10.1038/nmat3342
  • Merlini M, Crichton WA, Hanfland M, Gemmi M, Müller H, Kupenko I, Dubrovinsky L. Structures of dolomite at ultrahigh pressure and their influence on the deep carbon cycle. Proc Natl Acad Sci USA. 2012;109:13509–13514. doi: 10.1073/pnas.1201336109
  • Lavina B, Dera P, Kim E, Meng Y, Downs RT, Weck PF, Sutton SR, Zhao Y. Discovery of the recoverable high-pressure iron oxide . Proc Natl Acad Sci USA. 2011;108:17281–17285. doi: 10.1073/pnas.1107573108
  • Koch M, Woodland AB, Angel RJ. Stability of spinelloid phases in the system –– at 1100°C and up to 10.5 GPa. Phys Earth Planet Int. 2004;143–144:171–183. doi: 10.1016/j.pepi.2003.06.001
  • Merlini M, Hanfland M, Gemmi M, Huotari S, Simonelli L, Strobel P. Fe3+ spin transition in at high pressure. Am Mineral. 2010;95:200–203. doi: 10.2138/am.2010.3347
  • Prescher C, Dubrovinsky L, McCammon C, Glazyrin K, Nakajima Y, Kantor A, Merlini M, Hanfland M. Structurally hidden magnetic transitions in Fe3C at high pressures. Phys Rev B. 2012;85: 140402 (R). doi: 10.1103/PhysRevB.85.140402
  • Boffa Ballaran T, Kurnosov A, Glazyrin K, Frost DJ, Merlini M, Hanfland M, Caracas R. Effect of chemistry on the compressibility of silicate perovskite in the lower mantle. Earth Planet Sci Lett. 2012;333–334:181–190. doi: 10.1016/j.epsl.2012.03.029
  • Dubrovinsky L, Boffa Ballaran T, Glazyrin K, Kurnosov A, Frost DJ, Merlini M, Hanfland M, Prakapenka VB, Schouwink P, Pippinger T, Dubrovinskaia N. Single crystal X-ray diffraction at megabar pressures and temperatures of thousands of degrees. High Press Res. 2010;30:620–633. doi: 10.1080/08957959.2010.534092

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.