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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 190, 2015 - Issue 12: Robert Holmes Special Issue
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Original Articles

Synthesis and Characterization of (Disilylanilino)Phosphines

Pradeep DevulapalliDepartment of Chemistry, Texas Christian University, Fort Worth, 76134, TX, USA
,
Bin WangDepartment of Chemistry, Texas Christian University, Fort Worth, 76134, TX, USA
&
Robert H. NeilsonDepartment of Chemistry, Texas Christian University, Fort Worth, 76134, TX, USACorrespondence[email protected]
Pages 2154-2163 | Received 17 Jun 2015, Accepted 29 Jun 2015, Published online: 10 Dec 2015

REFERENCES

  • Neilson, R.H. Phosphorus-nitrogen compounds. In: R.B. King (Ed.), Encyclopedia of Inorganic Chemistry, Vol 6; John Wiley & Sons: Chichester, England, 1994, pp. 3180-3199.
  • For example, see the following and references cited therein: (a) Scheide, G.M.; Neilson, R.H. Organometallics 1989, 8, 1987-1991. (b)Morton, D.W.; Neilson, R.H. Organometallics 1982, 1, 289-295. (c)Neilson, R.H.; Wisian-Neilson, P.; Wilburn, J.C. Inorg. Chem. 1980, 19, 413-416. (d)Wilburn, J.C.; Neilson, R.H. Inorg. Chem. 1979, 18, 347-351.
  • For early examples, see: (a) Wisian-Neilson, P.; Neilson, R.H.; Cowley, A.H. Inorg. Chem. 1977, 16, 1460-1463. (b)Wisian-Neilson, P.; Neilson, R.H. J. Am. Chem. Soc. 1980, 102, 2848-2849.
  • See, for example: (a) Neilson, R.H.; Klaehn, J.R. J. Inorg. Organomet. Polym. 2006, 16, 319-326.(b)Wisian-Neilson, P.; Johnson, R.S.; Zhang, H.; Jung, J.-H.; Neilson, R.H.; Ji, J.; Watson, W.H.; Krawiec, M. Inorg. Chem. 2002, 41, 4775-4779. (c)Jung, J.-H.; Pomeroy, J.C.; Zhang, H.; Wisian-Neilson, P. J. Am. Chem. Soc. 2003, 125, 15537-15542.
  • See, for example: (a) Neilson, R.H.; Hani, R.; Wisian-Neilson, P.; Meister, J.J.; Roy, A.K.; Hagnauer, G.L. Macromolecules 1987, 20, 910-916. (b)Neilson, R.H.; Wisian-Neilson, P. Chem. Rev. 1988, 88, 541-562. (c)Wisian-Neilson, P.; Neilson, R.H. Inorg. Synth. 1989, 25, 69-74. (d)Matyjaszewski, K.; Dauth, J.; Montague, R.A.; Reddick, C.; White, M.L. J. Am. Chem. Soc. 1990, 112, 6721-6723.(e)White, M.L.; Matyjaszewski, K. J. Polym. Science (A) 1996, 34, 277-289. (f)Honeyman, C.H.; Manners, I.; Morrissey, C.T.; Allcock, H.R. J. Am. Chem. Soc. 1995, 117, 7035-7036.(g)Allcock, H.R.; Crane, C.A.; Morrissey, C.T.; Nelson, J.M.; Reeves, S.D.; Honeyman, C.H.; Manners, I. Macromolecules 1996, 29, 7740-7747. (h)Allcock, H.R.; Nelson, J.M.; Reeves, S.D.; Honeyman, C.H.; Manners, I. Macromolecules 1997, 30, 50-56. (i)Wang, B.; Rivard, E.; Manners, I. Inorg. Chem. 2002, 41, 1690-1691. (j)Wang, B. Macromolecules 2005, 38, 643-645.
  • Some preliminary aspects of this work were briefly reported in a conference proceedings but without experimental details. See: Neilson, R.H.; Devulapalli, P.; Jackson, B.K.; Neilson, A.R.; Parveen, S.; Wang, B. ACS Sympos. Ser. 2006, 917, 325-334.
  • Broser, W.; Harrer, W. Angew. Chem. Int. Ed. Engl. 1965, 4, 1081.
  • Nöth, H.; Vetter, H.-J. Chem. Ber. 1963, 96, 1109.
  • Lenton, M.V.; Lewis, B. Chem. Indus. 1965, 946-947.
  • For other syntheses and NMR data of Me(Ph)PCl, see: (a) Wolfsberger, W. J. Organomet. Chem. 1986, 317, 167-173.(b)Lindner, E.; Merkle, R.D.; Mayer, H.A. Chem. Ber. 1986, 119, 645-658.
  • Wilburn, J.C.; Neilson, R.H. Inorg. Chem. 1979, 18, 347-351. (b)Neilson, R.H.; Wisian-Neilson, P. Inorg. Chem. 1982, 21, 3568-3569.
  • For comparative 31P NMR data, see: (a) Crutchfield, M.M.; Dungan, C.H.; Letcher, J.H.; Mark, V.; Van Wazer, J.R. P-31 nuclear magnetic resonance. In: M. Grayson; E.J. Griffith (Eds.), Topics in Phosphorus Chemistry, . Vol. 5; John Wiley & Sons: New York, 1967. (b)Verkade, J.G.; Quin, L.D. Phosphorus-31 NMR spectroscopy in stereochemical analysis. In: A.P. Marchand (Ed.), Methods in Stereochemical Analysis, Vol. 8; VCH Publishers: Dearfield Beach, FL, 1987.

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