1,085
Views
37
CrossRef citations to date
0
Altmetric
Original Articles

Thin Layer Chromatographic Analysis of Biological Samples. A Review

&
Pages 2297-2314 | Received 24 Mar 2005, Accepted 11 Apr 2005, Published online: 06 Feb 2007

References

  • Zarzycki , P. , Kulhanek , K. M. , Smith , R. , Bartoszuk , M. A. and Lamparczyk , H. 2005 . Planar chromatography versus column chromatography: a performance comparison . LCGC North America , 23 : 286 288 292 294 296 299 300
  • Fried , B. and Sherma , J. 1999 . Thin Layer Chromatography , 4th Ed. New York : Marcel Dekker, Inc. .
  • Sherma , J. and Fried , B. , eds. 2003 . Handbook of Thin Layer Chromatography , 3rd Ed. New York : Marcel Dekker, Inc. .
  • Fried , B. and Sherma , J. , eds. 1996 . Practical Thin Layer Chromatography Boca Raton, FL : CRC Press .
  • Bladek , J. and Neffe , S. 2003 . Application of thin layer chromatography in clinical chemistry . Separ. Purif. Rev. , 32 : 61 – 120 .
  • Boddy , A. V. and Idle , J. R. 1992 . Combined thin layer chromatography‐photography‐densitometry for the quantification of ifosfamide and its principal metabolites in urine, cerebrospinal fluid, and plasma . J. Chromatogr. , 575 : 137 – 142 .
  • Negroni , E. , Chigorno , V. , Tettamanti , G. and Sonnino , S. 1996 . Evaluation of the efficiency of an assay procedure for gangliosides in human serum . Glycoconj. J. , 13 : 347 – 352 .
  • Wilson , J. F. , Williams , J. , Walker , P. A. , Toseland , B. L. , Smith , A. and Burnett , D. 1991 . Performance of techniques used to detect drugs of abuse in urine: study based on external quality assessment . Clin. Chem. , 37 : 442 – 447 .
  • Cenni , B. and Betschart , B. 1994 . The determination of halofantrine in biological samples by high performance thin layer chromatography . J. Planar Chromatogr.—Mod. TLC , 7 : 294 – 296 .
  • van Ginkel , L. A. , van Blitterswijk , H. , Zoontijes , P. W. , van den Bosch , D. and Stephany , R. W. 1988 . Assay for trenbolone and its metabolite 17 alpha‐trenbolone in bovine urine based on immunoaffinity chromatographic cleanup and off‐line high performance liquid chromatography‐thin layer chromatography . J. Chromatogr. , 445 : 385 – 392 .
  • Kharat , V. R. , Verma , K. K. and Dhake , J. D. 2002 . Determination of lacidipine from urine by HPTLC using off‐line SPE . J. Pharm. Biomed. Anal. , 28 : 789 – 793 .
  • Tyrpien , K. , Wielkoszynski , T. , Janoszka , B. , Dobosz , C. , Bodzek , D. and Steplewski , Z. 2000 . Application of liquid separation techniques to the determination of the main urinary nicotine metabolites . J. Chromatogr. A , 870 : 29 – 38 .
  • Schneck , J. L. , Fried , B. and Sherma , J. 2004 . Thin layer chromatographic analysis of neutral lipids in snail conditioned water and feces of Biomphalaria glabrata infected with Echinostoma caproni . J. Liq. Chromatogr. & Relat. Technol. , 27 : 2039 – 2045 .
  • Misztal , G. , Paw , B. , Skibinski , R. , Komsta , L. and Iwaniak , K. 2002 . Analysis of some nonselective calcium channel blockers in normal phase chromatographic systems . J. Planar Chromatogr.—Mod. TLC , 15 : 458 – 462 .
  • Tyrpien , K. , Bodzek , P. and and Manka , G. 2001 . Application of planar chromatography to the determination of nicotine in urine of active and passive smoking pregnant women . Biomed. Chromatogr. , 15 : 50 – 55 .
  • Eidam , P. M. , Schariter , J. A. , Fried , B. and Sherma , J. 2001 . HPTLC analysis of tissue and blood of Biomphalaria glabrata snails to assess the effects of a diet of Romaine lettuce leaf versus midrib on the concentrations of lipids, pigments, and carbohydrates . J. Liq. Chromatogr. & Relat. Technol. , 24 : 1467 – 1478 .
  • Cserhati , T. 1991 . Retention behavior of some synthetic nucleosides on CN, diol, and NH2 precoated high performance thin layer chromatographic plates . J. Chromatogr. Sci. , 29 : 210 – 216 .
  • Pachuski , J. , Fried , B. and Sherma , J. 2002 . HPTLC analysis of amino acids in Biomphalaria glabrata infected with Schistosoma mansoni . J. Liq. Chromatogr. & Relat. Technol. , 25 : 2345 – 2349 .
  • Li , L. , Shen , G. , Jiang , J. , Cheng , X. , Zhou , X. , Zhang , Ch. and Zhao , G. 1985 . Thin layer chromatographic determinations of the ratio of serum free branched chain amino acids to aromatic amino acids . Chinese, J. Med. , 68 : 298 – 301 .
  • Steinberg , J. J. , Cajigas , A. and Brownlee , M. 1992 . Enzymatic shotgun 5′‐phosphorylation and 3′‐sister phosphate exchange: a two‐dimensional thin layer chromatographic technique to measure DNA deoxynucleotide modification . J. Chromatogr. , 574 : 41 – 55 .
  • Abjean , J.‐P. and Lahogne , V. 1997 . Planar chromatography for quantitative determination of ampicillin residues in milk and muscle . J. AOAC Int. , 80 : 1171 – 1176 .
  • Wang , P.‐L. , Feng , Y.‐L. and Chen , L. 1997 . Simultaneous determination of norfloxacin, pefloxacin, and ciprofloxacin in body fluid by TLC‐fluorescence spectrodensitometry . Microchem. J. , 56 : 229 – 235 .
  • Anderton , C. A. , Fried , B. and Sherma , J. 1993 . HPTLC determination of sugars in the hemolymph and digestive gland‐gonad complex of Biomphalaria glabrata snails . J. Planar Chromatogr.—Mod. TLC , 6 : 51 – 54 .
  • Bereznitski , Y. , Thompson , R. , O'Neill , E. and Grinberg , N. 2001 . Thin layer chromatography‐a useful techniques for the separation of enantiomers . J. AOAC Int. , 84 : 1242 – 1251 .
  • Pandya , K. K. , Satia , M. C. , Modi , I. A. , Modi , R. I. , Chakravarthy , B. K. and Gandhi , T. P. 1997 . High performance thin layer chromatography for the determination of nimesulide in human plasma, and its use in pharmacokinetic studies . J. Pharm. Pharmacol. , 49 : 773 – 776 .
  • Palamarev , Ch. E. , Kandinska , M. I. and Palamareva , M. D. 2004 . Automatic selection of mobile phases. IV. thin layer chromatography on silica of simple and complex organic compounds . J. Liq. Chromatogr. & Relat. Technol. , 27 : 2003 – 2018 .
  • 1987 . Weinheim, , Germany : VCH . International Association of Forensic Toxicology. Report VII of the DFG Commission for Clinical‐Toxicological Analysis (special issue of the TIAFT bulletin)
  • Hsieh , M. C. and Berry , H. K. 1992 . Detection of metabolic diseases by thin layer chromatography . J. Planar Chromatogr.—Mod. TLC , 2 : 118 – 123 .
  • Marsit , C. J. , Fried , B. and Sherma , J. 2000 . Carbohydrate analysis, by high performance thin layer chromatography, of Cerithidea californica (Gastropoda: Prosobranchia) . J. Liq. Chromatogr. & Relat. Technol. , 23 : 2413 – 2417 .
  • Farwanah , H. , Neubert , R. , Zellmer , S. and Raith , K. 2002 . Improved procedure for the separation of major stratum corneum lipids by means of automated multiple development . J. Chromatogr. B , 780 : 443 – 450 .
  • Bladek , J. and Zdrojewski , A. 2003 . Thin layer chromatography and solid phase extraction analysis of urinary porphyrins . Chem. Analit. (Warsaw) , 48 : 689 – 696 .
  • Tyihak , E. , Botz , L. , Ott , P. , Nagy , S. , Kiraly‐Veghely , Zs. and Mincsovics , E. 2003 . The combination of overpressured layer chromatography and bioautography and its application to the analysis of molecules influencing cell proliferation . Chem. Analit. (Warsaw) , 48 : 543 – 553 .
  • Tyihak , E. , Katy , Z. , Ostorics , Z. and Mincsovics , E. 1998 . Analysis of amino acids by a personal OPLC system. 1. separation of the main protein amino acids in a double layer system . J. Planar Chromatogr.—Mod. TLC , 11 : 5 – 11 .
  • Schariter , J. A. , Pachuski , J. , Fried , B. and Sherma , J. 2002 . Determination of neutral lipids and phospholipids in the cercariae of Schistosoma mansoni by high performance thin layer chromatography . J. Liq. Chromatogr. & Relat. Technol. , 25 : 1615 – 1622 .
  • Ponder , E. L. , Fried , B. and Sherma , J. 2004 . Thin layer chromatographic analysis of hydrophilic vitamins in standards and from Helisoma trivolvis snails . Acta Chromatogr. , 14 : 70 – 81 .
  • Klaus , R. , Fischer , W. and Hauck , H. E. 1993 . Extension of the application of thermal in situ reaction on NH2‐layers to the detection of catecholamines in biological materials . Chromatographia , 37 : 133 – 143 .
  • Muething , J. and Cacic , M. 1997 . Glycosphingolipid expression in human skeletal and heart muscle assessed by immunostaining thin layer chromatography . Glycoconj. J. , 14 : 19 – 28 .
  • Muething , J. 1996 . High resolution thin layer chromatography of gangliosides . J. Chromatogr. , 720 : 3 – 25 .
  • Ebel , S. and Kang , J. S. 1990 . UV/Vis spectra and spectral libraries in TLC/HPTLC. 1. Background correction and normalization . J. Planar Chromatogr.—Mod. TLC , 3 : 42 – 46 .
  • Spangenberg , B. , Post , P. and Ebel , S. 2002 . Fiber optical scanning in TLC by use of a diode array detector‐linearization models for absorption and fluorescence evaluation . J. Planar Chromatogr.—Mod. TLC , 15 : 88 – 93 .
  • Pisternick , W. , Kovar , K.‐A. and Ensslin , H. 1997 . High performance thin layer chromatographic determination of N‐ethyl‐3,4‐methylenedioxyamphetamine and its major metabolites in urine and comparison with high performance liquid chromatography . J. Chromatogr. B , 688 : 63 – 69 .
  • Wagner , J. , Jork , H. and Koglin , E. 1993 . HPTLC as a reference method in clinical chemistry: on‐line coupling with spectroscopic methods . J. Planar Chromatogr.—Mod. TLC , 6 : 446 – 451 .
  • Brzezinska , H. , Dallakian , P. and Budzikiewicz , H. 1999 . Thin layer chromatography and mass spectrometry for screening of biological samples for drugs and metabolites . J. Planar Chromatogr.—Mod. TLC , 12 : 96 – 108 .
  • Rudloff , S. , Pohlentz , G. , Diekmann , L. , Egge , H. and Kunz , C. 1996 . Urinary excretion of lactose and oligosaccharides in pre‐term infants fed human milk or infant formula . Acta Pediat. , 85 : 598 – 603 .
  • Cserhati , T. and Forgacs , E. 1998 . Hyphenated techniques in thin layer chromatography . J. AOAC Int. , 81 : 329 – 332 .
  • Bauer , G. K. , Pfeifer , A. M. , Hauck , H. E. and Kovar , K.‐A. 1998 . Development of an optimized sorbent for direct HPTLC‐FTIR on‐line coupling . J. Planar Chromatogr.—Mod. TLC , 11 : 84 – 89 .
  • Busch , K. 1992 . Coupling thin layer chromatography with mass spectrometry . J. Planar Chromatogr.—Mod. TLC , 5 : 72 – 79 .
  • Tames , F. , Watson , I. D. , Morden , W. E. and Wilson , I. D. 2000 . Analysis of benzodiazepines by thin layer chromatography and tanden mass spectrometry . J. Planar Chromatogr.—Mod. TLC , 13 : 432 – 436 .
  • Lekeyi , B. , Csanyi , J. and Nanasi , P. 1986 . A rapid determination of sucrose and fructose in biological samples by videodensitometry . J. Liq. Chromatogr. , 9 : 1869 – 1875 .
  • Anderton , S. M. , Layman , L. R. and Sherma , J. 1998 . Determination of blood glucose by quantitative TLC on preadsorbent silica gel plates . J. Liq. Chromatogr & Relat. Technol. , 21 : 1045 – 1049 .
  • De Maglio , D. C. and Svanberg , G. K. 1996 . A thin layer chromatographic procedure for the separation of proline and hydroxyproline from biological samples . J. Liq. Chromatogr. & Relat. Technol. , 19 : 969 – 975 .
  • Corley , R. A. , Swanson , S. P. and Buck , W. B. 1985 . Glucuronide conjugates of T‐2 toxin and metabolites in swine bile and urine . J. Agric. Food Chem. , 33 : 1085 – 1089 .
  • Hazai , I. 2004 . Use of multiple readings to increase the sensitivity of phosphor image detection in TLC . J. Planar Chromatogr.—Mod. TLC , 17 : 449 – 453 .
  • Klebovich , I. 2001 . “ Application of planar chromatography and digital autoradiography in metabolism research ” . In Planar Chromatography Edited by: Nyiredy , Sz. 293 – 311 . Budapest, , Hungary : Springer Scientific Publisher .
  • Christelle , C. , Vingler , P. , Boyera , N. , Galey , I. and Bernard , B. A. 1997 . Direct quantitative digital autoradiography TLC coupling for the analysis of neutral 14C‐lipids neosynthesized by the human sebaceous gland . J. Planar Chromatogr.—Mod. TLC , 10 : 243 – 250 .
  • Ohtake , H. , Hase , Y. , Sakemoto , K. , Oura , T. , Wada , Y. and Kodama , H. 1995 . A new method to detect homocysteine in dried blood spots using thin layer chromatography . Screening , 4 : 17 – 26 .
  • Guermouche , M.‐H. 1991 . Assay of pyrazinamide in human serum by HPTLC . J. Planar Chromatogr.—Mod. TLC , 4 : 166 – 167 .
  • Feng , Y.‐L. and Dong , C. 2004 . Simultaneous determination of trace ofloxacin, ciprofloxacin, and sparfloxacin by micelle TLC‐fluorimetry . J. Chromatogr. Sci. , 42 : 474 – 477 .
  • Bailey , D. N. 1994 . Thin layer chromatographic detection of cocaethylene in human urine . Am. J. Clin. Path. , 101 : 342 – 345 .
  • Ojanpera , I. , Ojansivu , R.‐L. , Nokua , J. and Vuori , E. 1999 . Comprehensive TLC drug screening in forensic toxicology: comparison of findings in urine and liver . J. Planar Chromatogr.—Mod. TLC , 12 : 38 – 41 .
  • Ludanyi , K. , Gomory , A. , Klebovich , I. , Monostory , K. , Vereczkey , L. , Ujszaszy , K. and Vekey , K. 1997 . Application of TLC‐FAB mass spectrometry in metabolism research . J. Planar Chromatogr.—Mod. TLC , 10 : 90 – 96 .
  • Bhogte , Ch. P. , Patravale , V. B. and Devarajan , P. V. 1997 . Fluorodensitometric evaluation of gentamycin from plasma and urine by high performance thin layer chromatography . J. Chromatogr. B , 694 : 443 – 447 .
  • Guermouche , M. H. , Habel , D. and Guermouche , S. 1999 . Assay if tinidazole in human serum by high performance thin layer chromatography‐comparison with high performance liquid chromatography . J. AOAC Int. , 82 : 244 – 247 .
  • Batisse , C. , Daurade , M.‐H. and Bounias , M. 1992 . TLC separation and spectrodensitometric quantitation of cell wall neutral sugars . J. Planar Chromatogr.—Mod. TLC , 5 : 131 – 133 .
  • Jarusiewicz , J. A. , Fried , B. and Sherma , J. 2004 . High performance thin layer chromatographic analysis of neutral lipids and phospholipids in the apple snail Pomacea bridgesii . J. Planar Chromatogr.—Mod. TLC , 17 : 454 – 458 .
  • Skarkova , J. and Ostry , V. 2000 . An HPTLC method for confirmation of the presence of utlra‐trace amounts of aflatoxin M1 in human urine . J. Planar Chromatogr.—Mod. TLC , 13 : 42 – 44 .
  • Degtiar , W. G. , Tyaglov , B. V. , Degterev , E. V. , Krylov , V. M. , Malakhova , I. I. and Krasikov , V. D. 2000 . Quantitative analysis of L‐lysine, L‐threonine, L‐homoserine, and cobalamines in fermentation broth . J. Planar Chromatogr.—Mod. TLC , 13 : 217 – 220 .
  • Yrjonen , T. , Haansuu , J. P. , Haahtela , K. , Vuorela , H. and Vuorela , P. 2001 . Rapid screening of indole‐3‐acetic acid and other indole derivatives in bacterial culture broths by planar chromatography . J. Planar Chromatogr.—Mod. TLC , 14 : 47 – 52 .
  • Tyihak , E. , Ott , P. , Moricz , A. M. , Katay , G. and Kiraly‐Veghely , Z. 2004 . Antibiosis, Antibiotics, and the formaldehyde cycle: the unique importance of planar chromatographic techniques to progress in these fields . J. Planar Chromatogr.—Mod. TLC , 17 : 84 – 88 .
  • LeFevre , J. W. , Gublo , E. J. , Botting , C. , Wall , R. , Nigro , A. , Pham , M. T. and Ganci , G. 2000 . Qualitative reversed phase thin layer chromatographic analysis of the stereochemistry of D‐ and L‐alpha‐amino acids in small peptides . J. Planar Chromatogr.—Mod. TLC , 13 : 160 – 165 .
  • Kim , Y. , Fried , B. and Sherma , J. 2002 . Thin layer chromatographic analysis of lutein and beta‐carotene in Biomphalaria glabrata maintained on a high fat diet . Veliger , 45 : 256 – 258 .
  • Balikova , M. , Novakova , E. and Kohlicek , J. 1988 . Identification of polychlorinated phenols in urine by gas and thin layer chromatography . J. Chromatogr. , 431 : 431 – 437 .
  • Lamperti , L. and Vega , M. 1992 . Separation of hydroxylated conjugated bile acids by instrumental HPTLC . J. Planar Chromatogr.—Mod. TLC , 5 : 139 – 140 .
  • Makki , S. , Thanh , T. T. , Chinkarenko , T. and Guinchard , C. 1991 . Optimizing the one‐dimensional planar chromatographic separation of the principal psoralens used in therapy . J. Planar Chromatogr.—Mod. TLC , 4 : 213 – 217 .

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.