Development and Validation of a Rapid HPLC Method for the Direct Determination of Colchicine in Pharmaceuticals and Biological Fluids

References

• Tsai , T.‐H. 2001 . Analytical approaches for traditional Chinese medicines exhibiting antineoplastic activity . J. Chromatogr. B , 764 : 27 – 48 .
   PubMed Web of Science ®Google Scholar
• Jones , G. , Singer , P. and Bannach , B. 2002 . Application of LC‐MS analysis to a colchicine fatality . J. Anal. Toxicol. , 26 : 365 – 369 .
   PubMed Web of Science ®Google Scholar
• Klintschar , M. , Beham‐Schimdt , C. , Radner , H. , Henning , G. and Roll , P. 1999 . Forensic science international , 106 : 191 – 200 .
   PubMed Web of Science ®Google Scholar
• (March 2005) http://www.merck.com/mrkshared/mmanual/section21/chapter289/289a.jsp
   Google Scholar
• (March 2005) http://www.medicinenet.com/colchicine/article.htm
   Google Scholar
• Allender , W. J. 1982 . Colchicine poisoning as a mode of suicide . J. Forensic Sci. , 27 : 944 – 947 .
   PubMed Web of Science ®Google Scholar
• Kintz , P. , Jamey , C. , Tracqui , A. and Mangin , P. 1997 . Colchicine poisoning: report of a fatal case and presentation of an HPLC procedure for body fluid and tissue analyses . J. Anal. Toxicol. , 21 : 70 – 72 .
   PubMed Web of Science ®Google Scholar
• Ko , R. J. , Li , W. Y. and Koda , R. T. 1990 . Determination of the antimitotic agents N‐desacetylcolchicine, demecolcine and colchicine in serum and urine . J. Chromatogr. B. , 525 ( 2 ) : 411 – 418 .
   Google Scholar
• Fernandez , P. , Bermejo , A. M. , Tabernero , M. J. , Lopezrivadulla , M. and Cruz , A. 1993 . Determination of colchicine in biological‐fluids by reverse‐phase HPLC – variation of colchicine levels in rats . Forensic Sci. Inter. , 59 ( 1 ) : 15 – 18 .
   PubMed Web of Science ®Google Scholar
• Rosso , A. and Zuccaro , S. 1998 . Determination of alkaloids from the colchicine family by reversed‐phase high‐performance liquid chromatography . J. Chromatogr. A , 825 ( 1 ) : 96 – 101 .
   Web of Science ®Google Scholar
• Dehon , B. , Chagnon , J. L. , Vinner , E. , Pommery , J. , Mathieu , D. and Lhermitte , M. 1999 . Colchicine poisoning: report of a fatal case with body fluid and post‐mortem tissue analysis by HPLC . Biomed. Chromatogr. , 13 : 235 – 238 .
   PubMed Web of Science ®Google Scholar
• Petty , H. , Fernando , M. , Kindzelskii , A. , Zarewych , B.N. , Ksebati , M. and Hryhorczuk Mobashery , S. 2001 . Identification of colchicine in placental blood from patients using herbal medicines . Chem. Res. Toxicol. , 14 : 1254 – 1258 .
   PubMed Web of Science ®Google Scholar
• Li , W. , Fitzloff , J. F. , Farnsworth , N. R. and Fong , H. H.S. 2002 . Evaluation of commercial Ginkgo biloba dietary supplements for the presence of colchicine by HPLC . Phytomedicine , 9 : 442 – 446 .
   PubMed Web of Science ®Google Scholar
• Ellington , E. , Bastida , J. , Viladomat , F. and Codina , C. 2003 . Supercritical carbon dioxide extraction of colchicine and related alkaloids from seeds of colchicum autumnale . Phytochem. Anal. , 14 ( 3 ) : 164 – 169 .
   PubMed Web of Science ®Google Scholar
• Deveaux , M. , Hubert , N. and Demarly , C. 2004 . Colchicine poisoning: case report of two suicides . Forensic Sci. Inter. , 143 : 219 – 222 .
   PubMed Web of Science ®Google Scholar
• Hoja , H. , Marquet , P. , Verneuil , B. , Lotfi , H. , Dupuy , J. L. , Dreyfuss , M. F. and Lachatre , G. 1996 . Determination of colchicine in biological fluids by liquid chromatography mass spectrometry with pneumatically assisted electrospray ionization . Analusis , 24 ( 9–10 ) : 391 – 394 .
   Google Scholar
• Tracqui , A. , Kintz , P. , Ludes , B. , Rouge , C. , Douibi , H. and Mangin , P. 1996 . High‐performance liquid chromatography coupled to ion spray mass spectrometry for the determination of colchicine at ppb levels in human biofluids . J. Chromatogr. B , 675 ( 2 ) : 235 – 242 .
   PubMed Web of Science ®Google Scholar
• Li , W. , Sun , Y. , Fitzloff , J. F. and Van Breemen , R. B. 2002 . Evaluation of commercial Ginkgo and Echinacea Dietary Supplements for colchicine using Liquid Chromatography‐Tandem Mass Spectrometry . Chem. Res. Toxicol. , 15 : 1174 – 1178 .
   PubMed Web of Science ®Google Scholar
• Popova , O. I. and Kudrin , S. A. 1991 . Quantitative‐determination of colchamine and colchicine by gas‐liquid‐chromatography . Khimiko‐Farmatsevticheskii Zhurnal Mar , 25 ( 3 ) : 59 – 60 .
   Google Scholar
• Clevenger , C. V. , August , T. F. and Shaw , L. M. 1991 . Colchicine poisoning—report of a fatal case with body‐fluid analysis by Gc/Ms and histopathologic examination of postmortem tissues . J. Anal. Toxicol. , 15 ( 3 ) : 151 – 154 .
   PubMed Web of Science ®Google Scholar
• Sarg , T. M. , Eldomiaty , M. M. , Bishr , M. M. , Salama , O. M. and Elgindy , A. R. 1989 . Thin‐layer chromatographic scanner, spectrophotometric and high‐performance liquid‐chromatographic methods for the determination of colchicine analyst. , 114 ( 5 ) : 575 – 578 .
   Google Scholar
• Glavac , D. 1992 . R m Values of some colchicine and colchiceinamides determined by reversed‐phase thin‐layer chromatography . J. Chromatogr. , 591 ( 1–2 ) : 367 – 370 .
   PubMedGoogle Scholar
• Panariti , E. 1996 . Meadow saffron (colchicum autumnale) intoxication in a nomadic albanian sheep flock.vet . Human Toxicol. , 38 ( 3 ) : 227 – 228 .
   Google Scholar
• Bodoki , E. , Oprean , R. , Vlase , L. , Tamas , M. and Sandulescu , R. 2004 . Fast determination of colchicine by TLC densitometry from pharmaceuticals and vegetal extracts . J. Pharm. Biomed. Anal. , 18 ( 3 ) : 24 – 27 .
   Google Scholar
• Kovatsis , V. A. , Christianopoulou , M. N. and Papageorgiou , V. P. 1980 . “ Determination of Colchicine in Biological Samples by Indirect Atomic Absorption Spectroscopy ” . In Toxicological Aspects Vol. 220 , Procds. IXth International Congress of the European Association of poison control centers and European meeting of the International Association of Forensic Toxicologists, Thessaloniki, August 1980, 24–27.
   Google Scholar
• Li , G. Z. and Liu , Y. M. 1999 . Fluorescence analysis of colchicine by hydrolysis and complexation with lanthanium . Fenxi Shiyaushi , 18 ( 3 ) : 74 – 76 .
   Google Scholar
• Liu , Y. M. and Li , G. Z. 2000 . Determination of colchicine in tablet by fluorimetry . Chinese J. Anal. Chem. , 28 ( 3 ) : 330 – 332 .
   Web of Science ®Google Scholar
• Singh , D. K. , Srivastava , B. and Sahu , A. 2004 . Spectrophotometric determination of colchicine using iron(III) chloride and 1,10‐phenanthroline . J. Indian Chem. Soc. , 81 ( 2 ) : 171 – 173 .
   Web of Science ®Google Scholar
• Wang , J. and Ozsoz , M. 1990 . Trace measurements of colchicine by adsorptive stripping voltammetry . Talanta , 37 ( 8 ) : 783 – 787 .
   PubMed Web of Science ®Google Scholar
• Yu , S. H. , Leng , Z. Z. , Hu , X. Y. and Yang , C. 1997 . Adsorptive voltammetry behaviour of colchicine on a carbon paste electrode . Fenxi Huaxue , 23 ( 10 ) : 1217 – 1220 .
   Google Scholar
• Holak , W. and Plank , Wm. 1980 . Differential pulse polarographic‐determination of colchicine . J. Pharm. Sci. , 69 ( 12 ) : 1436 – 1438 .
   PubMed Web of Science ®Google Scholar
• Kasim , E. A. 2002 . Voltammetric behaviour of the anti‐inflammatory alkaloid colchicine at a glassy electrode and a hanging mercury electrode and its determination at ppb levels . Anal. Lett. , 35 ( 12 ) : 1987 – 2004 .
   Web of Science ®Google Scholar
• Poulev , A. , Deusneumann , B. , Bombardelli , E. and Zenk , M. H. 1994 . Immunoassays for the quantitative‐determination of colchicine . Planta Medica , 60 ( 1 ) : 77 – 83 .
   PubMed Web of Science ®Google Scholar
• Rouan , S. K.E. , Otterness , I. G. , Gans , D. J. and Rhodes , C. T. 1991 . A radioimmunoassay for colchicine using a highly specific, high‐affinity monoclonal‐antibody . Drug Dev. Ind. Pharm. , 17 ( 17 ) : 2391 – 2400 .
   Web of Science ®Google Scholar
• Sabouraud , A. , Cano , N. and Scherrmann , J. M. 1994 . Radioimmunoassay of colchicine with antisera exhibiting variable cross‐reactivity . Ther. Drug Monit. , 16 ( 2 ) : 179 – 185 .
   PubMed Web of Science ®Google Scholar
• Wang , N. , Zhao , B. and Shao , B. 1993 . Preparation and application of colchicine sensor . Huaxue Chuanganai , 13 ( 1 ) : 71 – 74 .
   Google Scholar
• Wang , Y. , Wang , K. M. , Liu , W. H. , Shen , G. L. and Yu , R. Q. 1997 . A new fluorescence optical‐fiber sensor for colchicine . Anal. Sci. , 13 ( 3 ) : 447 – 451 .
   Web of Science ®Google Scholar
• Yang , X. , Xie , J. W. , Shen , G. L. and Yu , R. Q. 2003 . An optical fibre sensor for colchicine using photo‐polymerized N‐vinylcarbazole . Microchimica Acta , 142 ( 4 ) : 225 – 230 .
   Web of Science ®Google Scholar
• Fang , R. B. and Zhang , S. H. 1999 . Supercritical fluid carbon dioxide extraction of colchicine from colchicum autumnale (Liliaceae) . Sepu , 17 ( 3 ) : 249 – 252 .
   Google Scholar