114
Views
8
CrossRef citations to date
0
Altmetric
Original Articles

Preparative Separation of Phenylpropanoid Glycoside from Scrophularia ningpoensis Hemsley by High Speed Countercurrent Chromatography and ESI-MSn Analysis

, , &
Pages 2322-2333 | Received 03 Feb 2009, Accepted 14 Apr 2009, Published online: 04 Sep 2009

REFERENCES

  • China Pharmacopoeia Committee . Pharmacopoeia of the People's Republic of China, First Div. , 2000 Ed. ; China Chemical Industry Press : Beijing , 2000 ; 88 .
  • Sagare , A.P. ; Kuo , C.L. ; Chueh , F.S. ; Tsay , H.S. De novo regeneration of Scrophularia yoshimurae Yamazaki (Scrophulariaceae) and quantitative analysis of harpagoside, an iridoid glucoside, formed in aerial and underground parts of in vitro propagated and wild plants by HPLC . Biol. Pharm. Bull. 2001 , 24 ( 11 ), 1311 – 1315 .
  • Zhang , D.J. ; Wang , R. ; Bi , K.S. The determination of the content of harpagoside and angoroside C in the Radix Scrophulariae by micellar electrokinetic capillary chromatography . Shenyang Yao Ke Da Xue Xue Bao. 2001 , 18 ( 3 ), 189 – 191 .
  • Li , Y.M. ; Jiang , S.H. ; Gao , W.Y. ; Zhu , D.Y. Phenylpropanoid glycosides from Scrophularia ningpoensis . Phytochemistry 2000 , 54 ( 8 ), 923 – 925 .
  • Liu , C.W. ; Bi , Z.M. ; Zhu , Y.F. ; Li , P. Simultaneous determination of four kinds of bioactive components in radix scrophulariae by HPLC . Zhongguo Yao Xue Za Zhi. 2007 , 42 ( 21 ), 1614 – 1616 .
  • Li , Y.M. ; Jiang , S.H. ; Gao , W.Y. ; Zhu , D.Y. Phenylpropanoid glycosides of Ningpo Figwort (Scrophularia ningpoensis) . Zhong Cao Yao. 1999 , 30 ( 7 ), 487 – 490 .
  • Zhang , W.J. ; Liu , Y.Q. ; Li , X.C. ; Pu , X.Y. ; Jin , Y.Q. ; Yang , C.R. Chemical constituents from scrophularia ningpoensis . Yunnan Zhi Wu Yan Jiu 1994, 16 (4), 407–412.
  • Lei , L. ; Yang , F.Q. ; Zhang , T.Y. ; Tu , P.F. ; Wu , L.J. ; Ito , Y. Preparative isolation and purification of acteoside and 2′-acetyl acteoside from Cistanches salsa (C.A . Mey.) G. Beck by high speed countercurrent chromatography. J. Chromatogr. A. 2001 , 912 ( 1 ), 181 – 185 .
  • Li , L. ; Tsao , R. ; Liu , Z.Q. ; Liu , S.Y. ; Yang , R. ; Young , J.C. ; Zhu , H.H. ; Deng , Z.Y. ; Xie , M.Y. ; Fu , Z.H. Isolation and purification of acteoside and isoacteoside from Plantago psyllium L . by high-speed countercurrent chromatography. J. Chromatogr. A. 2005 , 1063 ( 1–2 ), 161 – 169 .
  • Li , L. ; Tsao , R. ; Yang , R. ; Liu , C.M. ; Young , J.C. ; Zhu , H.H. Isolation and purification of phenylethanoid glycosides from Cistanche deserticola by high-speed countercurrent chromatography . Food Chem. 2008 , 108 ( 2 ), 702 – 710 .
  • Tong , S.Q. ; Yan , J.Z. ; Lou , J.Z. Preparative isolation and purification of harpagoside from Scrophularia ningpoensis Hemsley by high-speed countercurrent chromatography . Phytochem. Anal. 2006 , 17 ( 6 ), 406 – 408 .
  • Li , L. ; Liu , C.M. ; Liu , Z.Q. ; Lv , L. ; Liu , S.Y. Extraction and ESI/MSn studies of phenlethanoid glycosides in Cistanche deserticola . Zhipu Xue Bao 2006 , 27 ( 4 ), 232 – 236 .
  • Li , L. ; Liu , Z.Q. ; Liu , C.M. ; Tsao , R. ; Lv , L. ; Liu , S.Y. Studies on phenylethanoid glycosides in plant extract of Plantago asiatical by electrospray ionization multi-stage tandem mass spectrometry . Gaodeng Xuexiao Hua Xue Xue Bao. 2006 , 27 ( 8 ), 1430 – 1434 .
  • Wang , Y.M. ; Zhang , S.J. ; Luo , G.A. ; Hu , Y.N. ; Hu , J.P. ; Liu , L. ; Zhu , Y. ; Wang , H.J. Analysis of phenylethanoid glycosides in the extract of herba cistanchis by LC/ESI-MS/MS . Yao Xue Xue Bao. 2000 , 35 ( 11 ), 839 – 842 .
  • Ito , Y. Golden rules and pitfalls in selecting optimum conditions for high-speed countercurrent chromatography . J. Chromatogr. A. 2005 , 1065 ( 2 ), 145 – 168 .

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.