628
Views
3
CrossRef citations to date
0
Altmetric
Original Articles

DEVELOPMENT, COMPARISON, AND PEAK VALIDATION OF A HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY METHOD FOR DIRECT DETERMINATION OF GLUCOSAMINE HYDROCHLORIDE IN PHARMACEUTICAL FORMULATIONS

, , , , , & show all
Pages 2533-2547 | Published online: 01 Dec 2011

REFERENCES

  • Hauselmann , H. J. Nutripharmaceuticals for Osteoarthritis . Best Pract. Res. Clin. Rheumatol. 2001 , 15 , 595 – 607 .
  • Mankin , H. J. ; Brandt , K. D. ; Shulman , L. E. Workshop on Etiopathogenesis of Osteoarthritis. Proceedings and Recommendations . J. Rheumatol. 1986 , 13 , 1130 – 1160 .
  • Jordan , K. M. ; Arden , N. K. ; Doherty , M. ; Bannwarth , B. ; Bijlama , J. W. ; Dieppe , P. ; Gunther , K. ; Hauselmann , H. J. ; Herrero-Beaumont , G. ; Kaklamanis , P. ; Lohmander , S. ; Leeb , B. ; Lequesne , M. ; Mazieres , B. ; Martin-Mola , E. ; Pavelka , K. ; Pendleton , A. ; Punzi , L. ; Serni , U. ; Swoboda , B. ; Verbruggen , G. ; Zimmerman-Gorska , I. ; Dougados , M. EULAR Recommendations 2003: An Evidence Based Approach to the Management of Knee Osteoarthritis: Report of a Task Force of the Standing Committee for International Clinical Studies Including Therapeutic Trials (ESCISIT) . Ann. Rheum. Dis. 2003 , 62 , 1145 – 1155 .
  • Chinese Pharmacopoeia, Vol. II; China Medico-Pharmaceutical Science & Technology Publishing House: Beijing , 2010 .
  • WS1-XG-028-2001 . Quality Standard for Glucosamine Hydrochloride Raw Materials , China State Food and Drug Administration : Beijing , 2001 .
  • WS1-(X-090)-2005Z . Quality Standard for Glucosamine Hydrochloride Capsules , China State Food and Drug Administration : Beijing , 2005 .
  • Elson , L. A. ; Morgan , W. T. J. A Colorimetric Method for the Determination of Glucosamine and Chondrosamine . Biochem. J. 1933 , 27 , 1824 – 1828 .
  • Yamaguchi , T. ; Inoue , M. ; Miyachi , K. ; Tominaga , H. ; Fujita , Y. Spectrophotometric Determination of Glucosamine and Its Analogous Amino Sugars with o-hydroxyhydroquinonephthalein and Palladium (II) . Anal. Sci. 2004 , 20 , 387 – 389 .
  • Gaonkar , P. ; Khanvilkar , V. ; Shettigar , R. ; Gadgoli , C. Spectrophotometric Method for Determination of Glucosamine in Tablets . Indian J. Pharm. Sci. 2006 , 68 , 83 – 84 .
  • Wu , Y. ; Hussain , M. ; Fassihi , R. Development of a Simple Analytical Methodology for Determination of Glucosamine Release from Modified Release Matrix Tablets . J. Pham. Biomed. Anal. 2005 , 38 , 263 – 269 .
  • Qi , L. ; Zhang , S. ; Zuo , M. ; Chen , Y. Capillary Eletrophoretic Determination of Glucosamine in Osteoarthritis Tablets via Microwave-Accelerated Dansylation . J. Pham. Biomed. Anal. 2006 , 41 , 1620 – 1624 .
  • Volpi , N. Capillary Eletrophoresis Determination of Glucosamine in Nutraceutical Formulations After Labeling with Anthranilic Acid and UV Detection . J. Pham. Biomed. Anal. 2009 , 49 , 868 – 871 .
  • Eater , V. ; Angenot , L. ; Brandt , V. ; Frederich , M. ; Tits , M. ; Nerum , C. V. ; Wauters , J.-N. ; Hubert , P. Validation of a High-Performance Thin-Layer Chromatography/Densitometry Method for the Quantitative Determination of Glucosamine of Glucosamine in a Herbal Dietary Supplement . J. Chromatogr. A. 2006 , 1112 , 156 – 164 .
  • Nemati , M. ; Valizadeh , H. ; Ansarin , M. ; Ghaderi , F. Development of a Simple and Sensitive High-Performance Liquid Chromatography Method for Determination of Glucosamine in Pharmaceutical Formulations . J. AOAC Int. 2007 , 90 , 354 – 357 .
  • Liang , Z. ; Leslie , J. ; Abimbowale , A. ; Ashraf , M. ; Eddington , N. D. Determination of the Nutraceutical, Glucosamine Hydrochloride, in Raw Materials, Dosage Forms and Plasma Using Pre-Column Derivatization with Ultraviolet HPLC . J. Pham. Biomed. Anal. 1999 , 20 , 807 – 814 .
  • Zhou , J. Z. ; Waszkuc , T. ; Mohammed , F. Single Laboratory Validation of a Method for Determination of Glucosamine in Raw Materials and Dietary Supplements Containing Glucosamine Sulfate and/or Glucosamine Hydrochloride by High-Performance Liquid Chromatography with FMOC-Su Derivatization . J. AOAC Int. 2004 , 87 , 1083 – 1092 .
  • Zhou , J. Z. ; Waszkuc , T. ; Mohammed , F. Determination of Glucosamine in Raw Materials and Dietary Supplements Containing Glucosamine Sulfate and/or Glucosamine Hydrochloride by High-Performance Liquid Chromatography with FMOC-Su Derivatization: Collaborative Study . J. AOAC Int. 2005 , 88 , 1048 – 1058 .
  • Shao , Y. ; Alluri , R. ; Mummert , M. ; Koetter , U. ; Lech , S. A Stability-Indicating HPLC Method for the Determination of Glucosamine in Pharmaceutical Formulations. J. Pham. Biomed. Anal. 2004 , 35 , 625 – 631 .
  • Jac , P. ; Los , P. ; Spacil , Z. ; Pospisilova , M. ; Polasek , M. Fast Assay of Glucosamine in Pharmaceuticals and Nutraceuticals by Capillary Zone Eletrophoresis with Contactless Conductivity Detection. Electrophoresis. 2008, 29, 3511–3518.
  • USP32-NF27 . United States Pharmacopeial Convention Inc. : Rockville , MD , 2009 ; pp. 1029 – 1031 .
  • Zeng , M. ; Li , J. ; Wang , Y. ; Wang , L. Discussion on Assay Method of D-glucosamine Sulfate Potassium Chloride . Chin. JMAP 2008 , 25 , 251 – 254 .
  • ICH-Q2A. Text on Validation of Analytical Procedures. March 1995 .
  • ICH-Q2B. Validation of Analytical Procedures: Methodology. November 1996 .
  • European Pharmacopoeia. 5th ed.; Council of Europe: Strasbourg, France; 2005, pp. 69–72 .
  • Center for Drug Evaluation and Research, U.S. Food and Drug Administration . Reviewer Guidance. Validation of Chromatographic Methods , FDA : Rockville , MD , November 1994 .

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.