Structural and chemical imaging analysis of bitumen

References

• ASTM D. (2007). Standard test method for characteristic groups in rubber extender and proceeding oils and other petroleum-derived oils by the clay-gel absorption chromatographic method.
   Google Scholar
• ASTM D. (4124). Standard test methods for separation of asphalt into four fractions.
   Google Scholar
• Bearsley, S., Forbes, A., & Haverkamp, R. G. (2004). Direct observation of the asphaltene structure in paving-grade bitumen using confocal laser-scanning microscopy. Journal of Microscopy, 215, 149–155. doi: 10.1111/j.0022-2720.2004.01373.x
   PubMed Web of Science ®Google Scholar
• Benninghoven, A. (1994). Surface analysis by secondary ion mass spectrometry (SIMS). Surface Science, 299/300, 246–260. doi: 10.1016/0039-6028(94)90658-0
   Web of Science ®Google Scholar
• Bensebaa, F., Kotlyar, L., Pleizier, G., Sparks, B., Deslandes, Y., & Chung, K. (2000). Surface chemistry of end cuts from Athabasca bitumen. Surface and Interface Analysis, 30, 207–211. doi: 10.1002/1096-9918(200008)30:1<207::AID-SIA816>3.0.CO;2-5
   Web of Science ®Google Scholar
• Blom, J., Soenen, H., Katsiki, A., Van den Brande, N., Rahier, H., & van den Bergh, W. (2018). Investigation of the bulk and surface microstructure of bitumen by atomic force microscopy. Construction and Building Materials, 177, 158–169. doi: 10.1016/j.conbuildmat.2018.05.062
   Web of Science ®Google Scholar
• Boduszynski, M. M., McKay, J. F., & Latham, D. R. (1980). Asphaltenes where are you? Proceedings of the Association of Asphalt Paving Technologists, 49, 123–143.
   Google Scholar
• Branthaver, J. F., Petersen, J. C., Robertson, R. E., Duvall, J. J., Kim, S. S., Harnsberger, P. M., … Schabron, J. F. (1993). Binder characterization and evaluation, Vol. 2: Chemistry. SHRP-A-368. Washington, DC: National Research Council.
   Google Scholar
• Carbognani, L., DeLima, L., Orea, M., & Ehrmann, U. (2000). Studies of large crude oil alkanes. II. Isolation and characterization of aromatic waxes and waxy asphaltenes. Petroleum Science and Technology, 18, 607–634. doi: 10.1080/10916460008949863
   Web of Science ®Google Scholar
• Claudy, P., Letoffe, J. M., King, G. N., & Planche, J. P. (1992). Characterization of asphalt cements by thermomicroscopy and differential scanning calorimetry: Correlation to classic physical properties. Fuel Science and Technology International, 10, 735–765. doi: 10.1080/08843759208916019
   Google Scholar
• Das, P. K., Kringos, N., Wallqvist, V., & Birgisson, B. (2013). Micro-mechanical investigation of phase separation in bitumen by combining atomic force microscopy with differential scanning calorimetry results. Road Materials and Pavement Design, 14, 25–37. doi: 10.1080/14680629.2013.774744
   Web of Science ®Google Scholar
• Donnet, J. B., Ducret, J., Kennel, M., & Papirer, E. (1977). Electron microscopic observations of the morphology of bitumens. Fuel, 56, 97–100. doi: 10.1016/0016-2361(77)90049-7
   Web of Science ®Google Scholar
• Eberhardsteinera, L., Fussl, J., Hofko, B., Handle, F., Hospodka, M., Blab, R., & Grothe, H. (2015). Towards a microstructural model of bitumen ageing behavior. International Journal of Pavement Engineering, 16, 939–949. doi: 10.1080/10298436.2014.993192
   Web of Science ®Google Scholar
• Fischer, H. R., & Cernescu, A. (2015). Relation of chemical composition to asphalt microstructure – Details and properties of micro-structures in bitumen as seen by thermal and friction force microscopy and by scanning near-field optical microscopy. Fuel, 153, 628–633. doi: 10.1016/j.fuel.2015.03.043
   Web of Science ®Google Scholar
• Gaskin, J. (2013). On bitumen microstructure and the effects of crack healing (Ph. D thesis). University of Nottingham, UK.
   Google Scholar
• Handle, F., Fussl, J., Neudl, S., Grossegger, D., Eberhardsteiner, L., Hofko, B., … Grothe, H. (2016). The bitumen microstructure: A fluorescent approach. Materials and Structures, 49, 167–180. doi: 10.1617/s11527-014-0484-3
   Web of Science ®Google Scholar
• Hofko, B., Cannone Falchetto, A., Grenfell, J., Huber, L., Lu, X., Porot, L., … You, Z. (2017). Effect of short-term ageing temperature on bitumen properties. Road Materials and Pavement Design, 18, 108–117. doi: 10.1080/14680629.2017.1304268
   Web of Science ®Google Scholar
• Hung, A. M., & Fini, E. H. (2015). AFM study of asphalt binder “bee” structures: Origin, mechanical fracture, topological evolution, and experimental artifacts. RSC Advances, 5, 96972–96982. doi: 10.1039/C5RA13982A
   Web of Science ®Google Scholar
• Jäger, A., Lackner, R., Eisenmenger-Sittner, C., & Blab, R. (2004). Identification of four material phases in bitumen by atomic force microscopy. Road Materials and Pavement Design, 5, 9–24. doi: 10.1080/14680629.2004.9689985
   Google Scholar
• Keller, B. A., & Hug, P. (1999). Time-of-fight secondary ion mass spectrometry of industrial materials. Analytica Chimica Acta, 393, 201–212. doi: 10.1016/S0003-2670(99)00017-3
   Web of Science ®Google Scholar
• Loeber, L., Muller, G., Morel, J., & Sutton, O. (1998). Bitumen in colloid science: A chemical, structural and rheological approach. Fuel, 77, 1443–1450. doi: 10.1016/S0016-2361(98)00054-4
   Web of Science ®Google Scholar
• Loeber, L., Sutton, O., Morel, J., Valleton, J. M., & Muller, G. (1996). New direct observations of asphalts and asphalt binders by scanning electron microscopy and atomic force microscopy. Journal of Microscopy, 182, 32–39. doi: 10.1046/j.1365-2818.1996.134416.x
   Web of Science ®Google Scholar
• Lu, X., Langton, M., Olofsson, P., & Redelius, P. (2005). Wax morphology in bitumen. Journal of Materials Science, 40, 1893–1900. doi: 10.1007/s10853-005-1208-4
   Web of Science ®Google Scholar
• Lu, X., & Redelius, P. (2006). Compositional and structural characterization of waxes isolated from bitumens. Fuel, 20, 653–660. doi: 10.1021/ef0503414
   Web of Science ®Google Scholar
• Lu, X., Sjövall, P., & Soenen, H. (2017). Structural and chemical analysis of bitumen using time-of-flight secondary ion mass spectrometry (TOF-SIMS). Fuel, 199, 206–218. doi: 10.1016/j.fuel.2017.02.090
   Web of Science ®Google Scholar
• Lu, X., Sjövall, P., Soenen, H., & Andersson, M. (2018). Microstructures of bitumen observed by environmental scanning electron microscopy (ESEM) and chemical analysis using time-of-flight secondary ion mass spectrometry (TOF-SIMS). Fuel, 229, 198–208. doi: 10.1016/j.fuel.2018.05.036
   Web of Science ®Google Scholar
• Lyne, Å. L., Wallqvist, V., Rutland, M. W., Claesson, P., & Birgisson, B. (2013). Surface wrinkling: The phenomenon causing bees in bitumen. Journal of Materials Science, 48, 6970–6976. doi: 10.1007/s10853-013-7505-4
   Web of Science ®Google Scholar
• Masson, J. F., Leblond, V., & Margeson, J. (2006). Bitumen morphologies by phase-detection atomic force microscopy. Journal of Microscopy, 221, 17–29. doi: 10.1111/j.1365-2818.2006.01540.x
   PubMed Web of Science ®Google Scholar
• McKay, J. F., Branthaver, J. F., & Robertson, R. E. (1995). Isolation of waxes from asphalts and the influence of waxes on asphalt rheological properties. Preprints, division of petroleum chemistry. ACS 210th National Meeting, Chicago, IL, August 20–25, 1995. p. 794–8.
   Google Scholar
• Michon, L. C., Williams, T. M., Miknis, F. P., Planche, J. P., & Martin, D. (1998). Use of the environmental scanning electron microscope to investigate three polymer modified asphalts. Petroleum Science and Technology, 16, 797–809. doi: 10.1080/10916469808949812
   Web of Science ®Google Scholar
• Mikhailenko, P., Kadhim, H., & Baaj, H. (2017). Observation of bitumen microstructure oxidation and blending with ESEM. Road Materials and Pavement Design, 18(Sup 2), 216–225. doi: 10.1080/14680629.2017.1304251
   Google Scholar
• Mikhailenko, P., Kou, C., Baaj, H., Poulikakos, L., Cannone-Falchetto, A., Besamusca, J., & Hofko, B. (2019). Comparison of ESEM and physical properties of virgin and laboratory aged asphalt binders. Fuel, 235, 627–638. doi: 10.1016/j.fuel.2018.08.052
   Web of Science ®Google Scholar
• Mullins, O. C. (2010). The modified Yen model. Energy & Fuels, 24, 2179–2207. doi: 10.1021/ef900975e
   Web of Science ®Google Scholar
• Mullins, O. C., Sheu, E. Y., Mammami, A., & Marshall, A. G. (2007). Asphaltenes, heavy oils, and petroleomics. New York: Springer.
   Google Scholar
• Nellensteyn, F. J. (1924). The constitution of asphalt. Journal of the Institute of Petroleum Technology, 10, 311–325.
   Google Scholar
• Pahlavan, F., Mousavi, M., Hung, A., & Fini, E. H. (2016). Investigating molecular interactions and surface morphology of wax-doped asphaltenes. Journal of Physical Chemistry, 18(13), 8840–8854.
   Google Scholar
• Pauli, A. T., Branthaver, J. F., Robertson, R. E., Grimes, W., & Eggleston, C. M. (2001). Atomic force microscopy investigation of SHRP asphalts. ACS Div. Fuel Chem., 46(2), 104–110.
   Google Scholar
• Pauli, T., Grimes, W., Cookman, A., & Huang, S.-C. (2014). Adherence energy of asphalt thin films measured by force-displacement atomic force microscopy. Journal of Materials in Civil Engineering, 26(12), 04014089. doi: 10.1061/(ASCE)MT.1943-5533.0001003
   Web of Science ®Google Scholar
• Petersen, J. C., Robertson, R. E., Branthaver, J. F., Harnsberger, P. M., Duvall, J. J., Kim, S. S., … Bahia, H. U. (1994). Binder characterization and evaluation, Vol. 1. SHRP-A-367. Washington, DC: National Research Council.
   Google Scholar
• Pfeiffer, J. P., & Saal, R. N. J. (1940). Asphaltic bitumen as colloidal system. Journal of Physical Chemistry, 44, 139–149. doi: 10.1021/j150398a001
   Google Scholar
• Redelius, P. G. (2000). Solubility parameters and bitumen. Fuel, 79, 27–35. doi: 10.1016/S0016-2361(99)00103-9
   Web of Science ®Google Scholar
• Redelius, P., Lu, X., & Isacsson, U. (2002). Non-classical wax in bitumen. Road Materials and Pavement Design, 3, 7–21. doi: 10.1080/14680629.2002.9689913
   Google Scholar
• Rozeveld, S. J., Shin, E. E., Bhurke, A., France, L., & Drzal, L. T. (1997). Network morphology of straight and polymer modified asphalt cements. Microscopy Research Technique, 38, 529–543. doi: 10.1002/(SICI)1097-0029(19970901)38:5<529::AID-JEMT11>3.0.CO;2-O
   PubMed Web of Science ®Google Scholar
• Schmets, A., Kringos, N., Pauli, T., Redelius, P., & Scarpas, T. (2010). On the existence of wax-induced phase separation in bitumen. International Journal of Pavement Engineering, 11, 555–563. doi: 10.1080/10298436.2010.488730
   Web of Science ®Google Scholar
• Schuler, B., Meyer, G., Pena, D., Mullins, O. C., & Gross, L. (2015). Unraveling the molecular structures of asphaltenes by atomic force microscopy. Journal of American Chemistry Society, 137(31), 9870–9876. doi: 10.1021/jacs.5b04056
   PubMed Web of Science ®Google Scholar
• Sjövall, P., Pomerantz, A. E., Lu, X., & Mullins, O. C. (2018). Time of flight-secondary ion mass spectrometry (TOF-SIMS) study of diverse asphaltenes. Fuel, 220, 638–644. doi: 10.1016/j.fuel.2018.02.017
   Web of Science ®Google Scholar
• Sodhi, R. N. S. (2004). Time-of-flight secondary ion mass spectrometry (TOF-SIMS): Versatility in chemical and imaging surface analysis. The Analyst, 129, 483–487. doi: 10.1039/B402607C
   PubMed Web of Science ®Google Scholar
• Soenen, H., Besamusca, J., Fischer, H. R., Poulikakos, L. D., Planche, J. P., Das, P. K., … Chailleux, E. (2014). Laboratory investigation of bitumen based on round robin. DSC and AFM tests. Materials and Structures, 47, 1205–1220. doi: 10.1617/s11527-013-0123-4
   Web of Science ®Google Scholar
• Stangl, K., Jager, A., & Lackner, R. (2006). Microstructure-based identification of bitumen performance. Road Materials and Pavement Design, 7(special issue), 111–142. doi: 10.1080/14680629.2006.9690061
   Google Scholar
• Stokes, D. J. (2008). Principles and practice of variable pressure/environmental scanning electron microscopy (VP-ESEM). West Sussex, UK: John Wiley & Sons Ltd.
   Google Scholar
• Thiel, V., & Sjövall, P. (2015). Time-of-flight secondary ion mass spectrometry (TOF-SIMS): Principles and practice in the biogeosciences. In K. Grice (Ed.), Principles and practice of analytical techniques in geosciences (pp. 122–170). London: RSC Detection Science Series No.4. published by the Royal Society of Chemistry.
   Google Scholar
• Wang, Y., & Zhao, K. (2016). Different forms of asphaltene microstructures discovered in transmission electron microscopy. Journal of Materials in Civil Engineering, 28(11), 04016137. doi: 10.1061/(ASCE)MT.1943-5533.0001660
   Web of Science ®Google Scholar
• Yen, T. F. (1961). Investigation of the structure of petroleum asphaltenes by X-ray Diffraction. Analytical Chemistry, 33, 1587–1594. doi: 10.1021/ac60179a039
   Web of Science ®Google Scholar
• Yen, T. F., & Chilingarian, G. V. (1994). Developments in petroleum science 40A: Asphaltenes and asphalts, 1. Amsterdam: Elsevier Science.
   Google Scholar
• Yu, X., Granados-Focil, S., Tao, M., & Burnham, N. A. (2018). Time and composition-dependent evolution of distinctive microstructures in bitumen. Energy & Fuels, 32, 67–80. doi: 10.1021/acs.energyfuels.7b02467
   Web of Science ®Google Scholar