Multi-residue method for detecting coccidiostats at carry-over level in feed by HPLC–MS/MS

References

• Belgian Federal Agency for the Safety of the Food Chain. 2008. Estimating measurement uncertainty in quantitative chemical analysis. Available at: http://www.favv-afsca.fgov.be/laboratories/approvedlaboratories/officecircular/_documents/03-11-2008-procedureENLAB-P-508-Measurement-uncertainty-v.01_en.pdf
   Google Scholar
• BEMEFA/APFACA 2008. Rapport annuel 2008 de l’APFACA, Belgium. p 50.
   Google Scholar
• Bertelsen , U , Dorne , JL , Fernández-Cruz , ML , Renshaw , DW , Peltonen , K , Anadón , A , Feil , A , Sanders , P , Wester , PW and Fink-Gremmels , J . 2008 . Risk assessment of coccidiostats after cross-contamination of feed: Implications for animal and human health . Toxicol Lett , 180 ( 1 ) : S61
   Google Scholar
• Commission Decision 2002/657/EC concerning the performance of analytical methods and the interpretation of results.
   Google Scholar
• Commission Directive 2009/8/EC amending Annex I to Directive 2002/32/EC of the European Parliament and of the Council as regards maximum levels of unavoidable carry-over of coccidiostats or histomonostats in nontarget feed.
   Google Scholar
• Commission Regulation 1999/2430/EC linking the authorisation of certain additives belonging to the group of coccidiostats and other medicinal substances in feedingstuffs to persons responsible for putting them into circulation.
   Google Scholar
• Commission Regulation 2002/1041/EC concerning the provisional authorisation of a new additive in feedingstuffs.
   Google Scholar
• Commission Regulation 2003/1831/EC of the European Parliament and of the council on additives for use in animal nutrition.
   Google Scholar
• Commission Regulation 2004/1289/EC concerning the authorisation for 10 years of the additive Deccox® in feedingstuffs, belonging to the group of coccidiostats and other medicinal substances.
   Google Scholar
• Commission Regulation 2004/1455/EC concerning the authorisation for 10 years of the additive “Avatec 15%” in feedingstuffs, belonging to the group of coccidiostats and other medicinal substances.
   Google Scholar
• Commission Regulation 2004/1464/EC concerning the authorisation for 10 years of the additive “Monteban” in feedingstuffs, belonging to the group of coccidiostats and other medicinal substances.
   Google Scholar
• Commission Regulation 2004/1800/EC concerning the authorisation for 10 years of the additive Cycostat 66G in feedingstuffs, belonging to the group of coccidiostats and other medicinal substances.
   Google Scholar
• Commission Regulation 2005/183/EC of the European Parliament and of the council laying down requirements for feed hygiene.
   Google Scholar
• Commission Regulation 2009/152/EC laying down the methods of sampling and analysis for the official control of feed.
   Google Scholar
• Daeseleire , E , Mortier , L , Delahaut , P and Huyghebaert , G . 2006 . Determination of concentration levels of anticoccidials in eggs due to the presence of low levels of those compounds in feed for laying hens caused by carry-over at the feeding mill . Accred Qual Assur J Qual Comp Reliab Chem Measur , 11 ( 1–2 ) : 44 – 48 .
   Google Scholar
• de Jong , J , Tomassen , M , Driessen , J , Keukens , H , Putzka , H-A and Brambilla , G . 2004 . Liquid chromatographic method for nicarbazin in broiler feeds and premixtures: Development, validation, and interlaboratory study . J AOAC Int , 87 ( 6 ) : 1269 – 1277 .
   Google Scholar
• Dubois , M , Pierret , G and Delahaut , P . 2004 . Efficient and sensitive detection of residues of nine coccidiostats in egg and muscle by liquid chromatography–electrospray tandem mass spectrometry . J Chromatogr B , 813 : 181 – 189 .
   Google Scholar
• Fodey , TL , Delahaut , P and Elliott , CT . 2007 . Use of antigen mimics to produce specific antibodies to anti-coccidial drugs . J Immunol Methods , 323 ( 1 ) : 31 – 38 .
   Google Scholar
• Huet , A-C , Mortier , L , Daeseleire , E , Fodey , T , Elliott , C and Delahaut , P . 2005 . Screening for the coccidiostats halofuginone and nicarbazin in egg and chicken muscle: development of an ELISA . Food Addit Contam , 22 ( 2 ) : 128 – 134 .
   Google Scholar
• Mortier , L , Daeseleire , E and Delahaut , P . 2003 . Simultaneous detection of five coccidiostats in eggs by liquid chromatography–tandem mass spectrometry . Anal Chim Acta , 483 ( 1/2 ) : 27 – 37 .
   Google Scholar
• Mortier , L , Daeseleire , E and Van Peteghem , C . 2005 . Liquid chromatographic tandem mass spectrometric determination of five coccidiostats in poultry eggs and feed . J Chromatogr B , 820 : 261 – 270 .
   Google Scholar
• Sanchez , AA and Campbell , HM . 2008 . Determination of decoquinate in animal feeds by liquid chromatography: Collaborative study . J AOAC Int , 91 ( 4 ) : 685 – 693 .
   Google Scholar
• Thalmann , A , Wagner , K , Tomassen , M , Driessen , J and de Jong , J . 2004 . Liquid chromatographic method to determine narasin in feedingstuffs and premixtures: Development, validation, and interlaboratory study . J AOAC Int , 87 ( 6 ) : 1278 – 1286 .
   Google Scholar
• Turnipseed , SB , Roybal , JE , Pfenning , AP , Gonzales , SA , Hurlbut , JA and Madson , MR . 2001 . LC/MS confirmation of ionophores in animal feeds . J AOAC Int , 84 ( 3 ) : 640 – 647 .
   Google Scholar
• Vincent , U , Chedin , M , Yasar , S and von Holst , C . 2008 . Determination of ionophore coccidiostats in feedingstuffs by liquid chromatography–tandem mass spectrometry: Part I . Application to targeted feed. J Pharm Biomed Anal , 47 ( 4/5 ) : 750 – 757 .
   Google Scholar
• Yamada , R , Kozono , M , Ohmori , T , Morimatsu , F and Kitayama , M . 2005 . Simultaneous determination of residual veterinary drugs in bovine, porcine, and chicken muscle using liquid chromatography coupled with electrospray ionization tandem mass spectrometry . Biosci Biotechnol Biochem , 70 ( 1 ) : 54 – 65 .
   Google Scholar