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Original Articles

Rapid multi-class multi-residue method for the confirmation of chloramphenicol and eleven nitroimidazoles in milk and honey by liquid chromatography-tandem mass spectrometry (LC-MS)

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Pages 1233-1246 | Received 17 Feb 2010, Accepted 25 Apr 2010, Published online: 30 Jun 2010

References

  • Aerts , R , Egberink , I , Kan , C , Keukens , H and Beek , W . 1991 . Liquid-chromatographic multicomponent method for determination of residues of ipronidazole, ronidazole, and dimetridazole and some relevant metabolites in eggs, plasma, and feces and its use in depletion studies in laying hens . J AOAC Int , 74 : 46 – 55 .
  • AOAC International . 2003 . Official methods of analysis (2003), , 17th , Gaithersburg (MD) : AOAC International. Method 995.10 .
  • Boyd , B , Bjork , H , Billing , J , Shimelis , O , Axelsson , S , Leonora , M and Yilmaz , E . 2007 . Development of an improved method for trace analysis of chloramphenicol using molecularly imprinted polymers . J Chromatogr A , 1174 : 63 – 71 .
  • Committee for Veterinary Medicinal Products, The European Agency for the Evaluation of Medical Products, Veterinary Medicines Evaluation Unit. 1997. Summary reports. EMEA/MRL/173/96-Final, July 1997. Available from: http://www.ema.europa.eu/pdfs/vet/mrls/017396en.pdf/
  • Cronly , M , Behan , P , Foley , B , Malone , E and Regan , L . 2009 . Development and validation of a rapid method for the determination and confirmation of 10 nitroimidazoles in animal plasma using liquid chromatography tandem mass spectrometry . J Chromatogr B , 877 : 1494 – 1500 .
  • Cronly , M , Behan , P , Foley , B , Malone , E and Regan , L . 2009 . Rapid confirmatory method for the determination of eleven nitroimidazoles in egg using liquid chromatography tandem mass spectrometry . J Chromatogr A , 1216 : 8101 – 8109 .
  • Daeseleire , E , De Ruyck , H and Van Renterghem , R . 2000 . Rapid confirmatory assay for the simultaneous detection of ronidazole, metronidazole and dimetridazole in eggs using liquid chromatography-tandem mass spectrometry . Analyst , 125 : 1533 – 1535 .
  • European Commission . 1990 . Establishment of MRLs of veterinary medical products in foodstuffs of animal origin. Council Regulation (EEC) no. 2377/90. . Off J Eur Comm , : L224:1 – 8 .
  • European Commission . 2002 . Commission Decision of 12 August (2002) implementing Council Directive 96/23/EC concerning the performance of analytical methods and interpretation of results . Off J Eur Comm , L221 : 8 – 36 .
  • European Commission. 2008. SANCO/2004/2726-rev 4–December 2008. Available from: http://ec.europa.eu/food/food/chemicalsafety/residues/cons_2004-2726rev4_en.pdf/
  • Fraselle , S , Derop , V , Degroodt , JM and Van Loco , J . 2007 . Validation of a method for the detection and confirmation of nitroimidazoles and the corresponding hydroxy metabolites in pig plasma by high performance liquid chromatography-tandem mass spectrometry . Anal Chim Acta , 586 : 383 – 393 .
  • International Agency for Research on Cancer (IARC). 1987. Monographs on the Evaluation of Carcinogenic Risks to Humans. Overall evaluations of carcinogenicity. Supplement 7, p. 250. Lyon (France): IARC.
  • International Organization for Standardization (ISO). 2008. ISO 11843-5:2008. Capability of detection–Part 5: methodology in the linear and non-linear calibration cases.
  • Lopez , MI , Pettis , JS , Barton-Smith , I and Pak-Sin , C . 2008 . Multiclass determination and confirmation of antibiotic residues in honey using LC-MS/MS . J Agric Food Chem , 56 : 1553 – 1559 .
  • Mohamed , R , Mottier , P , Treguier , L , Richoz-Payot , J , Yilmaz , E , Tabet , JC and Guy , PAJ . 2008 . Use of molecularly imprinted solid-phase extraction sorbent for the determination of four 5-nitroimidazoles and three of their metabolites from egg-based samples before tandem LC-ESIMS/MS analysis . J Agric Food Chem , 56 : 3500 – 3508 .
  • Mol , HGJ , Plaza-Bolaos , P , Zomer , P , De Rijk , TC , Stolker , AAM and Mulder , PPJ . 2008 . Toward a generic extraction method for simultaneous determination of pesticides, mycotoxins, plant toxins, and veterinary drugs in feed and food matrixes . Anal Chem , 80 : 9450 – 9459 .
  • Mottier , P , Huré , I , Gremaud , E and Guy , PA . 2006 . Analysis of four 5-nitroimidazoles and their corresponding hydroxylated metabolites in egg, processed egg, and chicken meat by isotope dilution liquid chromatography tandem mass spectrometry . J Agric Food Chem , 54 : 2018 – 2026 .
  • Ortelli , D , Cognard , E , Jan , P and Edder , P . 2009 . Comprehensive fast multiresidue screening of 150 veterinary drugs in milk by ultra-performance liquid chromatography coupled to time of flight mass spectrometry . J Chromatogr B , 877 : 2363 – 2374 .
  • Polzer , J and Gowik , P . 2005 . Nitroimidazoles in turkey muscle–the influence of sampling conditions on measurement results in residue control . Anal Chim Acta , 529 : 299 – 303 .
  • Polzer , J , Stachel , C and Gowik , P . 2004 . Treatment of turkeys with nitroimidazoles . Impact of the selection of target analytes and matrices on an effective residue control. Anal Chim Acta , 521 : 189 – 200 .
  • Rejtharova , M and Rejthar , L . 2009 . Determination of chloramphenicol in urine, feed water, milk and honey samples using molecular imprinted polymer clean-up . J Chromatogr A , 1216 : 8246 – 8253 .
  • Ronning , HT , Einarsen , K and Asp , TN . 2006 . Determination of chloramphenicol residues in meat, seafood, egg, honey, milk, plasma and urine with liquid chromatography-tandem mass spectrometry, and the validation of the method based on (2002)/657/EC . J Chromatogr A , 1118 : 226 – 233 .
  • Shen , JZ , Xia , X , Jiang , HY , Li , C , Li , JC , Li , XW and Ding , SY . 2009 . Determination of chloramphenicol, thiamphenicol, florfenicol, and florfenicol amine in poultry and porcine muscle and liver by gas chromatography-negative chemical ionization mass spectrometry . J Chromatogr B , 877 : 1523 – 1529 .
  • Sheridan , R , Policastro , B , Thomas , S and Rice , D . 2008 . Analysis and occurrence of 14 sulfonamide antibacterials and chloramphenicol in honey by solid-phase extraction followed by LC/MS/MS analysis . J Agric Food Chem , 56 : 3509 – 3516 .
  • Stolker , AA , Rutgers , P , Oosterink , E , Lasaroms , JJ , Peters , RJ , Van Rhijn , JA and Nielen , MW . 2008 . Comprehensive screening and quantification of veterinary drugs in milk using UPLC-ToF-MS . Anal Bioanal Chem , 391 : 2309 – 2322 .
  • Joint FAO/WHO Expert Committee on Food Additives (JECFA) . 1989 . Thirty-fourth Report of the Joint FAO/WHO Expert Committee on Food Additives. Evaluation of certain veterinary drug residues in food , Geneva, , Switzerland : World Health Organisation (WHO) .
  • Thompson , CS , Traynor , IM , Fodey , TL and Crooks , SRH . 2009 . Improved screening method for the detection of a range of nitroimidazoles in various matrices by optical biosensor . Anal Chim Acta , 657 : 259 – 264 .
  • Xia , X , Li , X , Shen , J , Zhang , S , Ding , S and Jiang , H . 2006 . Determination of four nitroimidazoles in poultry, swine muscle and eggs by liquid chromatography/tandem mass spectrometry . J AOAC Int , 89 : 94 – 99 .
  • Zhang , SX , Liu , ZW , Guo , X , Cheng , LL , Wang , ZH and Shen , JZ . 2008 . Simultaneous determination and confirmation of chloramphenicol, thiamphenicol, florfenicol and florfenicol amine in chicken muscle by liquid chromatography-tandem mass spectrometry . J Chromatogr B , 875 : 399 – 404 .
  • Zhou , J , Shen , J , Xue , X , Zhao , J , Li , Y , Zhang , J and Zhang , S . 2007 . Simultaneous determination of nitroimidazole residues in honey samples by high-performance liquid chromatography with ultraviolet detection . J AOAC Int , 90 : 872 – 878 .

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