379
Views
16
CrossRef citations to date
0
Altmetric
Original Articles

Simultaneous determination of lincomycin and spectinomycin residues in animal tissues by gas chromatography-nitrogen phosphorus detection and gas chromatography-mass spectrometry with accelerated solvent extraction

, , , , , , & show all
Pages 145-154 | Received 13 Sep 2010, Accepted 01 Nov 2010, Published online: 15 Jan 2011

References

  • Aiello , SE . 1998 . The Merck veterinary manual, , 8th , 2032 – 2033 . Whitehouse Station, NJ : Merck. .
  • Bergwerff , AA , Scherpenisse , P and Haagsma , N . 1998 . HPLC determination of residues of spectinomycin in various tissue types from husbandry animals . Analyst , 123 ( 10 ) : 2139 – 2144 .
  • Berrada , H , Moltó , JC , Mañes , J and Font , G . 2010 . Determination of aminoglycoside and macrolide antibiotics in meat by pressurized liquid extraction and LC-ESI-MS . J Sep Sci , 33 ( 4–5 ) : 522 – 529 .
  • Burton , SD , Hutchins , JE , Fredericksen , TL , Ricks , C and Tyczkowski , JK . 1991 . High performance liquid chromatographic method for the determination of spectinomycin in turkey plasma . J Chromatogr , 571 ( 1–2 ) : 209 – 216 .
  • Carson , MC and Heller , DN . 1998 . Confirmation of spectinomycin in milk using ion-pair solid-phase extraction and liquid chromatography-electrospray ion trap mass spectrometry . J Chromatogr B: Biomed Sci Appl , 718 ( 1 ) : 95 – 102 .
  • European Commission . 2002a . Commission Decision of August (2002) implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results (2002/657/EC) . Off J Eur Comm , L221 : 8
  • European Commission . 2002b . Commission Regulation (EC) No. 1181/(2002) of 1 July (2002) . Off J Eur Comm , L172 : 13
  • Farrington , WH , Cass , SD , Patey , AL and Shearer , G . 1988 . A method for the analysis of lincomycin in porcine and bovine kidney . Food Addit Contam A , 5 ( 1 ) : 67 – 75 .
  • Haagsma , N , Keegstra , JR and Scherpenisse , P . 1993 . High-performance liquid chromatographic determination of spectinomycin in swine, calf and chicken plasma . J Chromatogr B: Biomed Sci Appl , 615 ( 2 ) : 289 – 295 .
  • Haagsma , N , Scherpenisse , P , Simmonds , RJ , Wood , SA and Rees , SA . 1995 . High-performance liquid chromatographic determination of spectinomycin in swine, calf and chicken plasma using post-column derivatization . J Chromatogr B: Biomed Sci Appl , 672 ( 1 ) : 165 – 171 .
  • Hamamoto , K , Mizuno , Y , Koike , R , Yamaoka , R , Takahashi , T and Takahashi , Y . 2003 . Residue analysis of spectinomycin in tissues of chicken and swine by HPLC . Shokuhin Eiseigaku Zasshi , 44 ( 2 ) : 114 – 118 .
  • Hornish , RE and Wiest , JR . 1998 . Quantitation of spectinomycin residues in bovine tissues by ion-exchange high-performance liquid chromatography with post-column derivatization and confirmation by reversed-phase high-performance liquid chromatography-atmospheric pressure chemical ionization tandem mass spectrometry . J Chromatogr A , 812 ( 1–2 ) : 123 – 133 .
  • Juan , C , Moltó , JC , Mañes , J and Font , G . 2010 . Determination of macrolide and lincosamide antibiotics by pressurised liquid extraction and liquid chromatography-tandem mass spectrometry in meat and milk . Food Contr. , 21 ( 12 ) : 1703 – 1709 .
  • Luo , W , Hansen , EB , Ang , CY and Thompson , HC . 1996 . Determination of lincomycin residue in salmon tissues by ion-pair reversed-phase liquid chromatography with electrochemical detection . J AOAC Int , 79 ( 4 ) : 839 – 843 .
  • McLaughlin , LG , Henion , JD and Kijak , PJ . 1994 . Multi-residue confirmation of aminoglycoside antibiotics and bovine kidney by ion spray high-performance liquid chromatography tandem mass spectrometry . Biolog Mass Spectrom , 23 ( 7 ) : 417 – 429 .
  • Moats , WA . 1991 . Determination of lincomycin in milk and tissues by reversed-phase liquid . Chromatogr J Agric Food Chem , 39 : 1812 – 1816 .
  • Murray L, editor. 1991. Physician's desk reference, 45th ed. Mont Vale (NJ): Medical Economies. p. 2260–2261.
  • Peru , KM , Kuchta , SL , Headley , JV and Cessna , AJ . 2006 . Development of a hydrophilic interaction chromatography-mass spectrometry assay for spectinomycin and lincomycin in liquid hog manure supernatant and run-off from cropland . J Chromatogr A , 1107 ( 1–2 ) : 152 – 158 .
  • Richter , BE , Jones , BA , Ezzel , JL , Porter , NL , Avdalovic , N and Pohl , C . 1996 . ASE: a technique for sample preparation . Analyt Chem , 68 : 1033 – 1039 .
  • Schermerhorn , PG , Chu , PS and Kijak , PJ . 1995 . Determination of spectinomycin residues in bovine milk using liquid chromatography with electrochemical detection . J Agricult Food Chem , 43 ( 8 ) : 2122 – 2125 .
  • Sin , DWM , Ho , C , Wong , YC and Ho , SK . 2004 . Simultaneous determination of lincomycin and virginiamycin M1 in swine muscle, liver and kidney by liquid chromatography and electrospray ionization tandem mass spectrometry . Analyt Chimica Acta , 517 ( 1–2 ) : 39 – 45 .
  • Sin , DWM , Wong , YC and Alec , CB . 2004 . Quantitative analysis of lincomycin in animal tissues and bovine milk by liquid chromatography electrospray ionization tandem mass spectrometry . J Pharm Biomed Anal , 34 ( 3 ) : 651 – 659 .
  • Szunyog , J , Adams , E and Liekens , K . 2002 . Analysis of a formulation containing lincomycin and spectinomycin by liquid chromatography with pulsed electrochemical detection . J Pharmaceut Biomed Anal , 29 : 213 – 220 .
  • Thompson , TS , Noot , DK , Calvert , J and Pernal , SF . 2003 . Determination of lincomycin and tylosin residues in honey using solid-phase extraction and liquid chromatography-atmospheric pressure chemical ionization mass spectrometry . J Chromatogr A , 1020 ( 2 ) : 241 – 250 .

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.