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Food Additives & Contaminants: Part A Volume 29, 2012 - Issue 4: Ministério da Agricultura, Pecuária e Abastecimento do Brasil – Laboratórios Nacionais Agropecuários: Methods of analysis for residues and contaminants in the food chain
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Original Articles

Optimisation and validation of a quantitative and confirmatory method for residues of macrolide antibiotics and lincomycin in kidney by liquid chromatography coupled to mass spectrometry

C.P. Rezende Ministry of Agriculture, Livestock and Food Suply – MAPA, Laboratório Nacional Agropecuário – LANAGRO/MG, BrazilCorrespondence[email protected]
,
L.F. Souza Ministry of Agriculture, Livestock and Food Suply – MAPA, Laboratório Nacional Agropecuário – LANAGRO/MG, Brazil
,
M.P. Almeida Ministry of Agriculture, Livestock and Food Suply – MAPA, Laboratório Nacional Agropecuário – LANAGRO/MG, Brazil
,
P.G. Dias Ministry of Agriculture, Livestock and Food Suply – MAPA, Laboratório Nacional Agropecuário – LANAGRO/MG, Brazil
,
M.H. Diniz Ministry of Agriculture, Livestock and Food Suply – MAPA, Laboratório Nacional Agropecuário – LANAGRO/MG, Brazil
&
J.C. Garcia Ministry of Agriculture, Livestock and Food Suply – MAPA, Laboratório Nacional Agropecuário – LANAGRO/MG, Brazil
Pages 587-595 | Received 22 Nov 2010, Accepted 16 Dec 2011, Published online: 09 Feb 2012

References

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  • Berrada , H , Borrull , F , Font , G , Moltó , JC and Marcé , RM . 2007 . Validation of a confirmatory method for the determination of macrolides in liver and kidney animal tissues in accordance with the European Union regulation 2002/657/EC . J Chromatogr A , 1157 : 281 – 288 .
  • Codex Alimentarius Commission. 2003. Report of the twenty‐sixth Codex Committee on Residues of Veterinary Drugs in Food, ALINORM 03/23
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  • European Commission. 2002. Commission Decision 2002/657/EC of 12 August 2002 implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results. Brussels: European Commission
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  • Granelli , K , Elgerud , C , Lundström , A , Ohlsson , A and Sjöberg , P . 2009 . Rapid multi‐residue analysis of antibiotics in muscle by liquid chromatography‐tandem mass spectrometry . Analytica Chimica Acta , 637 : 87 – 91 .
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  • McGlinchey , TA , Rafter , PA , Regan , F and McMahon , GP . 2008 . A review of analytical methods for the determination of aminoglycoside and macrolide residues in foods matrices . Analytica Chimica Acta , 624 : 1 – 15 .
  • Meier , PC and Zünd , RE . 2000 . Statistical methods in analytical chemistry, , 2nd , 424 Hoboken , NJ : John Wiley & Sons .
  • Peters , RJB , Bolck , YJC , Rutgers , P , Stolker , AAM and Nielen , MWF . 2009 . Multi‐residue screening of veterinary drugs in egg, fish and meat using high‐resolution liquid chromatography accurate mass time‐of‐flight mass spectrometry . J Chromatogr A , 1216 : 8206 – 8216 .
  • Stubbings , G and Bigwood , T . 2009 . The development and validation of a multiclass liquid chromatography tandem mass spectrometry (LC‐MS/MS) procedure for the determination of veterinary drug residues in animal tissue using a QuEChERS (QUick, Easy, CHeap, Effective, Rugged and Safe) approach . Analytica Chimica Acta , 637 : 68 – 78 .

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