Multi-residue analysis of pesticides in traditional Chinese medicines using gas chromatography-negative chemical ionisation tandem mass spectrometry

References

• Alves AAR, Rodrigues AS, Barros EBP, Uekane TM, Bizzo HR, Rezende CM. 2014. Determination of pesticides residues in Brazilian grape juices using GC-MS-SIM. Food Anal Meth. 7:1834–1839.
   Web of Science ®Google Scholar
• Anagnostopoulos C, Charalampous A, Balayiannis G. 2015. EI and NCI GC-MS and GC-MS/MS: comparative study of performance characteristics for the determination of pesticide residues in plant matrix. Chromatographia. 78:109–118.
   Web of Science ®Google Scholar
• Anastassiades M, Lehotay SJ, Štajnbaher D, Schenck FJ. 2003. Fast and easy multiresidue method employing acetonitrile extraction/partitioning and ‘dispersive solid-phase extraction’ for the determination of pesticide residues in produce. J AOAC Int. 86:412–431.
   PubMed Web of Science ®Google Scholar
• Besil N, Ucles S, Mezcua M, Heinzen H, Fernandez-Alba AR. Forthcoming 2015. Negative chemical ionization gas chromatography coupled to hybrid quadrupole time-of-flight mass spectrometry and automated accurate mass data processing for determination of pesticides in fruit and vegetables. Anal Bioanal Chem.
   PubMedGoogle Scholar
• Bethem R, Boison J, Gale J, Heller D, Lehotay S, Loo J, Musser S, Price P, Stein S. 2003. Establishing the fitness for purpose of mass spectrometric methods. J Am Soc Mass Spectrom. 14:528–541.
   PubMed Web of Science ®Google Scholar
• Cao XW, Shen WJ, Zhu J, Zhang J, Jiang Y, Zhao ZY, Wu B, Yu KY, Liu H, Lian HZ, et al. 2013. A comparative study of the ionization modes in GC-MS multi-residue method for the determination of organochlorine pesticides and polychlorinated biphenyls in crayfish. Food Anal Meth. 6:445–456.
   Web of Science ®Google Scholar
• Chaler R, Vilanova R, Santiago-Silva M, Fernandez P, Grimalt JO. 1998. Enhanced sensitivity in the analysis of trace organochlorine compounds by negative-ion mass spectrometry with ammonia as reagent gas. J Chromatogr A. 823:73–79.
   PubMed Web of Science ®Google Scholar
• Chen LN, Song FR, Liu ZQ, Zheng Z, Xing JP, Liu SY. 2012. Multi-residue method for fast determination of pesticide residues in plants used in traditional Chinese medicine by ultra-high-performance liquid chromatography coupled to tandem mass spectrometry. J Chromatogr A. 1225:132–140.
   PubMed Web of Science ®Google Scholar
• Dong J, Pan YX, Lv JX, Sun J, Gong XM, Li K. 2011. Multiresidue method for the determination of pesticides in fruits and vegetables using gas chromatography-negative chemical ionization-triple quadrupole tandem mass spectrometry. Chromatographia. 74:109–119.
   Web of Science ®Google Scholar
• Erney DR, Gillespie AM, Gilvydis DM, Poole CF. 1993. Explanation of the matrix-induced chromatographic response enhancement of organophosphorus pesticides during open tubular column gas chromatography with splitless or hot on-column injection and flame photometric detection. J Chromatogr A. 638:57–63.
   Web of Science ®Google Scholar
• Feo ML, Eljarrat E, Barceló D. 2011. Performance of gas chromatography/tandem mass spectrometry in the analysis of pyrethroid insecticides in environmental and food samples. Rap Commun Mass Spectrom. 25:869–876.
   PubMed Web of Science ®Google Scholar
• Guo Q, Deng M, Yu BY, Tan L. 2010. Analysis of the residues of 20 organochlorine pesticides in Herba epimedii, a Chinese herbal medicine, by solid-phase extraction with gas chromatography/negative chemical ionization-mass spectrometry. J AOAC Int 93:295–305.
   PubMed Web of Science ®Google Scholar
• Harris ESJ, Cao SG, Littlefield BA, Craycroft JA, Scholten R, Kaptchuk T, Fu YL, Wang WQ, Liu Y, Chen HBA, et al. 2011. Heavy metal and pesticide content in commonly prescribed individual raw Chinese herbal medicines. Sci Tot Environ. 409:4297–4305.
   PubMed Web of Science ®Google Scholar
• Hosseini HM, Asaadi P, Rezaee M, Rezaei MR, Pourjavid MR, Arabieh M, Abhari AA. 2013. Homogeneous liquid–liquid microextraction via flotation assistance (HLLME-FA) method for the pretreatment of organochlorine pesticides in aqueous samples and determination by GC–MS. Chromatographia, 76:1779–1784.
   Web of Science ®Google Scholar
• Húšková R, Matisová E, Hrouzková S, Švorc L. 2009. Analysis of pesticide residues by fast gas chromatography in combination with negative chemical ionization mass spectrometry. J Chromatogr A. 1216:6326–6334.
   PubMed Web of Science ®Google Scholar
• Jia ZW, Mao XH, Chen K, Wang K, Ji S. 2010. Comprehensive multiresidue method for the simultaneous determination of 74 pesticides and metabolites in traditional Chinese herbal medicines by accelerated solvent extraction with high-performance liquid chromatography/tandem mass spectrometry. J AOAC Int. 93:1570–1588.
   PubMed Web of Science ®Google Scholar
• Kalachova K, Cajka T, Sandy C. 2013. High throughput sample preparation in combination with gas chromatography coupled to triple quadrupole tandem mass spectrometry (GC–MS/MS): A smart procedure for (ultra)trace analysis of brominated flame retardants in fish. Talanta. 105: 109–116
   PubMed Web of Science ®Google Scholar
• Koch DA, Clark K, Tessier DM. 2013. Quantification of pyrethroids in environmental samples using NCI-GC-MS with stable isotope analogue standards. J Agric Food Chem. 61:2330–2339.
   PubMed Web of Science ®Google Scholar
• Koesukwiwat U, Lehotay SJ, Miao S, Leepipatpiboon N. 2010. High throughput analysis of 150 pesticides in fruits and vegetables using QuEChERS and low-pressure gas chromatography-time-of-flight mass spectrometry. J Chromatogr A. 1217:6692–6703.
   PubMed Web of Science ®Google Scholar
• Kosalec I, Cvek J, Tomić S. 2009. Contaminants of medicinal herbs and herbal products. Arch Industrial Hyg Toxicol. 60:485–501.
   PubMed Web of Science ®Google Scholar
• Kwon H, Lehotay SJ, Geis-Asteggiante L. 2012. Variability of matrix effects in liquid and gas chromatography-mass spectrometry analysis of pesticide residues after QuEChERS sample preparation of different food crops. J Chromatogr A. 1270:235–245.
   PubMed Web of Science ®Google Scholar
• Lehotay SJ. 2007. Determination of pesticide residues in foods by acetonitrile extraction and partitioning with magnesium sulfate: collaborative study. J AOAC Int. 90:485–520.
   PubMed Web of Science ®Google Scholar
• Lehotay SJ, Son KA, Kwon H, Koesukwiwat H, Fu WS, Mastovska K, Hoh E, Leepipatpiboon N. (2010). Comparison of QuEChERS sample preparation methods for the analysis of pesticide residues in fruits and vegetables. J Chromatrogr A. 1271:2548–2560.
   Web of Science ®Google Scholar
• Lozano A, Rajski Ł, Belmonte-Valles N, Uclés A, Uclés S, Mezcua M, Fernández-Alba AR. 2012. Pesticide analysis in teas and chamomile by liquid chromatography and gas chromatography tandem mass spectrometry using a modified QuEChERS method: validation and pilot survey in real samples J Chromatogr A. 1268: 109–122. 10.1016/j.chroma.2012.10.013
   PubMed Web of Science ®Google Scholar
• Mao XJ, Wan YQ, Yan AP, Shen MY, Wei YL. 2012. Simultaneous determination of organophosphorus, organochlorine, pyrethriod and carbamate pesticides in Radix astragali by microwave-assisted extraction/dispersive-solid phase extraction coupled with GC-MS. Talanta. 97:131–141.
   PubMed Web of Science ®Google Scholar
• Martínez-Uroz MA, Mezcua M, Valles NB, Fernández-Alba AR. 2012. Determination of selected pesticides by GC with simultaneous detection by MS (NCI) and μ-ECD in fruit and vegetable matrices. Anal Bioanal Chem. 402:1365–1372.
   PubMed Web of Science ®Google Scholar
• Maštovská K, Lehotay SJ. 2004. Evaluation of common organic solvents for gas chromatographic analysis and stability of multiclass pesticide residues. J Chromatogr A. 1040:259–272.
   PubMed Web of Science ®Google Scholar
• Munson MSB, Field FH. 1966. Chemical ionization mass spectrometry. I. General introduction. J Am Chem Soc. 88:2621–2630.
   Web of Science ®Google Scholar
• Pizzutti IR, De Kok A, Cardoso CD, Reichert B, De Kroon M, Wind W, Righi LW, Da Silva RC. 2012. A multi-residue method for pesticides analysis in green coffee beans using gas chromatography-negative chemical ionization mass spectrometry in selective ion monitoring mode. J Chromatogr A 1251:16–26.
   PubMed Web of Science ®Google Scholar
• Shen CY, Cao XW, Shen WJ, Jiang YA, Zhao ZY, Wu B, Yu KY, Liu H, Lian HZ. 2011. Determination of 17 pyrethroid residues in troublesome matrices by gas chromatography/mass spectrometry with negative chemical ionization. Talanta. 84:141–147.
   PubMed Web of Science ®Google Scholar
• Smit ALC, Field FH. 1977. Gaseous anion chemistry. Formation and reactions of hydroxide(1-) ion; reactions of anions with nitrous oxide; hydroxide(1-) ion negative chemical ionization. J Am Chem Soc 99:6471–6483.
   Web of Science ®Google Scholar
• Tong HF, Tong YL, Xue J, Liu DJ, Wu XB. 2014. Multi-residual pesticide monitoring in commercial Chinese herbal medicines by gas chromatography-triple quadrupole tandem mass spectrometry. Food Anal Meth. 7:135–145.
   Web of Science ®Google Scholar
• Valles NB, Retamal M, Mezcua M, Fernández-Alba AR. 2012. A sensitive and selective method for the determination of selected pesticides in fruit by gas chromatography/mass spectrometry with negative chemical ionization. J Chromatogr A 1264:110–116.
   PubMed Web of Science ®Google Scholar
• Wong JW, Hennessy MK, Hayward DG, Krynitsky AJ, Cassias I, Schenck FJ. 2007. Analysis of organophosphorus pesticides in dried ground ginseng root by capillary gas chromatography−mass spectrometry and −flame photometric detection. J Agric Food Chem. 55:1117–1128.
   PubMed Web of Science ®Google Scholar
• Xue J, Hao LL, Peng F. 2008. Residues of 18 organochlorine pesticides in 30 traditional Chinese medicines. Chemosphere. 71:1051–1055.
   PubMed Web of Science ®Google Scholar
• Yoon HR, Cho SY, Kim JM, Yoon IB, Park MK, Park JH. 1999. Analysis of multi-component pesticide residues in herbal medicines by GC-MS with electron impact ionization and with positive and negative-ion chemical ionization. Chromatographia. 49:525–534.
   Web of Science ®Google Scholar