A rapid method for the simultaneous determination of 25 anti-hypertensive compounds in dietary supplements using ultra-high-pressure liquid chromatography

References

• Anandakumar K, Jothieswari D, Subathrai R, Santhi D, Vetrichelvan T. 2012. Validated RP-HPLC method for the simultaneous determination of amlodipine besylate, valsartan, and hydrochlorothiazide in bulk and in pharmaceutical formulation. Acta Chromatographica. 24:37–50.
   Web of Science ®Google Scholar
• AOAC Official Methods of Analysis. 2005. International conference on harmonization of harmonized tripartite guideline, validation of analytical procedures: text and methodology. Rockville (MD): AOAC International.
   Google Scholar
• Baing MM, Vaidya VV, Sane RT, Menon SN, Dalvi K. 2006. Simultaneous RP-LC determination of losartan potassium, ramipril, and hydrochlorothiazide in pharmaceutical preparations. Chromatographia. 64:293–296.
   Web of Science ®Google Scholar
• Basavaiah K, Chandrashekar U, Prameela HC. 2003. Sensitive spectrophotometric determination of amlodipine and felodipine using iron(III) and ferricyanide. Il Farmaco. 58:141–148.
   PubMedGoogle Scholar
• Belal F, Al-Zaagi IA, Gadkariem EA, Abounassif MA. 2001. A stability-indicating LC method for the simultaneous determination of ramipril and hydrochlorothiazide in dosage forms. J Pharm Biomed Anal. 24:335–342.
   PubMed Web of Science ®Google Scholar
• Caudron E, Laurent S, Billaud EM, Prognon P. 2004. Simultaneous determination of the acid/base antihypertensive drugs celiprolol, bisoprolol and irbesartan in human plasma by liquid chromatography. J Chromatogr B. 801:339–345.
   PubMed Web of Science ®Google Scholar
• Deconinck E, Sacré PY, Courselle P, De Beer JO. 2013. Chromatography in the detection and characterization of illegal pharmaceutical preparations. J Chromatogr Sci. 51:791–806.
   PubMed Web of Science ®Google Scholar
• Dhaneshwar SR, Patre NG, Mahadik MV. 2009. Validated TLC method for simultaneous quantitation of amlodipine besylate and valsartan in bulk drug and formulation. Chromatographia. 69:157–161.
   Web of Science ®Google Scholar
• Ediage EN, Di Mavungu JD, Scippo ML, Schneider YJ, Larondelle Y, Callebaut A, Robbens J, Van Peteghem C, De Saeger S. 2011. Screening, identification and quantification of glucosinolates in black radish (Raphanus sativus L. niger) based dietary supplements using liquid chromatography coupled with a photodiode array and liquid chromatography-mass spectrometry. J Chromatogr A. 1218:4395–4405.
   PubMed Web of Science ®Google Scholar
• European Medicines Agency. 2009. Evaluation of medicines for human use. Doc Ref: EMEA/CHMP/471165/2009.
   Google Scholar
• Ferraro MC, Castellano PM, Kaufman TS. 2001. A spectrophotometric-partial least squares (PLS-1) method for the simultaneous determination of furosemide and amiloride hydrochloride in pharmaceutical formulations. J Pharm Biomed Anal. 26:443–451.
   PubMed Web of Science ®Google Scholar
• Galande VR, Baheti KG, Dehghan MH. 2011. Development and validation of RP-HPLC and HPTLC method for the estimation of valsartan, hydrochlorothiazide and amlodipine besylate in combined tablet dosage form. Indian Drugs. 48:49–56.
   Google Scholar
• Guillarme D, Nguyen DT, Rudaz S, Veuthey JL. 2008. Method transfer for fast liquid chromatography in pharmaceutical analysis: application to short columns packed with small particles. Part II: gradient experiments. Eur J Pharm Biopharm. 68:430–440.
   PubMed Web of Science ®Google Scholar
• Gupta KR, Mahapatra AD, Wadodkar AR, Wadodkar SG. 2010. Simultaneous UV spectrophotometric determination of valsartan and amlodipine in tablet. Int J Chem Tech Res. 2:551–556.
   Google Scholar
• [ICH] International conference on Harmonization. 2005. Harmonized tripartite guideline, validation of analytical procedures: text and methodology Q2(R1). London: European Medicines Agency (EUMA).
   Google Scholar
• Jamerson KA, Bakris GL, Dahlöf B, Pitt B, Velazquez EJ, Lefkowitz M, Hester A, Shi V, Kjeldsen SE, Cushman W, et al. 2007. Exceptional early blood pressure control rates: the ACCOMPLISH trial. Blood Press. 16:80–86.
   PubMed Web of Science ®Google Scholar
• Kadam BR, Bari SB. 2007. Quantitative analysis of valsartan and hydrochlorothiazide in tablets by high performance thin-layer chromatography with ultraviolet absorption densitometry. Acta Chromatographica. 18:260–269.
   Web of Science ®Google Scholar
• Kjeldsen SE, Jamerson KA, Bakris GL, Pitt B, Dahlöf B, Velazquez EJ, Gupte J, Staikos L, Hua TA, Shi V, et al. 2008. Predictors of blood pressure response to intensified and fixed combination treatment of hypertension: the ACCOMPLISH study. Blood Press. 17:7–17.
   PubMed Web of Science ®Google Scholar
• Kul D, Dogan-Topal B, Kutucu T, Uslu B, Ozkan SA. 2010. High-performance liquid chromatographic and first derivative of the ratio spectrophotometric determination of amlodipine and valsartan in their binary mixtures. J AOAC Int. 93:882–890.
   PubMed Web of Science ®Google Scholar
• Lakshmi Narasimaham YS, Barhate VD. 2010. Validation of stability indicating UPLC method for the simultaneous determination of beta-blockers and diuretic drugs in pharmaceutical dosage forms. J Chem Metrol. 4:1–20.
   Google Scholar
• Lee HM, Lee BJ. 2011. A novel approach to simultaneous screening and confirmation of regulated pharmaceutical compounds in dietary supplements by LC/MS/MS with an information-dependent acquisition method. Food Addit Contam Part A. 28:396–407.
   Web of Science ®Google Scholar
• Pandya KK, Satia M, Gandhi TP, Modi IA, Modi RI, Chakravarthy BK. 1995. Detection and determination of total amlodipine by HPTLC: a useful technique for pharmacokinetic studies. J Chromatogr B. 667:315–320.
   PubMed Web of Science ®Google Scholar
• Prasad CV, Parihar C, Sunil K, Parimoo P. 1998. Simultaneous determination of amiloride HCl, hydrochlorothiazide and atenolol in combined formulations by derivative spectroscopy. J Pharm Biomed Anal. 17:877–884.
   PubMed Web of Science ®Google Scholar
• Rajeshwari KR, Sankar GG, Rao AL, Seshagirirao JVLN. 2006. RP-HPLC method for the simultaneous determination of atorvastatin and amlodipine in tablet dosage form. J Pharm Sci. 68:275–277.
   Google Scholar
• Shi F, Guo C, Gong L, Li J, Dong P, Zhang J, Cui P, Jiang S, Zhao Y, Zeng S. 2014. Application of a high resolution benchtop quadrupole-orbitrap mass spectrometry for the rapid screening, confirmation and quantification of illegal adulterated phosphodiesterase- 5 inhibitors in herbal medicines and dietary supplements. J Chromatogr A. 1344:91−98.
   PubMed Web of Science ®Google Scholar
• Singh S, Prasad B, Savaliya AA, Shah RP, Gohil VM, Kaur A. 2009. Strategies for characterizing sildenafil, vardenafil, tadalafil and their analogues in herbal dietary supplements, and detecting counterfeit products containing these drugs. Trends Anal Chem. 28:13–28.
   Web of Science ®Google Scholar
• Song F, El-Demerdash A, Lee SJ. 2012. Screening for multiple phosphodiesterase type 5 inhibitor drugs in dietary supplement materials by flow injection mass spectrometry and their quantification liquid chromatography tandem mass spectrometry. J Pharm Biomed Anal. 70:40−46.
   PubMed Web of Science ®Google Scholar
• U.S. Food and Drug Administration. 2009. Center for drug evaluation and research. Washington (DC): U.S. Food and Drug Administration.
   Google Scholar
• Vaclavik L, Krynitsky AJ, Rader JI. 2014. Targeted analysis of multiple pharmaceuticals, plant toxins and other secondary metabolites in herbal dietary supplements by ultra-high performance liquid chromatography-quadrupole-orbital ion trap mass spectrometry. Anal Chim Acta. 810:45–60.
   PubMed Web of Science ®Google Scholar
• Vignaduzzo SE, Castellano PM, Kaufman TS. 2011. Development and validation of an HPLC method for the simultaneous determination of amlodipine, hydrochlorothiazide, and valsartan in tablets of their novel triple combination and binary pharmaceutical associations. J Liq Chromatogr Relat Technol. 34:2383–2395.
   Web of Science ®Google Scholar
• White WB, Giles T, Bakris GL, Neutel JM, Davidai G, Weber MA. 2006. Measuring the efficacy of antihypertensive therapy by ambulatory blood pressure monitoring in the primary care setting. Am Heart J. 151:176–184.
   PubMed Web of Science ®Google Scholar