677
Views
22
CrossRef citations to date
0
Altmetric
Original Articles

Quantification of pesticides in food crops using QuEChERS approaches and GC-MS/MS

, , &
Pages 1803-1816 | Received 06 Jun 2016, Accepted 25 Aug 2016, Published online: 17 Nov 2016

References

  • Anastassiades M, Lehotay SJ, Stajnbaher D, Schenck FJ. 2003. Fast and easy multiresidue method employing acetonitrile extraction/partitioning and dispersive solid-phase extraction for the determination of pesticide residues in produce. J AOAC Intl. 86:412–431.
  • Anastassiades M, Mastovska K, Lehotay SJ. 2003. Evaluation of analyte protectants to improve gas chromatographic analysis of pesticides. J Chromatogr A. 1015:163–184.
  • Cajka T, Mastovska K, Lehotay SJ, Hajslova J. 2005. Use of automated direct sample introduction with analyte protectants in the GC-MS analysis of pesticide residues. J Sep Sci. 28:1048–1060.
  • Che D. 2012. Guideline for method validation, Korea Laboratory Accreditation Scheme-G-015. Korean Agency for Technology and Standard.
  • Gonzalez-Rodriguez RM, Rial-Otero R, Cancho-Grande B, Simal-Gandara J. 2008. Determination of 23 pesticide residues in leafy vegetables using gas chromatography-ion trap mass spectrometry and analyte protectants. J Chromatogr A. 1196-1197:100–109.
  • Hermann S, Poulsen ME. 2015. Clean-up of cereal extracts for gas chromatography-tandem quadrupole mass spectrometry pesticide residues analysis using primary and secondary amine and C18. J Chromatogr A. 1423:47–53.
  • Kolberg DI, Prestes OD, Adaime MB, Zanella R. 2011. Development of a fast multiresidue method for the determination of pesticides in dried sample (wheat grains, flour and bran) using QuEChERS based method and GC-MS. Food Chem. 125:1436–1442.
  • Kwon H, Lehotay SJ, Geis-Asteggiante L. 2012. Variability of matrix effects in liquid and gas chromatography-mass spectrometry analysis of pesticide residues after QuEChERS sample preparation of different food crop. J Chromatogr A. 1270:235–245.
  • Lehotay SJ, Kok A, Hiemstra M, Bodegraven P. 2005. Validation of fast and easy method for the determination of residues from 229 pesticides in fruits and vegetables using gas and liquid chromatography and mass spectrometric detection. J AOAC Intl. 88:595–614.
  • Li L, Li W, Qin D, Jiang S, Liu F. 2009. Application of graphitized carbon black to the QuEChERS method for pesticide multiresidue analysis in spinach. J of AOAC Int. 92:538–547.
  • Li Y, Chen X, Fan C, Pang G. 2012. Compensation for matrix effects in the gas chromatography-mass spectrometry analysis of 186 pesticides in tea matrices using analyte protectants. J Chromatogr A. 1266:131–142.
  • Mastovska K, Lehotay SJ, Anastassiades M. 2005. Combination of analyte protectants to overcome matrix effects in routine analysis of pesticide residues in food matrices. Anal Chem. 77:8129–8137.
  • Philstrom T, Fernandez-Alba AR. 2013. Guidance document on method validation and quality control procedures for pesticide residues in food and feed, SANTE/12571/2015. Brussels (Belgium): European Commission.
  • Rasche C, Fournes B, Dirks U, Speer K. 2015. Multi-residue pesticide analysis (gas chromatography-tandem mass spectrometry detection)-improvement of the quick, easy, cheap, effective, rugged, and safe method for dried fruit and fat-rich cereals-benefit and limit of a standardized apple puree calibration (screening). J Chromatogr A. 1403:21–31.
  • Schenck F, Brown A, Podhorniak LV, Parker A, Reliford M, Wong JW. 2008. A rapid multiresidue method for determination of pesticides in fruits and vegetables by using acetonitrile extraction/partitioning and solid-phase extraction column cleanup. J AOAC Int. 91:422–438.
  • Shimelis O, Yang Y, Stenerson K, Kaneko R, Ye M. 2007. Evaluation of a solid-phase extraction dual-layer carbon/primary secondary amine for clean-up of fatty acid matrix components from food extracts in multiresidue pesticide analysis. J Chromatogr A. 1165:18–25.
  • Sugitate K, Nakamura S, Orikata N, Mizukoshi K, Nakamura M, Toriba A, Hayakawa K. 2012. Search of components causing matrix effects on GC/MS for pesticide analysis in food. J Pest Sci. 37:156–163.
  • Yarita T, Aoyagi Y, Otake T. 2015. Evaluation of the impact of matrix effect on quantification of pesticides in food by gas chromatography-mass spectrometry using isotope-labeled internal standards. J Chromatogr A. 1396:109–116.
  • Wong J, Hao C, Zhang K, Yang P, Banerjee K, Hayward D, Iftakhard I, Schreiber A, Tech K, Sack C, et al. 2010. Development and interlaboratory validation of a QuEChERS-based liquid chromatography-tandem mass spectrometry method for multiresidue pesticide analysis. J Agric Food Chem. 58:5897–5903.

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.