Advanced search
Publication Cover
Food Additives & Contaminants: Part A Volume 40, 2023 - Issue 10
Submit an article Journal homepage
977
Views
0
CrossRef citations to date
0
Altmetric
Articles

Polar pesticides in food of animal origin: interlaboratory validation to evaluate method fitness-for-purpose of official control

Veronica Maria Teresa Lattanzioa Institute of Sciences of Food Production, National Research Council of Italy, Bari, ItalyView further author information
,
Biancamaria Ciascaa Institute of Sciences of Food Production, National Research Council of Italy, Bari, ItalyView further author information
,
Emanuela Verdinib Chemistry Department, Istituto Zooprofilattico Sperimentale dell’Umbria e delle Marche “Togo Rosati”, Perugia, ItalyCorrespondence[email protected]
ORCID Iconhttps://orcid.org/0000-0002-8146-600XView further author information
ORCID Icon,
Christoph von Holstc European Commission, Joint Research Centre (JRC), Retieseweg, BelgiumORCID Iconhttps://orcid.org/0000-0002-5892-2302View further author information
ORCID Icon &
Ivan Pecorellib Chemistry Department, Istituto Zooprofilattico Sperimentale dell’Umbria e delle Marche “Togo Rosati”, Perugia, ItalyView further author information
Pages 1345-1356 | Received 19 May 2023, Accepted 30 Aug 2023, Published online: 20 Sep 2023

References

  • Anastassiades M, Wachtler K, Kolberg DI, Eichhorn E, Benkenstein A, Zechmann S, Mack D, Barth A, Wildgrube C, Sigalov I, et al. 2019. Quick method for the analysis of numerous highly polar pesticides in foods of plant origin via LC-MS/MS involving simultaneous extraction with methanol II. Food of Animal Origin (QuPPe-AO-Method). EU Reference Laboratory for pesticides requiring Single Residue Methods (EURL-SRM). Fellbach: CVUA Stuttgart. www.eurl-pesticides.eu
  • Dias J, López SH, Mol H, de Kok A. 2021. Influence of different hydrophilic interaction liquid chromatography stationary phases on method performance for the determination of highly polar anionic pesticides in complex feed matrices. J Sep Sci. 44 (11):2165–2176. doi:10.1002/jssc.202001134.
  • [EC] European Commission. 2022. Commission IMPLEMENTING REGULATION (EU) 2022/2364 of 2 December 2022 amending Implementing Regulation (EU) No 540/2011 as regards the extension of the approval period of the active substance glyphosate. Off J Eur Union. L312:99–100.
  • [EC] European Commission. 2021. COMMISSION IMPLEMENTING REGULATION (EU) 2021/601 of 13 April 2021 concerning a coordinated multiannual control programme of the Union for 2022, 2023 and 2024 to ensure compliance with maximum residue levels of pesticides and to assess the consumer exposure to pesticide residues in and on food of plant and animal origin. Off J Eur Union. L127:29–41.
  • [EC] European Commission. 2023. European commission extension of the approval period of glyphosate. https://food.ec.europa.eu/plants/pesticides/approval-active-substances/renewal-approval/glyphosate_en
  • EFSA, ECHA. 2023. European food safety authority. https://echa.europa.eu/it/-/glyphosate-efsa-and-echa-update-timelines-for-assessments).
  • [EFSA] European Food Safety Authority. 2018. Reasoned Opinion on the review of the existing maximum residue levels for glyphosate according to Article 12 of Regulation (EC) No 396/2005. EFSA J. 16(5):230. doi:10.2903/j.efsa.2018.5263.
  • [EFSA] European Food Safety Authority. 2019. Review of the existing maximum residue levels for glyphosate according to Article 12 of 2005/2005 – revised version to take into account omitted data. EFSA J. 17(10):5862. doi:10.2903/j.efsa.2019.5862.
  • [EFSA] European Food Safety Authority. 2022. Report of pesticide peer review TC 80. https://www.efsa.europa.eu/sites/default/files/2023-01/glyphosate-peer-review-minutes-nov-dec-2022.pdf
  • European Union. 2005. Regulation (EC) No 396/2005 of the European Parliament and of the council of 23 February 2005 on maximum residue levels of pesticides in or on food and feed of plant and animal origin amending Council Directive 91/414/EEC. Off J Eur Union. L70:1–16.
  • EURL-SRM EU Reference Laboratories for Residues of Pesticides. 2021. Interlaboratory validation study polar pesticidesQuPPe Method “Gly&Co”. https://www.eurl-pesticides.eu/userfiles/file/EurlFV/Joint2021/Wachtler-Zipper.pdf.
  • EURL-SRM. 2014. EU proficiency test on the analysis of spiked pesticides requiring single residue methods in cow’s milk. 1–67. https://www.eurl-pesticides.eu/library/docs/srm/EUPT_SRM9_FinalReport.pdf
  • EURL-SRM. 2019. EU proficiency test on the analysis of bovine liver homogenate for residues of pesticides requiring single residue methods. 1–43. https://www.eurl-pesticides.eu/library/docs/srm/EUPT_SRM14_FinalReport.pdf
  • European Commission. 2021. Guidance document on analytical quality control and method validation for pesticide residues analysis in food and feed SANTE 11312/2021. Sante/11312/2021. 1–7. https://ec.europa.eu/food/system/files/2022-02/pesticides_mrl_guidelines_wrkdoc_2021-11312.pdf.
  • ISO 5725-5. 1994. Accuracy (trueness and precision) of measurement method and results. Part 5: alternative methods for the determination of the precision of a standard measurement method. Geneva: international Organization for Standardization.
  • Verdini E, Pecorelli I. 2022. The current status of analytical methods applied to the determination of polar pesticides in food of animal origin: a brief review. Foods. 11(10):1527. doi:10.3390/foods11101527.
  • Verdini E, Lattanzio VMT, Ciasca B, Fioroni L, Pecorelli I. 2023. Improved method for the detection of highly polar pesticides and their main metabolites in foods of animal origin: method validation and application to monitoring programme. Separations. 10(1):44. doi:10.3390/separations10010044.
  • Wu Y, Zhou Y, Jiao X, She Y, Zeng W, Cui H, Pan C. 2023. Development and inter-laboratory validation of analytical methods for glufosinate and its two metabolites in foods of plant origin. Anal Bioanal Chem. 1–12. doi:10.1007/s00216-023-04542-9.

Related research

People also read lists articles that other readers of this article have read.

Recommended articles lists articles that we recommend and is powered by our AI driven recommendation engine.

Cited by lists all citing articles based on Crossref citations.
Articles with the Crossref icon will open in a new tab.