References

• Anwar, S. H., & Kunz, B. (2011). The influence of drying methods on the stabilization of fish oil microcapsules: Comparison of spray granulation, spray drying, and freeze drying. Journal of Food Engineering, 105, 367–378. doi:10.1016/j.jfoodeng.2011.02.047
   Web of Science ®Google Scholar
• Balch, S. A., McKenney, C. B., & Auld, D. L. (2003). Evaluation of gamma-linolenic acid composition of evening primrose (Oenothera) species native to Texas. HortScience, 38, 595–598. doi:10.21273/HORTSCI.38.4.595
   Web of Science ®Google Scholar
• Benković, M., & Bauman, I. (2011). Agglomeration of cocoa powder mixtures–Influence of process conditions on physical properties of the agglomerates. Journal on Processing and Energy in Agriculture, 15, 46–53.
   Google Scholar
• Berti, M., Johnson, B. L., Dash, S., Fischer, S., Wilckens, R., & Hevia, F. (2007). Echium: A source of stearidonic acid adapted to the northern great plains in the US. In J. Janick & A. Whipkey (Eds.), Issues in new crops and new uses (pp. 120–125). Alexandria, VA: ASHS Press.
   Google Scholar
• Cal, K., & Sollohub, K. (2010). Spray drying technique. I: Hardware and process parameters. Journal of Pharmaceutical Sciences, 99, 575–586. doi:10.1002/jps.21886
   PubMed Web of Science ®Google Scholar
• Calvo, P., Castaño, Á. L., Hernández, M. T., & González-Gómez, D. (2011). Effects of microcapsule constitution on the quality of microencapsulated walnut oil. European Journal of Lipid Science and Technology, 113, 1273–1280. doi:10.1002/ejlt.201100039
   Web of Science ®Google Scholar
• Calvo, P., Castaño, Á. L., Lozano, M., & González-Gómez, D. (2012). Influence of the microencapsulation on the quality parameters and shelf-life of extra-virgin olive oil encapsulated in the presence of BHT and different capsule wall components. Food Research International, 45, 256–261. doi:10.1016/j.foodres.2011.10.036
   Web of Science ®Google Scholar
• Caparino, O. A., Tang, J., Nindo, C. I., Sablani, S. S., Powers, J. R., & Fellman, J. K. (2012). Effect of drying methods on the physical properties and microstructures of mango (Philippine ‘Carabao’ var.) powder. Journal of Food Engineering, 111, 135–148. doi:10.1016/j.jfoodeng.2012.01.010
   Web of Science ®Google Scholar
• Carneiro, H. C. F., Tonon, R. V., Grosso, C. R. F., & Hubinger, M. D. (2013). Encapsulation efficiency and oxidative stability of flaxseed oil microencapsulated by spray drying using different combinations of wall materials. Journal of Food Engineering, 115, 443–451. doi:10.1016/j.jfoodeng.2012.03.033
   Web of Science ®Google Scholar
• Celli, G. B., Ghanem, A., & Brooks, M. S.-L. (2015). Bioactive encapsulated powders for functional foods – A review of methods and current limitations. Food and Bioprocess Technology, 8, 1825–1837. doi:10.1007/s11947-015-1559-z
   Web of Science ®Google Scholar
• Choe, E., & Min, D. B. (2006). Comprehensive reviews in food science and food safety mechanisms and factors for edible oil oxidation. Comprehensive Reviews in Food Science and Food Safety, 5, 169–186. doi:10.1111/crfs.2006.5.issue-4
   Web of Science ®Google Scholar
• Coupland, K. (2008). Stearidonic acid: A plant produced omega-3 PUFA and a potential alternative for marine oil fatty acids. Lipid Technology, 20, 152–154. doi:10.1002/lite.v20:7
   Google Scholar
• Czaplicki, S., Ogrodowska, D., Derewiaka, D., Tańska, M., & Zadernowski, R. (2011). Bioactive compounds in unsaponifiable fraction of oils from unconventional sources. European Journal of Lipid Science and Technology, 113, 1456–1464. doi:10.1002/ejlt.201000410
   Web of Science ®Google Scholar
• Czaplicki, S., Tańska, M., & Konopka, I. (2016). Sea-buckthorn oil in vegetable oils stabilisation. Italian Journal of Food Science, 28, 412–425.
   Web of Science ®Google Scholar
• Czaplicki, S., Zadernowski, R., & Ogrodowska, D. (2009). Triacylglycerols from viper bugloss (Echium vulgare L.) seed bio-oil. European Journal of Lipid Science and Technology, 111, 1266–1269. doi:10.1002/(ISSN)1438-9312
   Web of Science ®Google Scholar
• Dobry, D. E., Settell, D. M., Baumann, J. M., Ray, R. J., Graham, L. J., & Beyerinck, R. A. (2009). A model-based methodology for spray-drying process development. Journal of Pharmaceutical Innovation, 4, 133–142. doi:10.1007/s12247-009-9064-4
   PubMed Web of Science ®Google Scholar
• El Asbahani, A., Miladi, K., Badri, W., Sala, M., Addi, E. H. A., Casabianca, H., … Elaissari, A. (2015). Essential oils: From extraction to encapsulation. International Journal of Pharmaceutics, 483, 220–243. doi:10.1016/j.ijpharm.2014.12.069
   PubMed Web of Science ®Google Scholar
• El Ghannam, M., El Nemr, T., Hassan, A., & Dyab, N. (2015). Encapsulation efficiency, microstructure and oxidation stability of fish oil encapsulated powder made by using whey protein concentrate. Alexandria Science Exchange Journal, 36, 236–248.
   Google Scholar
• Eskin, N. A. M. (2008). Borage and evening primrose oil. European Journal of Lipid Science and Technology, 110, 651–654. doi:10.1002/ejlt.v110:7
   Web of Science ®Google Scholar
• Ferreira, C. D., Janaína, E., Aparecida, B., Machado, S., & Hermes, V. S. (2016). Physicochemical characterization and oxidative stability of microencapsulated crude palm oil by spray drying. Food and Bioprocess Technology, 9, 124–136. doi:10.1007/s11947-015-1603-z
   Web of Science ®Google Scholar
• Gallardo, G., Guida, L., Martinez, V., López, M. C., Bernhardt, D., Blasco, R., … Hermida, L. G. (2013). Microencapsulation of linseed oil by spray drying for functional food application. Food Research International, 52, 473–482. doi:10.1016/j.foodres.2013.01.020
   Web of Science ®Google Scholar
• Giuffrè, A. M., & LouAdj, L. (2013). Influence of crop season and cultivar on sterol composition of monovarietal olive oils in Reggio Calabria (Italy). Czech Journal of Food Sciences, 31, 256–263. doi:10.17221/CJFS
   Web of Science ®Google Scholar
• Karaca, C. A., Low, N., & Nickerson, M. (2013). Encapsulation of flaxseed oil using a benchtop spray dryer for legume protein – Maltodextrin microcapsule preparation. Journal of Agricultural and Food Chemistry, 61, 5148–5155. doi:10.1021/jf400787j
   PubMed Web of Science ®Google Scholar
• Karim, F. T., Ghafoor, K., Ferdosh, S., Al-Juhaimi, F., Ali, E., Yunus, K. B., … Sarker, M. Z. I. (2017). Microencapsulation of fish oil using supercritical antisolvent process. Journal of Food and Drug Analysis, 25, 654–666. doi:10.1016/j.jfda.2016.11.017
   PubMed Web of Science ®Google Scholar
• Kawasaki, H., Shimanouchi, T., & Kimura, Y. (2019). Recent development of optimization of lyophilization process. Journal of Chemistry, 2019, 1–14. Article ID 9502856 doi: 10.1155/2019/9502856
   Web of Science ®Google Scholar
• Khan, M. A., & Shahidi, F. (2002). Photooxidative stability of stripped and non-stripped borage and evening primrose oils and their emulsions in water. Food Chemistry, 79, 47–53. doi:10.1016/S0308-8146(02)00176-0
   Web of Science ®Google Scholar
• Lin, Y., Knol, D., Valk, I., van Andel, V., Friedrichs, S., Lütjohann, D., … Trautwein, E. A. (2017). Thermal stability of plant sterols and formation of their oxidation products in vegetable oils and margarines upon controlled heating. Chemistry and Physics of Lipids, 207, 99–107. doi:10.1016/j.chemphyslip.2017.01.007
   PubMed Web of Science ®Google Scholar
• Liu, S., Low, N. H., & Nickerson, M. T. (2010). Entrapment of flaxseed oil within gelatin-gum arabic capsules. Journal of American Oil Chemists’ Society, 87, 809–815. doi:10.1007/s11746-010-1560-7
   Web of Science ®Google Scholar
• López-Martínez, J. C., Campra-Madrid, P., & Guil-Guerrero, J. L. (2004). γ-Linolenic acid enrichment from Borago officinalis and Echium fastuosum seed oils and fatty acids by low temperature crystallization. Journal of Bioscience and Bioengineering, 97, 294–298. doi:10.1016/S1389-1723(04)70208-X
   PubMed Web of Science ®Google Scholar
• Marwede, V., Schierholt, A., Möllers, C., & Becker, H. C. (2004). Genotype × environment interactions and heritability of tocopherol contents in canola. Crop Science, 44, 728–731. doi:10.2135/cropsci2004.7280
   Web of Science ®Google Scholar
• Melgosa, R., Benito-Román, Ó., Sanz, M. T., de Paz, E., & Beltrán, S. (2019). Omega–3 encapsulation by PGSS-drying and conventional drying methods. Particle characterization and oxidative stability. Food Chemistry, 270, 138–148. doi:10.1016/j.foodchem.2018.07.082
   PubMed Web of Science ®Google Scholar
• Montserrat-de la Paz, S., Fernandez-Arche, M. A., Angel-Martin, M., & Garcia-Gimenez, M. D. (2014). Phytochemical characterization of potential nutraceutical ingredients from evening primrose oil (Oenothera biennis L.). Phytochemistry Letters, 8, 158–162. doi:10.1016/j.phytol.2013.08.008
   Web of Science ®Google Scholar
• Najafi, M. N., & Kadkhodaee, R. (2011). Effect of drying process and wall material on the properties of encapsulated cardamom oil. Food Biophysics, 6, 68–76. doi:10.1007/s11483-010-9176-x
   Web of Science ®Google Scholar
• Ng, S. K., Jessie, L. Y. L., Tan, C. P., Long, K., & Nyam, K. L. (2013). Effect of accelerated storage on microencapsulated kenaf seed oil. Journal of the American Oil Chemists’ Society, 90, 1023–1029. doi:10.1007/s11746-013-2249-5
   Web of Science ®Google Scholar
• Nogala-Kalucka, M., Rudzinska, M., Zadernowski, R., Siger, A., & Krzyzostaniak, I. (2010). Phytochemical content and antioxidant properties of seeds of unconventional oil plants. Journal of the American Oil Chemists’ Society, 87, 1481–1487. doi:10.1007/s11746-010-1640-8
   Web of Science ®Google Scholar
• Ogrodowska, D., Tańska, M., & Brandt, W. (2017). The Influence of drying process conditions on the physical properties, bioactive compounds and stability of encapsulated pumpkin seed oil. Food and Bioprocess Technology, 10, 1265–1280. doi:10.1007/s11947-017-1898-z
   Web of Science ®Google Scholar
• Özcan, T. (2008). Analysis of the total oil and fatty acid composition of seeds of some Boraginaceae taxa from Turkey. Plant Systematics and Evolution, 274, 143–153. doi:10.1007/s00606-008-0039-6
   Web of Science ®Google Scholar
• Özcan, T. (2013). Molecular (RAPDs and Fatty acid) and micromorphological variations of Echium italicum L. populations from Turkey. Plant Systematics and Evolution, 299, 631–641. doi:10.1007/s00606-012-0749-7
   Web of Science ®Google Scholar
• Peiretti, P. G., Palmegiano, G. B., & Salamano, G. (2004). Quality and fatty acid content of borage (Borago officinalis L.) during the growth cycle. Italian Journal of Food Science, 16, 177–184.
   Web of Science ®Google Scholar
• Quispe-Condori, S., Saldaña, M. D. A., & Temelli, F. (2011). Microencapsulation of flax oil with zein using spray and freeze drying. LWT – Food Science and Technology, 44, 1880–1887. doi:10.1016/j.lwt.2011.01.005
   Web of Science ®Google Scholar
• Roche, J., Mouloungui, Z., Cerny, M., & Merah, O. (2019). Effect of sowing dates on fatty acids and phytosterols patterns of Carthamus tinctorius L. Applied Sciences, 9(2839), 1–10. doi:10.3390/app9142839
   Google Scholar
• Rudzińska, M., Przybylski, R., & Wąsowicz, E. (2009). Products formed during thermo‐oxidative degradation of phytosterols. Journal of the American Oil Chemists’ Society, 86, 651–662. doi:10.1007/s11746-009-1397-0
   Web of Science ®Google Scholar
• Scrimgeour, C., & Clough, P. (2014). Authentication of borage oil. Lipid Technology, 26, 230–233. doi:10.1002/lite.201400059
   Google Scholar
• Senanayake, S. P. J. N., & Shahidi, F. (2002). Chemical and stability characteristics of structured lipids from borage (Borago officinalis L.) and evening primrose (Oenothera biennis L.) oils. Journal of Food Science, 67, 2038–2045. doi:10.1111/jfds.2002.67.issue-6
   Web of Science ®Google Scholar
• Shaw, E. J., Kakuda, Y., & Rajcan, I. (2016). Effect of genotype, environment, and genotype × environment interaction on tocopherol accumulation in soybean seed. Crop Science, 56, 40–50. doi:10.2135/cropsci2015.02.0069
   Web of Science ®Google Scholar
• Silva, E. K., Zabot, G. L., Bargas, M. A., & Meireles, M. A. A. (2016). Microencapsulation of lipophilic bioactive compounds using prebiotic carbohydrates: Effect of the degree of inulin polymerization. Carbohydrate Polymers, 152, 775–783. doi:10.1016/j.carbpol.2016.07.066
   PubMed Web of Science ®Google Scholar
• Soh, S. H., & Lee, L. Y. (2019). Microencapsulation and nanoencapsulation using supercritical fluid (SCF) techniques. Pharmaceutics, 11, 21. doi:10.3390/pharmaceutics11010021
   Web of Science ®Google Scholar
• Szterk, A., Roszko, M., Sosińska, E., Derewiaka, D., & Lewicki, P. P. (2010). Chemical composition and oxidative stability of selected plant oils. Journal of the American Oil Chemists’ Society, 87, 637–645. doi:10.1007/s11746-009-1539-4
   Web of Science ®Google Scholar
• Tańska, M., Rotkiewicz, D., Kozirok, W., & Konopka, I. (2005). Measurement of the geometrical features and surface color of rapeseeds using digital image analysis. Food Research International, 38, 741–750. doi:10.1016/j.foodres.2005.01.008
   Web of Science ®Google Scholar
• Toivo, J., Phillips, K., Lampi, A. M., & Piironen, V. (2001). Determination of sterols in foods: Recovery of free, esterified, and glycosidic sterols. Journal of Food Composition and Analysis, 14, 631–643. doi:10.1006/jfca.2001.1019
   Web of Science ®Google Scholar
• Velasco, J., Holgado, F., Dobarganes, C., & Márquez-Ruiz, G. (2009). Influence of relative humidity on oxidation of the free and encapsulated oil fractions in freeze-dried microencapsulated oils. Food Research International, 42, 1492–1500. doi:10.1016/j.foodres.2009.08.007
   Web of Science ®Google Scholar
• Wagdare, N. A., Marcelis, A. T. M., Boom, R. M., & van Rijn, C. J. M. (2011). Microcapsules with a pH responsive polymer: Influence of the encapsulated oil on the capsule morphology. Colloids and Surfaces B: Biointerfaces, 88, 175–180. doi:10.1016/j.colsurfb.2011.06.028
   PubMed Web of Science ®Google Scholar
• Westergaard, V. (2004). Milk powder technology evaporation and spray drying (5th ed.). Copenhagen, Denmark: GEA Niro A/S.
   Google Scholar
• Yüksel, A., & Yeşilçubuk, N. Ş. (2012). Enzymatic production of human milk fat analogues containing stearidonic acid and optimization of reactions by response surface methodology. LWT – Food Science and Technology, 46, 210–216. doi:10.1016/j.lwt.2011.10.004
   Web of Science ®Google Scholar