Technical and environmental assessment of hydrothermally synthesized foshagite and tobermorite-like crystals as fibrillar C-S-H seeds in cementitious materials

References

• Miller SA, Moore FC. Climate and health damages from global concrete production. Nat Clim Change 2020;10(5):439–443.
   Web of Science ®Google Scholar
• Monteiro PJM, Miller SA, Horvath A. Towards sustainable concrete. Nat Mater. 2017;16(7):698–699.
   PubMed Web of Science ®Google Scholar
• Fransen T, Lebling K, Weyl D, et al. Toward a Tradable Low-Carbon Cement Standard: policy Design Considerations for the United States. WRIPUB [Internet]. 2021. [cited 2021 Nov 12]; Available from: https://www.wri.org/research/toward-tradable-low-carbon-cement-standard-policy-design-considerations-united-states.
   Google Scholar
• IEA and CSI. Technology Roadmap - Low-Carbon Transition in the Cement Industry [Internet]. 2018. p. 66. Available from: https://www.wbcsd. org/contentwbc/download/4586/61682/1.
   Google Scholar
• Adams MP. Concrete Solutions to Climate Change. 2021;20.
   Google Scholar
• PCA. Roadmap to Carbon Neutrality [Internet]. 2021. [cited 2021 Oct 21]. Available from: https://www.cement.org/sustainability/roadmap-to-carbon-neutrality.
   Google Scholar
• Golewski GL, Szostak B. Strengthening the very early-age structure of cementitious composites with coal fly ash via incorporating a novel nanoadmixture based on C-S-H phase activators. Constr Build Mater. 2021;312:125426.
   Web of Science ®Google Scholar
• Skibsted J, Snellings R. Reactivity of supplementary cementitious materials (SCMs) in cement blends. Cem Concr Res. 2019;124:105799.
   Web of Science ®Google Scholar
• Black L, Garbev K, Gee I. Surface carbonation of synthetic C-S-H samples: a comparison between fresh and aged C-S-H using X-ray photoelectron spectroscopy. Cem Concr Res. 2008;38(6):745–750.
   Web of Science ®Google Scholar
• Kumar A, Walder BJ, Kunhi Mohamed A, et al. The atomic-level structure of cementitious calcium silicate hydrate. J Phys Chem C. 2017;121(32):17188–17196.
   Web of Science ®Google Scholar
• Thomas JJ, Jennings HM, Chen JJ. Influence of nucleation seeding on the hydration mechanisms of tricalcium silicate and cement. J PhysChem C. 2009;113(11):4327–4334.
   Web of Science ®Google Scholar
• Nicoleau L. Accelerated growth of calcium silicate hydrates: experiments and simulations. Cem Concr Res. 2011;41(12):1339–1348.
   Web of Science ®Google Scholar
• Alizadeh R, Raki L, Makar JM, et al. Hydration of tricalcium silicate in the presence of synthetic calcium–silicate–hydrate. J. Mater. Chem. 2009;19(42):7937.
   Web of Science ®Google Scholar
• Land G, Stephan D. The effect of synthesis conditions on the efficiency of C-S-H seeds to accelerate cement hydration. Cem Concr Compos. 2018;87:73–78.
   Web of Science ®Google Scholar
• Li J, Zhang W, Xu K, et al. Fibrillar calcium silicate hydrate seeds from hydrated tricalcium silicate lower cement demand. Cem Concr Res. 2020;137:106195.
   Web of Science ®Google Scholar
• Hubler MH, Thomas JJ, Jennings HM. Influence of nucleation seeding on the hydration kinetics and compressive strength of alkali activated slag paste. Cem Concr Res. 2011;41(8):842–846.
   Web of Science ®Google Scholar
• He J, Long G, Ma K, et al. Improvement of the hydration of a fly ash–cement system by the synergic action of triethanolamine and C–S–H seeding. ACS Sustain Chem Eng. 2021;9(7):2804–2815.
   Web of Science ®Google Scholar
• Kanchanason V, Plank J. Effectiveness of a calcium silicate hydrate – polycarboxylate ether (C-S-H–PCE) nanocomposite on early strength development of fly ash cement. Constr Build Mater. 2018;169:20–27.
   Web of Science ®Google Scholar
• Morales-Cantero A, Cuesta A, De la Torre AG, et al. Portland and belite cement hydration acceleration by C-S-H seeds with variable w/c ratios. Materials. 2022;15(10):3553.
   PubMed Web of Science ®Google Scholar
• Szostak B, Golewski GL. Rheology of cement pastes with siliceous fly ash and the CSH nano-admixture. Materials. 2021;14(13):3640.
   PubMed Web of Science ®Google Scholar
• Zhou Z, Sofi M, Liu J, et al. Nano-CSH modified high volume fly ash concrete: early-age properties and environmental impact analysis. J Cleaner Prod. 2021;286:124924.
   Web of Science ®Google Scholar
• Kanchanason V, Plank J. Effect of Calcium Silicate Hydrate – Polycarboxylate Ether (C-S-H–P CE) Nanocomposite as Accelerating Admixture on Early Strength Enhancement of Slag and Calcined Clay Blended Cements. Cem Concr Res. 2019;119:44–50.
   Google Scholar
• Sun J, Dong H, Wu J, Jiang J, Li W, Shen X, Hou G. Properties Evolution of Cement-Metakaolin System with C-S-H/P CE Nanocomposites. Constr Build Mater. 2021;282:122707.
   Google Scholar
• Golewski GL, Szostak B. Application of the C-S-H phase nucleating agents to improve the performance of sustainable concrete composites containing fly ash for use in the precast concrete industry. Materials. 2021;14(21):6514.
   PubMed Web of Science ®Google Scholar
• Zhang G, Yang Y, Li H. Calcium-silicate-hydrate seeds as an accelerator for saving energy in cold weather concreting. Constr Build Mater. 2020;264:120191.
   Web of Science ®Google Scholar
• John E, Matschei T, Stephan D. Nucleation seeding with calcium silicate hydrate – a review. Cem Concr Res. 2018;113:74–85.
   Web of Science ®Google Scholar
• Wang B, Yao W, Stephan D. Preparation of calcium silicate hydrate seeds by means of mechanochemical method and its effect on the early hydration of cement. Adv Mech Eng. 2019;11(4):168781401984058.
   Web of Science ®Google Scholar
• Taylor HFW, Bessey GE. A review of hydrothermal reactions in the system CaO - SiO2 - H2O. Mag Concr Res. 1950;2(4):15–26.
   Google Scholar
• Hong S-Y, Glasser FP. Phase relations in the CaO–SiO2–H2O system to 200 °C at saturated steam pressure. Cem Concr Res. 2004;34(9):1529–1534.
   Web of Science ®Google Scholar
• National Research Council (U.S.). editor. Guide to compounds of interest in cement and concrete research. Washington: National Research Council; 1972.
   Google Scholar
• Bellmann F, Sowoidnich T, Horgnies M, et al. Basic mechanisms of afwillite seeding for acceleration of tricalcium silicate hydration. Cem Concr Res. 2020;132:106030.
   Web of Science ®Google Scholar
• Horgnies M, Fei L, Arroyo R, et al. The effects of seeding C3S pastes with afwillite. Cem Concr Res. 2016;89:145–157.
   Web of Science ®Google Scholar
• Davis RW, Young JF. Hydration and strength development in tricalcium silicate pastes seeded with afwillite. J Am Ceram Soc. 1975;58(1–2):67–70.
   Web of Science ®Google Scholar
• Eisinas A, Baltakys K, Siauciunas R. The effect of gyrolite additive on the hydration properties of Portland cement. Cem Concr Res. 2012;42(1):27–38.
   Web of Science ®Google Scholar
• John E, Lehmann C, Stephan D. Xonotlite and hillebrandite as model compounds for calcium silicate hydrate seeding in cementitious materials. Transp Res Rec. 2020;2765:9, https://doi.org/10.1177/036119812094320
   Google Scholar
• John E, Epping JD, Stephan D. The influence of the chemical and physical properties of C-S-H seeds on their potential to accelerate cement hydration. Constr Build Mater. 2019;228:116723.
   Web of Science ®Google Scholar
• Wang F, Kong X, Jiang L, et al. The acceleration mechanism of nano-C-S-H particles on OPC hydration. Constr Build Mater. 2020;249:118734.
   Web of Science ®Google Scholar
• Wyrzykowski M, Assmann A, Hesse C, et al. Microstructure development and autogenous shrinkage of mortars with C-S-H seeding and internal curing. Cem Concr Res. 2020;129:105967.
   Web of Science ®Google Scholar
• Biagioni C, Merlino S, Bonaccorsi E. The tobermorite supergroup: a new nomenclature. Min Mag. 2015;79(2):485–495.
   Web of Science ®Google Scholar
• Miseljic M, Olsen SI. LCA of nanomaterials. In: Hauschild MZ, Rosenbaum RK, Olsen SI, editors. Life cycle assessment: theory and practice [internet]. Cham: Springer International Publishing; 2018. p. 817–833. Available from:
   Google Scholar
• Minerals EP. Celatom Mineral Natural (MN) diatomaceous earth functional additive grades | EP Minerals [Internet]. [cited 2022 Apr 25]. Available from: https://epminerals.com/products/celatom-mineral-natural-mn.
   Google Scholar
• USGS. Diatomite Statistics and Information | U.S. Geological Survey [Internet]. 2022. [cited 2022 Apr 25]. Available from https://www.usgs.gov/centers/national-minerals-information-center/diatomite-statistics-and-information.
   Google Scholar
• Gardner DW, Li J, Morshedifard A, et al. Silicate bond characteristics in calcium–silicate–hydrates determined by high pressure raman spectroscopy. J Phys Chem C. 2020;124(33):18335–18345.
   Web of Science ®Google Scholar
• Cong, X., & Kirkpatrick, R. J. (1996). 29Si MAS NMR study of the structure of calcium silicate hydrate. Advanced Cement Based Materials, 3(3–4), 144–156.
   Google Scholar
• Tavakoli D, Tarighat A. Estimation of the elastic properties of important calcium silicate hydrates in nano scale - a molecular dynamics approach. Rehabilitation in Civil [Internet]. 2018. [cited 2021 Sep 10]; Available from:
   Google Scholar
• Gard JA, Taylor HFW. The crystal structure of foshagite. Acta Cryst. 1960;13(10):785–793.
   Google Scholar
• Meller N, Kyritsis K, Hall C. The mineralogy of the CaO–Al2O3–SiO2–H2O (CASH) hydroceramic system from 200 to 350 °C. Cem Concr Res. 2009;39(1):45–53.
   Web of Science ®Google Scholar
• ASTM C348-20. Test method for flexural strength of hydraulic-cement mortars [Internet]. ASTM International; 2020. [cited 2020 Dec 28]. Available from: http://www.astm.org/cgi-bin/resolver.cgi?C348-20.
   Google Scholar
• ASTM 1608-07. Test method for density and void content of freshly mixed pervious concrete [Internet]. ASTM International; 2012. [cited 2022 Apr 1]. Available from: http://www.astm.org/cgi-bin/resolver.cgi?C1688C1688M-14A.
   Google Scholar
• Deboucha W, Leklou N, Khelidj A, et al. Hydration development of mineral additives blended cement using thermogravimetric analysis (TGA): methodology of calculating the degree of hydration. Constr Build Mater. 2017;146:687–701.
   Web of Science ®Google Scholar
• Roychand R, De Silva S, Law D, et al. High volume fly ash cement composite modified with nano silica, hydrated lime and set accelerator. Mater Struct. 2016;49(5):1997–2008.
   Web of Science ®Google Scholar
• Alarcon-Ruiz L, Platret G, Massieu E, et al. The use of thermal analysis in assessing the effect of temperature on a cement paste. Cem Concr Res. 2005;35(3):609–613.
   Web of Science ®Google Scholar
• Gallucci E, Zhang X, Scrivener KL. Effect of temperature on the microstructure of calcium silicate hydrate (C-S-H). Cem Concr Res. 2013;53:185–195.
   Web of Science ®Google Scholar
• Ghafari E, Feys D, Khayat K. Feasibility of using natural SCMs in concrete for infrastructure applications. Constr Build Mater. 2016;127:724–732.
   Web of Science ®Google Scholar
• Kim T, Olek J. Effects of sample preparation and interpretation of thermogravimetric curves on calcium hydroxide in hydrated pastes and mortars. Transp Res Rec. 2012;2290(1):10–18.
   Google Scholar
• Foley EM, Kim JJ, Reda Taha MM. Synthesis and nano-mechanical characterization of calcium-silicate-hydrate (C-S-H) made with 1.5 CaO/SiO2 mixture. Cem Concr Res. 2012;42(9):1225–1232.
   Web of Science ®Google Scholar
• ASTM C109/C109M-20b. Test Method for Compressive Strength of Hydraulic Cement Mortars (Using 2-in. or [50-mm] Cube Specimens) [Internet]. ASTM International; [cited 2020 Dec 28]. Available from: http://www.astm.org/cgi-bin/resolver.cgi?C109C109M-20B.
   Google Scholar
• Chertow MR, Lombardi DR. Quantifying economic and environmental benefits of Co-Located firms. Environ Sci Technol. 2005;39(17):6535–6541.
   PubMed Web of Science ®Google Scholar
• Ruiz-Puente C, Jato-Espino D. Systemic analysis of the contributions of Co-Located industrial symbiosis to achieve sustainable development in an industrial park in Northern Spain. Sustainability. 2020;12(14):5802.
   Web of Science ®Google Scholar
• Holmberg H, Tuomaala M, Haikonen T, et al. Allocation of fuel costs and CO2-emissions to heat and power in an industrial CHP plant: case integrated pulp and paper mill. Appl Energy. 2012;93:614–623.
   Web of Science ®Google Scholar
• ISO. ISO 21930-2017. Sustainability in buildings and civil engineering Works- Core rules for environmental product declarations of construction products and services. 2017.
   Google Scholar
• Bräu M, Ma-Hock L, Hesse C, et al. Nanostructured calcium silicate hydrate seeds accelerate concrete hardening: a combined assessment of benefits and risks. Arch Toxicol. 2012;86(7):1077–1087.
   PubMed Web of Science ®Google Scholar
• Bare J. Tool for the reduction and assessment of chemical and other environmental impacts (TRACI). Version 2.1 - User’s Manual; EPA/600/R-12/554. 2012.
   Google Scholar
• GreenDelta. OpenLCA Software 1.8.0. Available online: www.greendelta.com (accessed on July 30 2020).
   Google Scholar
• Battocchio F, Monteiro PJM, Wenk H-R. Rietveld refinement of the structures of 1.0 C-S-H and 1.5 C-S-H. Cem Concr Res. 2012;42(11):1534–1548.
   Web of Science ®Google Scholar
• Merlino S, Bonaccorsi E, Armbruster T. Tobermorites; their real structure and order-disorder (OD) character. Am Min. 1999;84(10):1613–1621.
   Web of Science ®Google Scholar
• Kim JJ, Foley EM, Reda Taha MM. Nano-mechanical characterization of synthetic calcium–silicate–hydrate (C–S–H) with varying CaO/SiO2 mixture ratios. Cem Concr Compos. 2013;36:65–70.
   Web of Science ®Google Scholar
• Cuesta A, Santacruz I, De la Torre AG, et al. Local structure and Ca/Si ratio in C-S-H gels from hydration of blends of tricalcium silicate and silica fume. Cem Concr Res. 2021;143:106405.
   Web of Science ®Google Scholar
• Taylor HFW. Crestmoreite and riversideite |. Mineralogical magazine and journal of the Mineralogical Society | Cambridge Core [Internet]. 1952. [cited 2021 Sep 15]; Available from: https://www.cambridge.org/core/journals/mineralogical-magazine-and-journal-of-the-mineralogical-society/article/abs/crestmoreite-and-riversideite/533AA2FCC64B82AE2B5D65D113CDD2A3.
   Google Scholar
• Bell NS, Venigalla S, Gill PM, et al. Morphological forms of tobermorite in hydrothermally treated calcium silicate hydrate gels. J Am Ceram Soc. 1996;79(8):2175–2178.
   Web of Science ®Google Scholar
• Gard JA, Taylor HFW, Staples LW. Studies in crystal structure using electron diffraction of single crystals. In: Bargmann W, Möllenstedt G, Niehrs H, et al. editors. Verhandlungen: physikalisch-Technischer teil. [Internet]. Berlin, Heidelberg: Springer; 1960. p. 449–453. Available from:
   Google Scholar
• Weise K, Ukrainczyk N, Koenders E. A mass balance approach for thermogravimetric analysis in pozzolanic reactivity R3 test and effect of drying methods. Materials. 2021;14(19):5859.
   PubMed Web of Science ®Google Scholar
• Bhat PA, Debnath NC. Theoretical and experimental study of structures and properties of cement paste: the nanostructural aspects of C–S–H. J Phys Chem Solids. 2011;8:920–933.
   Google Scholar
• Sun J, Shi H, Qian B, et al. Effects of synthetic C-S-H/PCE nanocomposites on early cement hydration. Constr Build Mater. 2017;140:282–292.
   Web of Science ®Google Scholar
• Jayapalan AR, Lee BY, Kurtis KE. Can nanotechnology be ‘green’? Comparing efficacy of nano and microparticles in cementitious materials. Cem Concr Compos. 2013;36:16–24.
   Web of Science ®Google Scholar
• Maheswaran S, Ramesh Kumar V, Bhuvaneshwari B, et al. Studies on lime sludge for partial replacement of cement. AMM. 2011;71–78:1015–1019.
   Google Scholar
• Mateo S, Cuevas M, La Rubia MD, et al. Preliminary study of the use of spent diatomaceous earth from the brewing industry in clay matrix bricks. Adv Appl Ceram. 2017;116(2):77–84.
   Web of Science ®Google Scholar
• Mejía JM, Mejía de Gutiérrez R, Montes C. Rice husk ash and spent diatomaceous earth as a source of silica to fabricate a geopolymeric binary binder. J Cleaner Prod. 2016;118:133–139.
   Web of Science ®Google Scholar
• Santos LF, dos Magalhães RS, Barreto SS, et al. Characterization and reuse of spent foundry sand in the production of concrete for interlocking pavement. J Build Eng. 2021;36:102098.
   Web of Science ®Google Scholar