131
Views
6
CrossRef citations to date
0
Altmetric
PHARMACEUTICAL ANALYSIS

Sensitive Analysis of Prednisolone and Prednisone in Human Plasma by Reverse Phase High-Performance Liquid Chromatography with Ultraviolet Detection

, &
Pages 1573-1585 | Received 11 Dec 2002, Accepted 27 Feb 2003, Published online: 18 Aug 2006

References

  • Frey , B.M. and Frey , F.J. 1990 . Clinical pharmacokinetics of prednisone and prednisolone . Clin. Pharmacokin. , 19 : 126 – 146 .
  • Jenkins , J.S. and Sampson , P.A. 1967 . Conversion of cortisone to cortisol and prednisone to prednisolone . Br. Med. J. , 2 : 205 – 207 .
  • Wagner , J.G. , DiSanto , A.R. , Gillespie , W.R. and Albert , K.S. 1981 . Reversible metabolism and pharmacokinetics: application to prednisone-prednisolone . Res. Commun. Chem. Pathol. Pharmacol. , 32 : 387 – 405 .
  • Garg , V. and Jusko , W.J. 1994 . Bioavailability and reversible metabolism of prednisone and prednisolone in man . Biopharm. Drug Dispos. , 15 : 163 – 172 .
  • Rose , J.Q. , Yurchak , A.M. and Jusko , W.J. 1981 . Dose-dependent pharmacokinetics of prednisone and prednisolone in man . J. Pharmacokin. Biopharm. , 9 : 389 – 417 .
  • Jusko , W.J. and Ludwig , E.A. 1992 . “ Corticosteroids ” . In Applied Pharmacokinetics Edited by: Evans , W.E. , Schentag , J.J. and Jusko , W.J. p. 27-1 – 27-34 . Vancouver, WA, , USA : Applied Therapeutics .
  • Ichimura , K. , Yamanaka , H. , Chiba , K. , Shinozuka , T. , Shiki , Y. , Saito , K. , Kusano , S. , Ameniya , S. , Oyama , K. , Nozaki , Y. and Kato , K. 1986 . Simultaneous quantitative measurement of fourteen adrenal steroids by capillary column gas chromatography-mass spectrometry, and its clinical application . J. Chromatogr. , 374 : 5 – 16 .
  • AI-Hakiem , M.H.H. and Abbas , S.J. 1987 . Simple adaptation of a radioimmunoassay kit for serum cortisol used to measure salivary cortisol . Clin. Chem. , 33 : 191 – 192 .
  • Monji , N. , Gomez , N.O. , Hawashima , H. , Alei , H. and Castro , A. 1980 . Practical enzyme immunoassay for plasma cortisol using beta-galactosidase as enzyme label . J. Clin. Endocrinol. Metab. , 50 : 355 – 359 .
  • Al-habet , S.M.H. and Rogers , H.J. 1989 . Two chromatographic methods for the determination of corticosteroids in human biological fluids: pharmacokinetic applications . J. Pharm. Sci. , 78 : 660 – 666 .
  • Frey , F.J. , Frey , B.M. and Benet , L.Z. 1979 . Liquid-chromatographic measurement of endogenous and exogenous glucocorticoids in plasma . Clin. Chem. , 25 : 1944 – 1947 .
  • Ui , T. , Mitsunaga , M. , Tanaka , T. and Horiguchi , M. 1982 . Determination of prednisone and prednisolone in human serum by high-performance liquid chromatography—especially on impaired conversion of corticosteroids in patients with chronic liver disease . J. Chromatogr. , 239 : 711 – 716 .
  • Garg , V. and Jusko , W.J. 1991 . Simultaneous analysis of prednisone, prednisolone and their major hydroxylated metabolites in urine by high-performance liquid chromatography . J. Chromatogr. , 567 : 39 – 47 .
  • Jusko , W.J. , Pyszczynski , N.A. , Bushway , M.S. , D'Ambrosio , R. and Mis , S.M. 1994 . Fifteen years of operation of a high-performance liquid chromatographic assay for prednisolone, cortisol and prednisone in plasma . J. Chromatogr. , 658 : 47 – 54 .
  • Döppenschmitt , S.A. , Scheidel , B. , Harrison , F. and Surmann , J.P. 1995 . Simultaneous determination of prednisolone, prednisolone acetate and hydrocortisone in human serum by high-performance liquid chromatography . J. Chromatogr. , 674 : 237 – 246 .
  • Goto , J. , Shamsa , F. , Goto , N. and Nambara , T. 1983 . The simultaneous determination of serum cortisol and cortisone by high-performance liquid chromatography with fluorimetric detection . J. Pharm. Biomed. Anal. , 1 : 83 – 88 .
  • Shibata , N. , Hayakawa , T. , Takada , K. , Hoshino , N. , Minouchi , T. and Yamaji , A. 1998 . Simultaneous determination of glucocorticoids in plasma or urine by high-performance liquid chromatography with precolumn fluorimetric derivatization by 9-anthroyl nitrile . J. Chromatogr. , 706 : 191 – 199 .
  • Hirata , H. , Kasama , T. , Sawai , Y. and Fike , R.R. 1994 . Simultaneous determination of deflazacort metabolites II and III, cortisol, cortisone, prednisolone and prednisone in human serum by reverse-phase high-performance liquid chromatography . J. Chromatogr. , 658 : 55 – 61 .
  • Huber , F. , Wiedemann , M. , Heinrich , G. , Salama , Z. and Jaeger , H. 1990 . Development of a high performance liquid chromatography method for the simultaneous measurement of prednisone and prednisolone . Arzneim.-Forsch/Drug Res. , 40 : 926 – 931 .
  • Cheng , M.H. , Huang , W.Y. and Lipsey , A.I. 1988 . Simultaneous liquid-chromatographic determination of prednisone and prednisolone in plasma . Clin. Chem. , 34 : 1897 – 1899 .
  • Majid , O. , Akhlaghi , F. , Lee , T. , Holt , D.W. and Trull , A. 2001 . Simultaneous determination of plasma prednisolone, prednisone, and cortisol levels by high-performance liquid chromatography . Ther. Drug Monit. , 23 : 163 – 168 .
  • Kames , H.T. , Shiu , G. and Shah , V.P. 1991 . Validation of bioanalytical methods . Pharm. Res. , 8 : 421 – 426 .
  • Rohatagi , S. , Barth , J. , Möllmann , H. , Hochhaus , G. , Soldner , A. , Möllmann , C. and Derendorf , H. 1997 . Pharmacokinetics of methylprednisolone and prednisolone after single and multiple oral administration . J. Clin. Pharmacol. , 37 : 916 – 925 .

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.