References and Notes
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- Inouye , S. , Tsuruoka , T. , Ito , T. and Niida , T. 1968 . Structure and synthesis of nojirimycin . Tetrahedron , 24 ( 5 ) : 2125 – 2144 .
- Nayak , U. G. and Whistler , R. L. 1969 . Synthesis of 5‐thio‐D‐glucose . J. Org. Chem. , 34 ( 1 ) : 97 – 100 .
- Yamashita , M. , Yamada , M. , Sugiura , M. , Nomoto , H. and Oshikawa , T. 1987 . Functional group interconversion of a β‐nitro group of phosphorus compounds and synthesis of some phosphino sugars . Nippon Kagaku Kaishi , : 1207 – 1213 .
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- Crystal data of 6a: C12H14O5PBr, M = 349.12, colorless, prismatic, 0.30 × 0.30 × 0.20 mm, orthorhombic, Pna2 1 (no. 33), a = 7.016(4) Å, b = 18.560(5) Å, c = 11.003(4) Å, T = 296 K, Observations [I > 3.00σ(I)] = 847, Variables = 193, Reflection/Parameter ratio = 4.39, R, Rw = 0.067, 0.049. Full crystallographic data (excluding structure factors) have been deposited with the Cambridge Crystallographic Data Center. Copies may be requested free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK [fax: +44(0)‐1223‐336033, or e-mail: [email protected]]
- Cha , J. K. , Christ , W. J. and Kishi , Y. 1984 . On stereochemistry of osmium tetraoxide oxidation of allylic alcohol systems. Empirical rule . Tetrahedron , 40 ( 12 ) : 2247 – 2255 .