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- Preliminary characterization data obtained on un-desalted 5: 1H NMR (D2O) δ 6.07 (s, 1, H5), 5.97 (s, 1, CH(OD)2), 5.92 (d, ÷ = 4Hz, 1, H1′), 4.40 (m, 1, H3′), 4.01 (m, 1, H4′), 3.87 (m, 2, 5′-CH2). 13C NMR (D2O) δ 166 (C4), 156 and 152 (C2/C6), 101 (C5), 92 (C1′), 86 (CH(OD)2), 82 (C4′), 72 (C2′), 69 (C3′), 64 (C5′). Low resolution DCI (direct current ionization) mass spectrum, m/e: 213 (phosphoribosyl-H+H+)