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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 33, 2003 - Issue 4
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Original Articles

Reaction of Resorcinol with Mesityl Oxide: Synthesis of 2,2-Dimethyl-4-formyl- 7-methoxy-(2H)-1-benzopyran

A. K. Tripathi Regional Research Laboratory (CSIR), Jammu Tawi, India
,
K. R. Khan Barkatulla University, Bhopal, M.P., India
&
S. C. Taneja Regional Research Laboratory (CSIR), Jammu Tawi, IndiaCorrespondence[email protected]
Pages 579-585 | Received 08 Oct 2001, Published online: 16 Aug 2006

References

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  • Kondrat'eva , G.G. , Volkotrub , M.N. and Sin . 1969 . Issled. Eff. Khim Dobavok. Structure and conversion of the products of condensation of mesityl oxide with o-cresol and resorcinol . Polim. Mater. , 2 : 373 Chem. Abstr. 1972, 76, 59369z
  • Starkov , S.P. and Glushkova , L.V. 1968 . Structure and reactions of the condensation products of phenols and unsaturated carbonyl compounds: condensation of 3,4-xylenol with crotonaldehyde . Khim. Kreterotsiki. Soedin , 1 : 16 Chem. Abstr. 1968, 69, 77054c
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  • Mitsui Petrochemical Ind. Co. Ltd. Jpn Patents JP 82,16877 . 1982 . 2,4,4-Trimethyl-2-(2,4-dihydroxyphenyl)-7-hydroxy chroman, Chem. Abstr. 1982, 97, 6153b
  • JP 82,114,585 . 1982 . 2,4,4-Trimethyl-2-(2,4-dihydroxy phenyl)-7-hydroxy chroman. Chem. Abstr. 1982, 97, 216003d
  • Livant , P. , Web , T.R. and Xu , W. 1997 . Reaction of resorcinol with acetone . J. Org. Chem. , 62 : 737
  • Livant , P. and Xu , W. 1998 . Reaction of resorcinol with α-β-unsaturated ketones . J. Org. Chem. , 63 : 636
  • Reaction carried out at 35°C in presence of diethyl ether
  • Reaction at room temperature with constant stirring
  • Reaction carried out at 60°C with stirring

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