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- Zinc thiocyanate was prepared by stirring anhydrous potassium thiocyanate (4.08 g 42 mmol) with anhydrous zinc chloride (2.86 g, 21 mmol) in refluxing benzene (40 mL) for 8 h. Solvent was then decanted off and salts after initial drying in a flash evaporator, stored in a vaccum desiccator over fused calcium chloride