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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 33, 2003 - Issue 20
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Original Articles

A Novel and Efficient Strategy for the Preparation of 2,4-Disubstituted-1,2,3-triazoles

Yun Luo Department of Medicinal Chemistry, School of Pharmaceutical Science, Zhejiang University, Hangzhou, P.R. China
&
Yongzhou Hu Department of Medicinal Chemistry, School of Pharmaceutical Science, Zhejiang University, Hangzhou, P.R. ChinaCorrespondence[email protected]
Pages 3513-3517 | Received 28 Feb 2003, Published online: 15 Aug 2006

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  • For compound 3a IR (KBr, cm−1): 1471, 1377, 829. 1H NMR (400 MHz,CDCl3, ppm) δ: 7.79 (s, 1H, =CH), 7.70 (m, 2H, Ar-H), 7.39 (m, 2H, Ar-H), 4.23 (s, 3H, CH3). Anal. calcd. for C9H8N3Cl: C 55.83, H 4.16, N 21.70. Found: C 55.69, H 4.01, N 21.45. For compound 3o. IR (KBr, cm−1): 2923, 2853, 1614, 1547, 1495, 1453, 1376, 1030, 997, 830. 1H NMR (400 MHz,CDCl3, ppm) δ: 8.09 (m, 2H, Ar-H), 8.00 (s, 1H, =CH), 7.84 (m, 2H, Ar-H), 7.48 (m, 2H, Ar-H), 7.02 (m, 2H, Ar-H), 3.89 (s, 3H, CH3O). Anal. calcd. for C15H12N3Cl: C 66.79, H 4.45, N 15.58. Found: C 66.62, H 4.41, N 15.52

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