Efficient Microscale Preparation of Isotopically Enriched 1‐[⁷⁹Br]Bromo‐2‐Fluoroethylene, [⁷⁹Br]BrHC˭CHF

References

• Lide , D. R. 1998 . CRC Handbook of Chemistry and Physics 1 – 11 . New York : CRC Press Inc. .
   Google Scholar
• Shimada , J. , Tatamitani , Y. , Liu , B. and Ogata , T. 2002 . Microwave spectra, structures, and nuclear quadruple coupling constants of bromofluoroethenes: BrFC˭CH2, cis‐BrHC˭CHF and trans‐BrHC˭CHF . J. Mol. Struct. , 612 : 155 – 166 .
   Google Scholar
• Baldacci , A. , Stoppa , P. , Pietropolli Charmet , A. , Scaranto , J. and Gambi , A. 2004 . Experimental and theoretical studies of the vibrational spectra of cis‐1‐bromo‐2‐fluoroethene . Spectrochim. Acta , 60A : 1967 – 1975 .
   Google Scholar
• Swarts , F. 1897 . Sur quelques dérivés fluobromés en C2 (première communication) . Bull. Acad. Roy. Belg. , 33 : 439 – 474 .
   Google Scholar
• Swarts , F. 1897 . Chem. Zentr. , II : 1098 – 1099 .
   Google Scholar
• Swarts , F. 1909 . Sur le dibromfluoréthane et le bromfluoréthylène dissymétrique . Bull. Acad. Roy. Belg. , : 728 – 743 .
   Google Scholar
• Swarts , F. 1919 . Action du bromure de phénylmagnesium sur les dérivés polyhalogénés de l'éthane . Bull. Soc. Chim. Fr. , 25 : 145 – 174 .
   Google Scholar
• Drakesmith , F. G. , Richardson , R. D. , Steward , O. J. and Tarrant , P. 1968 . The preparation and reactions of some fluorine‐containing vinyl organometallic compounds . J. Org. Chem. , 33 : 286 – 291 .
   Google Scholar
• Edamura , K. and Ishikawa , N. 1978 . Formation of bromofluoroethylenes by elimination of hydrogen bromide from 1,2‐dibromo‐1‐fluoroethane . Nippon Kagaku Kaishi , 8 : 1173 – 1175 .
   Google Scholar
• Viehe , H. G. , Dale , J. and Franchimont , E. 1964 . Die isomerenverhaltnisse beim 2‐fluor‐1‐jod‐athylen . Ber. , 97 : 244 – 248 .
   Google Scholar
• Viehe , H. G. , Franchimont , E. , Reinstein , M. and Valange , P. 1960 . Geometrische isomerenpaare mit bevorzugter cis‐structur . Chem. Ber. , 93 : 1697 – 1709 .
   Google Scholar
• Baciocchi , E. 1983 . “ 1,2‐Dehalogenations and related reactions ” . In The Chemistry of Functional Groups, Supplement D, Vol. 1: The Chemistry of Halides, Pseudo‐halides and Azides Edited by: Patai , S. and Rappoport , Z. 161 – 201 . New York : Wiley .
   Google Scholar
• Totten , L. A. , Jans , U. and Roberts , L. A. 2001 . Alkyl bromides as mechanistic probes of reductive dehalogenation: Reactions of vicinal dibromide stereoisomers with zerovalent metals . Environ. Sci. Technol. , 35 : 2268 – 2274 .
   PubMedGoogle Scholar
• Shainyan , B. A. 1990 . Free‐radical thiylation of fluorobromoethylenes . Sulfur Letters , 11 : 109 – 116 .
   Google Scholar
• Baldan , A. 2004 . Microscale preparation of isotopically enriched 37ClHC˭CHF . Synth. Commun. , 34 : 1229 – 1235 .
   Web of Science ®Google Scholar
• Baldacci , A. , Baldan , A. , Gambi , A. and Stoppa , P. 2000 . The vibrational spectra and normal coordinates analysis of bromofluoromethane, CH2 BrF . J. Mol. Struct. , 517–518 : 197 – 208 .
   Web of Science ®Google Scholar
• Smith , L. G. 1949 . The infrared spectrum of C2 H6 . J. Chem. Phys. , 17 : 139 – 167 .
   Google Scholar
• Bak , B. and Christensen , D. 1958 . Infrared absorption spectra of deuterated vinyl fluorides . Spectrochim. Acta , 12 : 355 – 369 .
   Google Scholar
• McKean , D. C. 1975 . CH stretching frequencies, bond lengths and strengths in halogenated ethylenes . Spectrochim. Acta , 31A : 1167 – 1186 .
   Google Scholar
• Smith , D. C. and Saunders , R. A. 1952 . Infrared and Raman spectra of fluorinated ethanes. IV. The series CH3‐CH3, CH3‐CHF2 and CH3‐CF3 . J. Chem. Phys. , 20 : 847 – 859 .
   Web of Science ®Google Scholar