96
Views
13
CrossRef citations to date
0
Altmetric
Original Articles

Determination of Linalool in Different Hop Varieties Using a New Method Based on Fluidized-Bed Extraction with Gas Chromatographic-Mass Spectrometric Detection

, , , , , , & show all

References

  • Abbas, K. A., Mohamed, A., Abdulamir, A. S., and Abas, H. A. A review on supercritical fluid extraction as new analytical method. Am. J. Biochem. Biotechnol. 4:345–353, 2008.
  • Aberl, A., and Coelhan, M. Determination of volatile compounds in different hop varieties by headspace-trap GC/MS—In comparison with conventional hop essential oil analysis. J. Agric. Food Chem. 60:2785–2792, 2012.
  • American Society of Brewing Chemists. Methods of Analysis. Method Hops-13, Total essential oils in hops and hop pellets by steam distillation. The Society, St. Paul, MN, 2009. http://dx.doi.org/10.1094/ASBCMethod-Hops13
  • Anioł, M., Huszcza, E., Bartmahska, A., Żołnierczyk, A., Mąoczka, W., and Wawrzeńczyk, C. Trace analysis of hop essential oils in spent hop. J. Am. Soc. Brew. Chem. 65:214–218, 2007.
  • Basařová, G., Šavel, J., Basař, P., and Lejsek, T. Chapter 1 in: Brewery: Theory and Practice Beer Production (in Czech). VŠCHT Prague, 2010.
  • Briggs, D. E., Boulton, C. A., Brookes, P. A., and Stevens, R. The chemistry of hop constituents. Chapter 8 in: Brewing: Science and Practice. CRC Press, New York, 2004.
  • České odrůdy chmele (Czech Hop Varieties). Hop Research Institute, Žatec, 2012. ISBN 978-80-87357-11-8
  • Esslinger, H. M. Polyphenols. Chapter 3.3.3 in: Handbook of Brewing. Wiley-VCH Verlag, Weinheim, 2009. ISBN 978-3-527-31674-8
  • European Brewery Convection. Analytica-EBC. Methods 7.1, Sampling of hops and hop products; 7.7, α- and ß-acids in hop and hop products by HPLC; 7.12, Hop essential oils by capillary gas chromatography flame ionization detection. Fachferlag Hans Carl, Nürnberg, Germany, 2006.
  • Field, J. A., Nickerson, G., James, D. D., and Heider, C. Determination of essential oils in hops by headspace solid-phase microextraction. J. Agric. Food Chem. 44:1768–1772, 1996.
  • Fritsch, H. T, and Schieberle, P. Identification based on quantitative measurements and aroma recombination of the character impact odorants in a Bavarian pilsner-type beer. J. Agric. Food Chem. 53:7544–7551, 2005.
  • Goiris, K., De Ridder, M., De Rouck, G., Boeykens, A., Van Opstaele, F, Aerts, G., De Cooman, L., and De Keukeleire, D. The oxygenated sesquiterpenoid fraction of hops in relation to the spicy hop character of beer. J. Inst. Brew. 108:86–93, 2002.
  • Hanke, S., Herrmann, M., Rückerl, J., Schönberger, C, and Back, W. Hop volatile compounds (Part II): Transfer rates of hop compounds from hop pellets to wort and beer. Brew. Sci. 61:140–147, 2008.
  • Hanke, S., Kern, M., Herrmann, M., Back, W., Becker, T, and Krottenthaler, M. Suppression of gushing by hop constituents. Brew. Sci. 62:181–186, 2009.
  • Hanke, S., Ditz, V., Herrmann, M., Back, W., Becker, T, and Krottenhaler, M. Influence of ethyl acetate, isoamyl acetate and linalool on off-flavour perception in beer. Brew. Sci. 63:94–99, 2010.
  • Hanke, S., Ditz, V., Herrmann, M., Back, W., and Krottenhaler, M. How fermentation by-products and linalool affect off-flavours—Part 1. Brauwelt Int. 32:157–158, 2014.
  • Jelínek, L., Šneberger, M., Karabín, M., and Dostálek, P. Comparison of Czech hop cultivars based on their contents of secondary metabolites. Czech J. Food Sci. 28:309–316, 2010.
  • Jelínek, L., Dolečková, M., Hudcová, T, Karabín, M., and Dostálek, P. Profilling of Czech hop varieties by means of analyses of α- and ß-bitter acids, essential oils and polyphenols. Kvasny Prum. 57:272–276, 2011.
  • Kaltner, D., Steinhaus, M., Mitter, W., Biendl, M., and Schieberle, P. (R)-Linalool as key flavour for hop aroma in beer and its behaviour during beer staling. Monatsschr. Brauwiss. 56:192–196, 2003.
  • King, A., and Dickinson, J. R. Biotransformation of monoterpen alcohols by Saccharomyces cerevisiae, Torulaspora delbrueckii and Kluyveromyces lactis. Yeast 16:499–506, 2000.
  • Kovačevič, M., and Kač, M. Solid-phase microextraction of hop volatiles: Potential use for determination and verification of hop varieties. J. Chromatogr. A 918:159–167, 2001.
  • Kovačevič, M., and Kač, M. Determination and verification of hop varieties by analysis of essential oils. Food. Chem. 77:489–494, 2002.
  • Lermusieau, G., and Collin, S. Varietal discrimination of hop pellets. II. Comparison between fresh and aged samples. J. Am. Soc. Brew. Chem. 59:39–43, 2001.
  • Li, H.-J., and Deinzer, M. L. Structural identification and distribution of proanthocyanidins in 13 different hops. J. Agric. Food Chem. 54:4048–4056, 2006.
  • McLaughlin, I. R., Lederer, C, and Shellhammer, T. H. Bitternessmodifying properties of hop polyphenols extracted from spent hop material. J. Am. Soc. Brew. Chem. 66:174–183, 2008.
  • Mikyška, A., Hrabák, M., Hašková, D., and Šrogl, J. The role of malt and hop polyphenols in beer quality, flavour and haze stability. J. Inst. Brew. 108:78–86, 2002.
  • Mikyška, A., and Jurková, M. Evaluation of bitter acids and polyphenols content in Czech hops harvest in 2013—I: Contents of α-and ß-bitter acids. Kvasny Prum. 60:88–95, 2014.
  • Nijssen, L. M., Visscher, C. A., Maarse, H., Willemsens, L. C, and Boelens, M. H. Volatile compounds in food. Qualitative and quantitative data: Hop oil. No. 62. Central Institute for Nutrition and Food Research, Zeist, The Netherlands, 1996.
  • Olšovská, J., Kameník, Z., Čejka, P., Jurková, M., and Mikyška, A. Ultra-high-performance liquid chromatography profiling method for chemical screening of proanthocyanidins in Czech hops. Talanta 116:919–926, 2013.
  • Peana, A. T, D'Aquila, P. S., Panin, F, Serra, G., Pippia, P., and Moretti, M. D. L. Anti-inflammatory activity of linalool and linalyl acetate constituents of essential oils. Phytomedicine 9:721–726, 2002.
  • Perpète, P., Mélotte, L., Dupire, S., and Collin, S. Varietal discrimination of hop pellets by essential oil analysis. I. Comparison of fresh samples. J. Am. Soc. Brew. Chem. 56:104–108, 1998.
  • Rettberg, N., Thörner, S., and Garbe, L.-A. Bugging hop analysis—On the isomerization and oxidation of terpene alcohols during steam distillation. Brew. Sci. 65:112–117, 2012.
  • Saison, D., De Schutter, D. P., Delvaux, F, and Delvaux, F. R. Optimisation of a complete method for the analysis of volatiles involved in the flavour stability of beer by solid-phase microextraction in combination with gas chromatography and mass spectrometry. J. Chromatogr. A 1190:342–349, 2008.
  • Steinhaus, M., and Schieberle, P. Comparison of the most odor-active compounds in fresh and dried hop cones (Humulus lupulus L. variety Spalter Select) based on GC-olfactometry and odor dilution techniques. J. Agric. Food Chem. 48:1776–1783, 2000.
  • Steinhaus, M., Wilhelm, W., and Schieberle, P. Comparison of the most odor-active volatiles in different hop varieties by application of a comparative aroma extract dilution analysis. Eur. Food Res. Technol. 226:45–55, 2007.
  • Takoi, K., Koie, K., Itoga, Y., Katayama, Y, Shimase, M., Nakayama, Y, and Watari, J. Biotransformation of hop-derived monoterpene alcohols by lager yeast and their contribution to the flavour of hopped beer. J. Agric. Food Chem. 58:5050–5058, 2010.
  • Vázquez-Araújo, L., Rodríguez-Solana, R., Cortés-Diéguez, S. M., and Domínguez, J. M. Use of hydrodistillation and headspace solidphase microextraction to characterize the volatile composition of different hop cultivars. J. Sci. Food Agric. 93:2568–2574, 2013.

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.