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- The synthesis of sulfonium methylketones parallels that of Shaw,20 namely alkylation of dialkyl sulfides by bromomethylketones 27 In our approach however, bromomethylketones were prepared by direct derivatization of the precursor acids, the intermediate diazomethylketones were not isolated.28 Our methods also differ in the preparation of sulfonium tetrafluoroborates which are again obtained by an alkylation procedure. N-protected acids were prepared by classical procedures (jbc036)