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Original Articles

A Fourier Transform Infrared Spectroscopy Method for Analysis of Palm Oil Adulterated with Lard in Pre-Fried French fries

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Pages 354-362 | Received 31 Jul 2011, Accepted 15 Sep 2011, Published online: 03 Oct 2013
 

Abstract

Fourier transform infrared spectroscopy with attenuated total reflectance accessory was used to detect the presence of lard in French fries pre-fried in palm oil adulterated with lard. A Fourier transform infrared calibration model was obtained using partial least squares for prediction of lard in a blend mixture of lard and palm oil. The coefficient of determination (R2) of 0.9791 was obtained with 0.5% of detection limit. The error in calibration expressed with root mean square error of calibration was 0.979%. In addition, the error obtained during cross validation was 2.45%. A discriminant analysis test was able to distinguish between fries samples adulterated with lard and samples, which were pre-fried with palm oils. Fourier transform infrared spectroscopy is a fast and powerful technique for quantification of lard present in French fries.

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