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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 45, 2015 - Issue 4
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Original Articles

Efficient and Green Microwave-Assisted Multicomponent Biginelli Reaction for the Synthesis of Dihydropyrimidinones Catalyzed by Heteropolyanion-Based Ionic Liquids Under Solvent-Free Conditions

Renzhong FuJiangsu Laboratory of Advanced Functional Material, School of Chemistry and Materials Engineering, Changshu Institute of Technology, Changshu, Jiangsu, China
,
Yang YangJiangsu Laboratory of Advanced Functional Material, School of Chemistry and Materials Engineering, Changshu Institute of Technology, Changshu, Jiangsu, ChinaCorrespondence[email protected] [email protected]
,
Wenchen LaiJiangsu Laboratory of Advanced Functional Material, School of Chemistry and Materials Engineering, Changshu Institute of Technology, Changshu, Jiangsu, China
,
Yongfeng MaJiangsu Laboratory of Advanced Functional Material, School of Chemistry and Materials Engineering, Changshu Institute of Technology, Changshu, Jiangsu, China
,
Zhikai ChenJiangsu Laboratory of Advanced Functional Material, School of Chemistry and Materials Engineering, Changshu Institute of Technology, Changshu, Jiangsu, China
,
Jian ZhouJiangsu Laboratory of Advanced Functional Material, School of Chemistry and Materials Engineering, Changshu Institute of Technology, Changshu, Jiangsu, China
,
Wen ChaiJiangsu Laboratory of Advanced Functional Material, School of Chemistry and Materials Engineering, Changshu Institute of Technology, Changshu, Jiangsu, China
,
Quan WangJiangsu Laboratory of Advanced Functional Material, School of Chemistry and Materials Engineering, Changshu Institute of Technology, Changshu, Jiangsu, ChinaCorrespondence[email protected] [email protected]
&
Rongxin YuanJiangsu Laboratory of Advanced Functional Material, School of Chemistry and Materials Engineering, Changshu Institute of Technology, Changshu, Jiangsu, China
 show all
Pages 467-477 | Received 03 Sep 2014, Published online: 21 Dec 2014

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Behzad Mohammadi, Farahnaz K. Behbahani, Gholam B. Marandi & Behrouz Mirza. (2021) One-pot synthesis of 3,4-dihydropyrimidin-2(1H)-ones, thiones and 2-selenoxo DHPMs using 1-butyl-3-methylimidazolium hydrogen sulfate as non-halogenated ionic liquid. Phosphorus, Sulfur, and Silicon and the Related Elements 196:1, pages 54-60.
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Sanjay K. Rathwa, Mahesh S. Vasava, Manoj N. Bhoi, Mayuri A. Borad & Hitesh D. Patel. (2018) Recent advances in the synthesis of C-5-substituted analogs of 3,4-dihydropyrimidin-2-ones: A review. Synthetic Communications 48:9, pages 963-994.
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Karuppaiah Selvakumar, Thangamariyappan Shanmugaprabha, Murugan Kumaresan & Ponnusamy Sami. (2018) Heteropoly acid supported on activated natural clay-catalyzed synthesis of 3,4-dihydropyrimidinones/thiones through Biginelli reaction under solvent-free conditions. Synthetic Communications 48:2, pages 223-232.
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Yi-Ming Ren, Ze Zhang & Shuo Jin. (2016) Convenient and efficient method for synthesis of 2,4,6-triarylpyridines using catalytic amount of PEG1000-based dicationic acidic ionic liquid under solvent-free conditions. Synthetic Communications 46:6, pages 528-535.
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Rajendra Patil, Jagdish Chavan, Shivnath Patel, Vaishali Shinde & Anil Beldar. (2022) Mild Acidic Charcoal Catalyzed Synthesis of 3,4-dihydropyrimidin-2(1H)-one/-thione Derivatives. Chemistry Journal of Moldova 17:2, pages 101-108.
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B. Mohammadi, F. K. Behbahani, G. B. Marandi & B. Mirza. (2022) Synthesis of 3,4-Dihydropyrimidin-2(1H)-ones, -thione, and -selones, Catalyzed by TiO2 Nanoparticles. Russian Journal of Organic Chemistry 58:9, pages 1319-1326.
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GOBIND KUMAR, GAURAV BHARGAVA, YOGESH KUMAR & RUPESH KUMAR. (2022) Eosin Y photocatalyzed access to Biginelli reaction using primary alcohols via domino multicomponent cascade: an approach towards sustainable synthesis of 3,4-dihydropyrimidin-2(1H)-ones. Journal of Chemical Sciences 134:2.
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Lakha V. Chopda & Pragnesh N. Dave. (2021) 12-Phosphomolybdic acid H3[PMo12O40] over natural bentonite as a heterogeneous catalyst for the synthesis of 3,4-dihydropyrimidin-2-(1H)-ones. Results in Chemistry 3, pages 100169.
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Árpád Molnár. 2021. Green Sustainable Process for Chemical and Environmental Engineering and Science. Green Sustainable Process for Chemical and Environmental Engineering and Science 51 203 .
Asif A. Malik, Nisar A. Dangroo & Tabassum Ara. (2020) Microwave‐Assisted Tandem Kornblum Oxidation and Biginelli Reaction for the Synthesis of Dihydropyrimidones. ChemistrySelect 5:42, pages 12965-12970.
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Lakha V. Chopda & Pragnesh N. Dave. (2020) Recent Advances in Homogeneous and Heterogeneous Catalyst in Biginelli Reaction from 2015‐19: A Concise Review. ChemistrySelect 5:19, pages 5552-5572.
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Jaleel Fairoosa, Salim Saranya, Sankaran Radhika & Gopinathan Anilkumar. (2020) Recent Advances in Microwave Assisted Multicomponent Reactions. ChemistrySelect 5:17, pages 5180-5197.
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Leqin He, Shenjun Qin, Jianjun Liu, Wei Zhao & Tao Chang. (2020) Long-chain Brønsted acidic ionic liquids catalyzed one-pot three-component Biginelli reaction. World Journal of Engineering 17:1, pages 21-26.
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Majid Heravi & Vahideh Zadsirjan. 2020. Recent Advances in Applications of Name Reactions in Multicomponent Reactions. Recent Advances in Applications of Name Reactions in Multicomponent Reactions 15 138 .
Venkata Durga Nageswar Yadavalli & Jayathirtha Rao Vaidya. 2020. Nanotechnology-Based Industrial Applications of Ionic Liquids. Nanotechnology-Based Industrial Applications of Ionic Liquids 311 352 .
Mariana Matias, Gonçalo Campos, Adriana O. Santos, Amílcar Falcão, Samuel Silvestre & Gilberto Alves. (2019) Synthesis, in vitro evaluation and QSAR modelling of potential antitumoral 3,4-dihydropyrimidin-2-(1H)-thiones. Arabian Journal of Chemistry 12:8, pages 5086-5102.
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Elena Cini & Maurizio Taddei. 2019. Green Synthetic Processes and Procedures. Green Synthetic Processes and Procedures 216 244 .
Rajendra V. Patil, Jagdish U. Chavan, Dipak S. Dalal, Vaishali S. Shinde & Anil G. Beldar. (2019) Biginelli Reaction: Polymer Supported Catalytic Approaches. ACS Combinatorial Science 21:3, pages 105-148.
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Majid Momahed Heravi, Vahideh Zadsirjan, Malihe Mollaiye, Masumeh Heydari & Afsaneh Taheri Kal Koshvandi. (2018) Salicylaldehydes as privileged synthons in multicomponent reactions. Russian Chemical Reviews 87:6, pages 553-585.
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Renzhong Fu, Yang Yang, Xudong Ma, Yu Sun, Jin Li, Hang Gao, Huaxing Hu, Xiaojun Zeng & Jun Yi. (2017) An Efficient, Eco-friendly and Sustainable One-Pot Synthesis of 3,4-Dihydropyrimidin-2(1H)-ones Directly from Alcohols Catalyzed by Heteropolyanion-Based Ionic Liquids. Molecules 22:9, pages 1531.
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Barbara Floris, Federica Sabuzi, Pierluca Galloni & Valeria Conte. (2017) The Beneficial Sinergy of MW Irradiation and Ionic Liquids in Catalysis of Organic Reactions. Catalysts 7:9, pages 261.
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M. Afradi, N. Foroughifar, H. Pasdar, H. Moghanian & N. Foroughifar. (2017) Facile green one-pot synthesis of novel thiazolo[3,2-a]pyrimidine derivatives using Fe 3 O 4 @ l -arginine and their biological investigation as potent antimicrobial agents . Applied Organometallic Chemistry 31:9, pages e3683.
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Ali Maleki, Abbas Ali Jafari & Somayeh Yousefi. (2017) MgFe2O4/cellulose/SO3H nanocomposite: a new biopolymer-based nanocatalyst for one-pot multicomponent syntheses of polysubstituted tetrahydropyridines and dihydropyrimidinones. Journal of the Iranian Chemical Society 14:8, pages 1801-1813.
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Ayhan Yıldırım & Yunus Kaya. (2017) Sustainable synthetic approaches using [C16Im][Oxa] as a flexible organocatalyst and DFT studies toward 3,4-dihydropyrimidinones and benzoxazines. Monatshefte für Chemie - Chemical Monthly 148:6, pages 1085-1094.
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Renzhong Fu, Yang Yang, Wei Feng, Qiuxia Ge, Yan Feng, Xiaojun Zeng, Wen Chai, Jun Yi & Rongxin Yuan. (2016) An efficient, eco-friendly and sustainable tandem oxidative amidation of alcohols with amines catalyzed by heteropolyanion-based ionic liquids via a bifunctional catalysis process. Tetrahedron 72:50, pages 8319-8326.
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Arpit Kumar Pathak, Chetna Ameta, Rakshit Ameta & Pinki B. Punjabi. (2016) Microwave-Assisted Organic Synthesis in Ionic Liquids. Journal of Heterocyclic Chemistry 53:6, pages 1697-1705.
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Bin-Bin Feng, Rong-Zhang Jin, Mei-Mei Zhang & Xiang-Shan Wang. (2016) Green Synthesis of Spiro[indoline-3,4′-pyrazolo[3,4- b ][1,6]naphthyridine]-2,5′(1′ H )-diones Catalyzed by TsOH in Ionic Liquids . Journal of Heterocyclic Chemistry 53:5, pages 1578-1583.
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Hemantkumar M. Savanur, Rajesh G. Kalkhambkar, Gopalakrishnan Aridoss & Kenneth K. Laali. (2016) [bmim(SO 3 H)][OTf]/[bmim][X] and Zn(NTf 2 ) 2 /[bmim][X] (X = PF 6 and BF 4 ); efficient catalytic systems for the synthesis of tetrahydropyrimidin-ones (-thiones) via the Biginelli reaction. Tetrahedron Letters 57:27-28, pages 3029-3035.
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Kamal Mohammadi, Farhad Shirini & Asieh Yahyazadeh. (2015) 1, 3-Disulfonic acid imidazolium hydrogen sulphate as an efficient and reusable ionic liquid for the multicomponent synthesis of polyhydroquinoline derivatives under solvent-free conditions. Research on Chemical Intermediates 42:3, pages 2047-2054.
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Renzhong Fu, Yang Yang, Weihua Jin, Hui Gu, Xiaojun Zeng, Wen Chai, Yunsheng Ma, Quan Wang, Jun Yi & Rongxin Yuan. (2016) Microwave-assisted heteropolyanion-based ionic liquid promoted sustainable protocol to N-heteroaryl amides via N-directing dual catalyzed oxidative amidation of aldehydes. RSC Advances 6:109, pages 107699-107707.
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Renzhong Fu, Yang Yang, Jin Zhang, Jintao Shao, Xuming Xia, Yunsheng Ma & Rongxin Yuan. (2016) Direct oxidative amidation of aldehydes with amines catalyzed by heteropolyanion-based ionic liquids under solvent-free conditions via a dual-catalysis process. Organic & Biomolecular Chemistry 14:5, pages 1784-1793.
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Nóra Zs. Kiss, Erika Bálint & György Keglevich. 2016. Milestones in Microwave Chemistry. Milestones in Microwave Chemistry 11 45 .
Renzhong Fu, Yang Yang, Yunsheng Ma, Fei Yang, Jingjing Li, Wen Chai, Quan Wang & Rongxin Yuan. (2015) Microwave-promoted direct amidation of unactivated esters catalyzed by heteropolyanion-based ionic liquids under solvent-free conditions. Tetrahedron Letters 56:30, pages 4527-4531.
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Renzhong Fu, Yang Yang, Wenchen Lai, Yongfeng Ma, Zhikai Chen, Jian Zhou, Wen Chai, Quan Wang & Rongxin Yuan. (2015) ChemInform Abstract: Efficient and Green Microwave‐Assisted Multicomponent Biginelli Reaction for the Synthesis of Dihydropyrimidinones Catalyzed by Heteropolyanion‐Based Ionic Liquids under Solvent‐Free Conditions.. ChemInform 46:23.
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