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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 24, 1994 - Issue 8
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Original Articles

A Convenient Synthesis of Isothiocyanates from Primary Nitroalkanes

Jae Nyoung Kim Korea Research Institute of Chemical Technology, P. O. Box 9, Daedeog-Danji, Daejeon, 305-606, Korea
,
Jong Hwan Song Korea Research Institute of Chemical Technology, P. O. Box 9, Daedeog-Danji, Daejeon, 305-606, Korea
&
Eung K. Ryu Korea Research Institute of Chemical Technology, P. O. Box 9, Daedeog-Danji, Daejeon, 305-606, Korea
Pages 1101-1105 | Received 21 Sep 1993, Published online: 23 Sep 2006

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Prasanna Babu Racheeti, Ratna Babu Gunturu, Srinivasa Rao Pinapati, Anitha Kowthalam, Ramana Tamminana & Rameshraju Rudraraju. (2023) Hypervalent iodine(III) promoted synthesis of isothiocyanates in water. Synthetic Communications 53:1, pages 23-31.
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Nitin Srivastava. (2021) Tetrabutylammonium Iodide/I2 Mediated Convenient and Green Synthesis of Substituted Organic Isothiocyanates. Organic Preparations and Procedures International 53:6, pages 562-570.
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A. C. Chaskar, B. P. Bandgar, R. K. Modhave, A. B. Patil & S. Yewale. (2009) Novel Synthesis of Anthelmintic Drug 4-Isothiocyanato-4′-nitrodiphenyl Ether and Its Analogs. Synthetic Communications 39:6, pages 992-1001.
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Gaofeng Bian, Huayu Qiu, Jianxiong Jiang, Jirong Wu & Guoqiao Lai. (2007) A New Method for the Synthesis of Isothiocyanates from Dithiocarbamates or Alkyl Amines Using Chlorosilanes as Decomposition Reagents. Phosphorus, Sulfur, and Silicon and the Related Elements 182:3, pages 503-508.
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KeumShin Jung, HongJung Lee, HyunNam Song & JaeNyoung Kim. (1998) A Study on the Stability of 5,5-Diamino-substituted-1,4,2-oxathiazoline Derivatives. Synthetic Communications 28:10, pages 1879-1884.
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Articles from other publishers (16)

R. Nickisch, P. Conen, S. M. Gabrielsen & M. A. R. Meier. (2021) A more sustainable isothiocyanate synthesis by amine catalyzed sulfurization of isocyanides with elemental sulfur. RSC Advances 11:5, pages 3134-3142.
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Roberto Ballini & Alessandro Palmieri. (2018) Synthetic Procedures for the Preparation of Nitroalkanes. Advanced Synthesis & Catalysis 360:12, pages 2240-2266.
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L. Santhosh, S. Durgamma, Shekharappa Shekharappa & Vommina V. Sureshbabu. (2018) Staudinger/aza-Wittig reaction to access N β -protected amino alkyl isothiocyanates . Organic & Biomolecular Chemistry 16:26, pages 4874-4880.
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Mingchun Gao, Rongxuan Ye, Weijia Shen & Bin Xu. (2018) Copper nitrate: a privileged reagent for organic synthesis. Organic & Biomolecular Chemistry 16:15, pages 2602-2618.
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Srinivasarao Pinapati, Usharani Mandapati & Ramesh Raju Rudraraju. (2017) Iron-Mediated Desulphurization Towards the Synthesis of 2-Halo Aromatic Isothiocyanates. ChemistrySelect 2:1, pages 295-299.
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Ko Hoon Kim, Su Yeon Kim, Junseong Lee & Jae Nyoung Kim. (2016) An Efficient Synthesis of α-Isothiocyanato-α,β-unsaturated Esters from Morita-Baylis-Hillman Adducts. Bulletin of the Korean Chemical Society 37:4, pages 592-595.
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Li-Juan Yu, Farzaneh Sarrami, Robert J. O’Reilly & Amir Karton. (2015) Reaction barrier heights for cycloreversion of heterocyclic rings: An Achilles’ heel for DFT and standard ab initio procedures. Chemical Physics 458, pages 1-8.
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Robert J. O’Reilly & Leo Radom. (2009) Ab Initio Investigation of the Fragmentation of 5,5-Diamino-Substituted 1,4,2-Oxathiazoles. Organic Letters 11:6, pages 1325-1328.
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Gaofeng Bian, Weiguang Shan & Weike Su. (2019) A One-pot Preparation of Isothiocyanates from Amines Using Two Phosgene Substitutes: Bis-(trichloromethyl) Carbonate and Trichloromethyl Chloroformates. Journal of Chemical Research 2005:9, pages 585-586.
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R.A. Aitken. 2005. Comprehensive Organic Functional Group Transformations II. Comprehensive Organic Functional Group Transformations II 975 990 .
Jacek G Sośnicki & Sławomir Westerlich. (2002) Structurally dependent behavior of the nitromethyl group of aliphatic γ-nitrothioamides under nitrile oxide generation reaction conditions. Tetrahedron Letters 43:7, pages 1325-1328.
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Xuechun Zhang, Nouri Neamati, Young K Lee, Ann Orr, Ryan D Brown, Noel Whitaker, Yves Pommier & Terrence R BurkeJr.Jr.. (2001) Arylisothiocyanate-Containing esters of caffeic acid designed as affinity ligands for HIV-1 integrase. Bioorganic & Medicinal Chemistry 9:7, pages 1649-1657.
Crossref
Harashadas M. Mesheram, Srinivas Dale & J.S. Yadav. (1997) A general synthesis of isothiocyanates from dithiocarbamates using Claycop. Tetrahedron Letters 38:50, pages 8743-8744.
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Jae Nyoung Kim, Keum Shin Jung, Hong Jung Lee & Ji Suk Son. (1997) A facile one-pot preparation of isothiocyanates from aldoximes. Tetrahedron Letters 38:9, pages 1597-1598.
Crossref
Roberto Ballini. 1996. Structure and Chemistry (Part E). Structure and Chemistry (Part E) 117 184 .
J. N. KIM, J. H. SONG & E. K. RYU. (2010) ChemInform Abstract: A Convenient Synthesis of Isothiocyanates from Primary Nitroalkanes.. ChemInform 25:43.
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