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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 18
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Original Articles

MICROWAVE ASSISTED KNOEVENAGEL CONDENSATION: A FACILE METHOD FOR THE SYNTHESIS OF CHALCONES *

G. Venkat Reddy Organic Division-II, Indian Institute of Chemical Technology, Hyderabad, 500 007, India
,
D. Maitraie Organic Division-II, Indian Institute of Chemical Technology, Hyderabad, 500 007, India
,
B. Narsaiah Organic Division-II, Indian Institute of Chemical Technology, Hyderabad, 500 007, India
,
Y. Rambabu Organic Division-II, Indian Institute of Chemical Technology, Hyderabad, 500 007, India
&
P. Shanthan Rao Organic Division-II, Indian Institute of Chemical Technology, Hyderabad, 500 007, IndiaCorrespondence[email protected]
Pages 2881-2884 | Received 13 Sep 2000, Published online: 15 Aug 2006

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Sagar Tanpure, Vishvanath Ghanwat, Bipin Shinde, Kiran Tanpure & Shamrao Lawande. (2022) The Eggshell Waste Transformed Green and Efficient Synthesis of K-Ca(OH)2 Catalyst for Room Temperature Synthesis of Chalcones. Polycyclic Aromatic Compounds 42:4, pages 1322-1340.
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P.S. Kulkarni, P.M. Swami & P.K. Zubaidha. (2013) Calcium Hydroxide Is an Efficient Catalyst for Synthesis of Polyhydroxy Chalcones. Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry 43:5, pages 617-620.
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Dhruva Kumar, Suresh & JagirS. Sandhu. (2010) An efficient green protocol for the synthesis of chalcones by a Claisen–Schmidt reaction using bismuth(III)chloride as a catalyst under solvent-free condition. Green Chemistry Letters and Reviews 3:4, pages 283-286.
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Manoharan Karuppiah Pillai, Sooboo Singh & SreekanthB. Jonnalagadda. (2010) Solvent-Free Knoevenagel Condensation over Cobalt Hydroxyapatite. Synthetic Communications 40:24, pages 3710-3715.
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S. Kumar, M.S. Lamba & J.K. Makrandi. (2008) An efficient green procedure for the synthesis of chalcones using C-200 as solid support under grinding conditions. Green Chemistry Letters and Reviews 1:2, pages 123-125.
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B.P. V. Lingaiah, G. Venkat Reddy, T. Yakaiah, B. Narsaiah, S. N. Reddy, R. Yadla & P. Shanthan Rao. (2004) Efficient and Convenient Method for the Synthesis of Poly Functionalised 4H‐Pyrans. Synthetic Communications 34:23, pages 4431-4437.
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Vitaliy O. Chornous, Mykhaylo K. Bratenko & Mykhaylo V. Vovk. (2004) Microwave‐Assisted Synthesis of 3‐(4‐Pyrazolyl)propenoic Acids. Synthetic Communications 34:1, pages 79-83.
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Ojasvi Gupta, Tathagata Pradhan, Rohit Bhatia & Vikramdeep Monga. (2021) Recent advancements in anti-leishmanial research: Synthetic strategies and structural activity relationships. European Journal of Medicinal Chemistry 223, pages 113606.
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Ganapati D. Yadav & Dipti P. Wagh. (2020) Claisen‐Schmidt Condensation using Green Catalytic Processes: A Critical Review. ChemistrySelect 5:29, pages 9059-9085.
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Emília P.T. Leitão. (2020) Chalcones: Retrospective Synthetic Approaches and Mechanistic Aspects of a Privileged Scaffold. Current Pharmaceutical Design 26:24, pages 2843-2858.
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Duha Adnan, Bijender Singh, Surinder Kumar Mehta, Vinod Kumar & Ramesh Kataria. (2020) Simple and solvent free practical procedure for chalcones: An expeditious, mild and greener approach. Current Research in Green and Sustainable Chemistry 3, pages 100041.
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Sukanya Das, Bikoshita Porashar, Susmita Saikia & Ruli Borah. (2020) Brönsted Acidic Ionic Liquids Catalysed Sequential Michael‐Like Addition of Indole with Chalcones via Claisen‐Schmidt Condensation. ChemistrySelect 5:10, pages 3041-3047.
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V. Usha & V. Thangaraj. (2018) Synthesis and Characterisation of Substituted 2-benzofuranyl Chalcones. Materials Today: Proceedings 5:8, pages 16703-16715.
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Danish Khan, Sayeed Mukhtar, Meshari A. Alsharif, Mohammed Issa Alahmdi & Naseem Ahmed. (2017) PhI(OAc) 2 mediated an efficient Knoevenagel reaction and their synthetic application for coumarin derivatives. Tetrahedron Letters 58:32, pages 3183-3187.
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Renganathan Arulkumaran, Rajasekaran Sundararajan, Sambandamoorthy Vijayakumar, S. Palanivel Sakthinathan, Ramamoorthy Suresh, Dakshnamoorthy Kamalakkannan, Kaliyaperumal Ranganathan, Ganesan Vanangamudi & Ganesamoorthy Thirunarayanan. (2016) Solvent free synthesis, spectral correlation and antimicrobial activities of some 2 E 4′-nitrochalcones. Journal of Saudi Chemical Society 20, pages S122-S131.
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P. Janaki, K.G. Sekar & G. Thirunarayanan. (2016) Synthesis, spectral correlation and insect antifeedant activities of some 2-benzimidazole chalcones. Journal of Saudi Chemical Society 20:1, pages 58-68.
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Dinesh Sharma. (2013) An efficient and eco-friendly synthesis of quinolinyl chalcones under solvent-free conditions at room temperature. Research on Chemical Intermediates 41:2, pages 927-933.
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Dalip Kumar, N. Maruthi Kumar, Mukund P. Tantak, Maiko Ogura, Eriko Kusaka & Takeo Ito. (2014) Synthesis and identification of α-cyano bis(indolyl)chalcones as novel anticancer agents. Bioorganic & Medicinal Chemistry Letters 24:22, pages 5170-5174.
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K. Sathiyamoorthi, V. Mala, S.P. Sakthinathan, D. Kamalakkannan, R. Suresh, G. Vanangamudi & G. Thirunarayanan. (2013) Solvent-free synthesis, spectral correlations and antimicrobial activities of some aryl E 2-propen-1-ones. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy 112, pages 245-256.
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M. Subramanian, G. Vanangamudi & G. Thirunarayanan. (2013) Hydroxyapatite catalyzed aldol condensation: Synthesis, spectral linearity, antimicrobial and insect antifeedant activities of some 2,5-dimethyl-3-furyl chalcones. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy 110, pages 116-123.
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V. Mala, K. Sathiyamoorthi, SP. Sakthinathan, D. Kamalakkannan, R. Suresh, G. Vanangamudi & G. Thirunarayanan. (2013) Solvent-free synthesis, spectral correlations and antimicrobial activities of some 3,4-dimethoxy chalcones. QScience Connect:2013, pages 7.
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Yassine Riadi, Younes Abrouki, Rachid Mamouni, Mohammadine El Haddad, Sylvain Routier, Gérald Guillaumet & Saïd Lazar. (2012) New eco-friendly animal bone meal catalysts for preparation of chalcones and aza-Michael adducts. Chemistry Central Journal 6:1.
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G. Thirunarayanan, P. Mayavel & K. Thirumurthy. (2012) Fly-ash:H2SO4 catalyzed solvent free efficient synthesis of some aryl chalcones under microwave irradiation. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy 91, pages 18-22.
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Shyam J. Deshpande, Paul R. Leger & Stephen R. Sieck. (2012) Microwave synthesis of α-cyano chalcones. Tetrahedron Letters 53:14, pages 1772-1775.
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M. K. Pillai, S. Singh & S. B. Jonnalagadda. (2011) Solvent-free Knoevenagel condensation over iridium and platinum hydroxyapatites. Kinetics and Catalysis 52:4, pages 536-539.
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Parvin Kumar, Sunil Kumar, Khalid Husain & Ashwani Kumar. (2011) An efficient synthesis of pyrazole chalcones under solvent free conditions at room temperature. Chinese Chemical Letters 22:1, pages 37-40.
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Angela Patti & Sonia Pedotti. (2010) Hydrogenation of ortho-nitrochalcones over Pd/C as a simple access to 2-substituted 1,2,3,4-tetrahydroquinolines. Tetrahedron 66:30, pages 5607-5611.
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Christian Ruzié, Michael Krayer & Jonathan S. Lindsey. (2009) Fast and Robust Route to Hydroporphyrin−Chalcones with Extended Red or Near-Infrared Absorption. Organic Letters 11:8, pages 1761-1764.
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B. Venkat Lingaiah, G. Ezikiel, T. Yakaiah, G. Venkat Reddy & P. Shanthan Rao. (2006) Gadolinium(III) chloride: a novel and an efficient reagent for the synthesis of homoallylic alcohols. Tetrahedron Letters 47:26, pages 4315-4318.
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M. K. Bratenko, V. A. Chornous & M. V. Vovk. (2006) Polyfunctional pyrazoles. 4. Synthesis of 3-[3-aryl-1-(2-ethoxycarbonyl)-4-pyrazolyl]acrylic and-propionic acids. Chemistry of Heterocyclic Compounds 42:5, pages 600-604.
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M. Nüchter, B. Ondruschka, D. Weiß, R. Beckert, W. Bonrath & A. Gum. (2005) Contribution to the Qualification of Technical Microwave Systems and to the Validation of Microwave‐Assisted Reactions and Processes. Chemical Engineering & Technology 28:8, pages 871-881.
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M. Nüchter, U. Müller, B. Ondruschka, A. Tied & W. Lautenschläger. (2003) Microwave‐Assisted Chemical Reactions. Chemical Engineering & Technology 26:12, pages 1207-1216.
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V.B. HelaviS.B. SolabannavarU.V. DesaiR.B. Mane. (2019) MicrowavE Assisted hydrolysis of Meldrum'S Acid Derivatives and decarboxylation of Derived Malonic Acids. Journal of Chemical Research 2003:3, pages 174-175.
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G. Venkat Reddy, D. Maitraie, B. Narsaiah, Y. Rambabu & P. Shanthan Rao. (2010) ChemInform Abstract: Microwave Assisted Knoevenagel Condensation: A Facile Method for the Synthesis of Chalcones.. ChemInform 33:2.
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